81 resultados para <0.2 µm

em Chinese Academy of Sciences Institutional Repositories Grid Portal


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为了重建东亚季风区域2.5MaB.P.前后植被和气候变化的历史,更好地了解低纬度地区植被变化及其对全球变化的响应,本研究选择了南海南部ODP1143站深海沉积物中的孢粉样品进行研究。通过高分辨率(7ka)的孢粉样品的分析研究,建立起3.0~2.0MaB.P.时段南海深海沉积孢粉组合序列,系统建立了这一时段植被演替序列。在此基础上,重点研究了2.5MaB.P.前后气候变化在南海周边地区植被演替中的响应,为探索和揭示东亚古季风及古环境演变提供了孢粉学依据。 ODP 1143站位于南沙海区,北纬9º22´,东经113º17´,深海柱状样采于水深2772m的大陆坡。本研究以生物地层学和氧同位素年代学为依据建立了年龄框架,对1143站135~95m(3.0~2.6 Ma B. P.)深海沉积中的孢粉样品进行了分析,建立了3.0~2.0MaB.P.时段南海深海沉积孢粉组合序列。孢粉样品处理方法主要是用盐酸去掉钙质和氢氟酸浸泡溶解硅质后,再用筛子将样品在超声波发生器中震荡过滤。孢粉的鉴定和统计在光学透视显微镜下完成。研究结果表明: 1、孢粉谱的主要特征是沉积率变化显著。与3.0~2.6 Ma B. P. 相比,2.6~2.0 Ma B. P.各类型花粉及孢子沉积率均有显著提高。该结果表明2.6 Ma B. P.南海海平面有显著下降,可与北半球冰盖形成、东亚季风增强相对应。 2、2.6 Ma B. P.以来,各类型孢粉沉积率变化与深海氧同位素分期相对应,代表了多次冰期-间冰期旋回。该结果表明南海海平面曾有多次上升和下降。 3、频谱分析结果表明,3.0~2.0 Ma B. P.存在0.1 Ma(偏心率)和46.9ka(斜率)的周期。

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半导体材料开放实验室基金,国家自然科学基金

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于2010-11-23批量导入

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掺杂的CeO2基固体电解质因其在中低温条件下(500 ̄700℃)具有高氧离子电导率而成为有希望的IT-SOFCs(intermediate temperature-solid oxide fuel

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Microstructures and mechanical properties of the peak-aged Mg-4.5Zn-xGd (x = 0, 2, 3 and 5 wt.%) alloys have been investigated. The results showed that grain size increased with increasing Gd. Phase analysis showed that MgZn2 phase was observed in the Mg-4.5Zn alloy. While with Gd additions, Mg3Gd and Mg3Gd2Zn3 phases formed, and the volume fraction of the Mg3Gd2Zn3 phase increased with increasing Gd. Tensile test results indicated that the optimal mechanical properties were obtained in the Mg-4.5Zn-2Gd alloy, and the ultimate tensile strength and yield strength were 215 MPa and 121 MPa, respectively.

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The Ruddlesden-Popper series of compounds Ca4Mn3-xNbxO10(x = 0-0.2) have been prepared by solid-state methods. Structural, magnetic, electrical, and magnetoresistive studies were performed on the compounds. Nb doping caused increases in both unit cell volume and octahedral distortion. The magnetization measurements indicated that the doped samples displayed ferromagnetism-like behavior, which could be explained by the double-exchange interaction between Mn4+ and Mn3+ induced by the charge-compensation effect.

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Mg-5Y-3Nd-0.6Zr-xGd (x = 0, 2 and 4 wt.%) alloys were prepared by metal mould casting technique, the structures and mechanical properties were investigated. The alloys were mainly composed of alpha-Mg solid solution and beta-phase. With increasing Gd content, Mg5RE phase increased and the grain was refined. The Mg-5Y-3Nd-2Gd-0.6Zr alloy exhibited highest ultimate tