124 resultados para Pulse Transit Time
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Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
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Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
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Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
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Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)
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Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)
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Pós-graduação em Ciência e Tecnologia Animal - FEIS
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Radial profiles are reported of average and rms temperature in a propane flame for the first, second, and third acoustic modes at four different axial positions above the burner in a Rijke-tube combustor. Selected plots of the power spectral density (PSD) of temperature fluctuations are also reported. These radial profiles are then compared to similar ones made in the same flame, but in the absence of the acoustic field. Visual observations and photographs of the flame showed a remarkable change in flame height and structure with the onset of acoustic oscillations. This reduction in flame length, caused by the enhanced mixing due to the acoustic velocity fluctuations, gave rise to higher and lower average and rms temperatures near or well above the burner, respectively. In general, the PSD plots had a broad frequency content. The general trend was a decrease in magnitude with an increase in frequency. All cases presented broad-band peaks at around 5 Hz related to the flame flickering phenomenon. Preferred frequencies were observed in the oscillating PSD plots related to the fundamental frequency as well as subharmonics in the tube. (C) 2000 Elsevier B.V. Ltd. All rights reserved.
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The degradation behaviour of SnO(2)-based varistors (SCNCr) due to current pulses (8/20 mu s) is reported here for the first time in comparison with the ZnO-based commercial varistors (ZnO). Puncturing and/or cracking failures were observed in ZnO-based varistors possessing inferior thermo-mechanical properties in comparison with that found in a SCNCr system free of failures. Both systems presented electric degradation related to the increase in the leakage current and decrease in the electric breakdown field, non-linear coefficient and average value of the potential barrier height. However, it was found that a more severe degradation occurred in the ZnO-based varistors concerning their non-ohmic behaviour, while in the SCNCr system, a strong non-ohmic behaviour remained after the degradation. These results indicate that the degradation in the metal oxide varistors is controlled by a defect diffusion process whose rate depends on the mobility, the concentration of meta-stable defects and the amount of electrically active interfaces. The improved behaviour of the SCNCr system is then inferred to be associated with the higher amount of electrically active interfaces (85%) and to a higher energy necessary to activate the diffusion of the specific defects.
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A solid paraffin-based carbon paste electrode modified with 2-aminothiazole organofunctionalized silica (SiAt-SPCPE) was applied to Ni2+ determination in commercial ethanol fuel samples. The proposed method comprised four steps: (1) Ni2+ preconcentration at open circuit potential directly in the ethanol fuel sample, (2) transference of the electrode to an electrochemical cell containing DMG, (3) differential pulse voltammogram registering and (4) surface regeneration by polishing the electrode. The proposed method combines the high Ni2+ adsorption capacity presented by 2-aminothiazole organofunctionalized silica with the electrochemical properties of the Ni(DMG)2 complex, whose electrochemical reduction provides the analytical signal.All experimental parameters involved in the proposed method were optimized. Using a preconcentration time of 20 min, it was obtained a linear range from 7.5 x 10(-9) to 1.0 x 10(-6) mol L-1 with detection limit of 2.0 x 10(-9) mol L-1. Recovery values between 96.5 and 102.4% were obtained for commercial samples spiked with 1.0 mu mol L-1 Ni2+ and the developed electrode was totally stable in ethanolic solutions. The contents of Ni2+ found in the commercial samples using the proposed method were compared to those obtained by graphite furnace atomic absorption spectroscopy by using the F- and t-test. Neither the F- nor t-values exceeded the critical values at 95% confidence level, confirming that there are not statistical differences between the results obtained by both methods. These results indicate that the developed electrode can be successfully employed to reliable Ni2+ determination in commercial ethanol fuel samples without any sample pretreatment or dilution step. (c) 2006 Elsevier B.V. All rights reserved.
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Solid paraffin-based carbon paste electrodes modified with 2-aminothiazole organofunctionalized silica have been applied to the anodic stripping determination of copper ions in ethanol fuel samples without any sample treatment. The proposed method comprised four steps: (1) copper ions preconcentration at open circuit potential directly in the ethanol fuel sample; (2) exchange of the solution and immediate cathodic reduction of the absorbate at controlled potential; (3) differential pulse anodic stripping voltammetry; (4) electrochemical surface regeneration by applying a positive potential in acid media. Factors affecting the preconcentration, reduction and stripping steps were investigated and the optimum conditions were employed to develop the analytical procedure. Using a preconcentration time of 20 min and reduction time of 120 s at -0.3 V versus Ag/AgCl(sat) a linear range from 7.5 x 10(-8) to 2.5 x 10(-6) mol L(-1) with detection limit of 3.1 x 10(-8) mol L(-1) was obtained. Interference studies have shown a decrease in the interference effect according to the sequence: Ni > Zn > Cd > Pb > Fe. However, the interference effects of these ions have not forbidden the application of the proposed method. Recovery values between 98.8 and 102.3% were obtained for synthetic samples spiked with known amounts of Cu(2+) and interfering metallic ions. The developed electrode was successfully applied to the determination of Cu(2+) in commercial ethanol fuel samples. The results were compared to those obtained by flame atomic absorption spectroscopy by using the F-test and t-test. Neither F-value nor t-value have exceeded the critical values at 95% confidence level, confirming that there are no significant differences between the results obtained by both methods. (c) 2006 Elsevier B.V. All rights reserved.
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Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
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Calathea louisae is an herbaceous ornamental plant native of Brazil whose cut foliage has potential to be used as a new product for the local ornamental market, as well as the international market, due to its decorative dark green leaves with greenish white splotches along midrib, and purple undersides. The objective of this study was to evaluate pulse treatments of benzyladenine and gibberellic acid for maintaining quality and extending keepability of foliage. The experiment was conducted in a complete randomized design with three replications (three stems in each vase) and seven treatments: distilled water (control) and pulsing cut petioles in benzyladenine or gibberellic acid for 4 h at 100, 250 and 500 mg L-1. The senescence symptoms were characterized by leaf rolling and a decrease in the angle formed between leaf and petiole as a response to water stress. Gibberellic acid or benzyladenine pulse treatments (250 and 500 mg L-1) significantly extended the longevity of cut foliage compared to the control. Gibberellic acid pulse (250 and 500 mg L-1) maintained leaves' green coloration and brightness for a longer time compared to control and benzyladenine pulse. Pulsing with gibberellic acid or benzyladenine (at all tested concentrations) maintained upright leaves for a longer time, showing a significantly higher angle between leaf and petiole compared to control. Foliage pulsed with gibberellic acid (500 mg L-1) showed a significantly higher leaf relative water content, a significantly smaller loss of accumulated fresh mass percentage compared to control and other gibbberellic acid and benzyladenine treatments.
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Marantaceae leaves have a contrasting color pattern and a decorative design which are interesting traits for its use as cut foliage. No postharvest research has been carried out on the potential as cut foliage for species of Ctenanthe, a member of the Marantaceae. Grey-maranta (Ctenathe setosa) is an herbaceous ornamental plant native of Brazil whose cut foliage has potential to be used as new crop product for local and international ornamental markets. The objective of this study was to evaluate pulse treatments to extend the longevity of foliage. The experiment was conducted in a complete randomized design with three replications and eight treatments: distilled water; pulsing cut petioles-ends in citric acid (pH = 2.8/1h); 2% sucrose (4h); 1% sucrose plus 200 mg L-1 citric acid (4h); 0.01% Tween® 20 (4h); 100 mg L -1 benzyladenine plus 0.01% Tween® 20 (4h); 100 mg L-1 gibberellic acid plus 0.01% Tween® 20 (4h); and maintenance of cut petiole in holding solution with commercial sodium hypochlorite (0.5 mL L-1). The senescence symptoms were mainly characterized by leaf rolling and by a decrease in the angle formed between leaf and petiole as a response to water deficit stress. Gibberellic acid or benzyladenine pulse treatments significantly extended longevity (6 days compared to control) and maintained leaves' green coloration and brightness for a longer time compared to control. However, only the benzyladenine plus Tween® 20 pulse maintained leaves in an erect form for a longer time, showing a significantly higher angle between leaf and petiole compared to control. Also, foliage pulsed with benzyladenine plus Tween® 20 showed a significant smallest loss of accumulated fresh mass percentage compared to control by the T test as to parallelism of treatments lines.
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AC Biosusceptometry (ACB) was previously employed towards recording gastrointestinal motility. Our data show a reliable and successful evaluation of gastrointestinal transit of liquid and solid meals in rats, considering the methods scarcity and number of experiments needed to endorsement of drugs and medicinal plants. ACB permits real time and simultaneous experiments using the same animal, preserving the physiological conditions employing both meals with simplicity and accuracy. © 2012 Quini et al.; licensee BioMed Central Ltd.
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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)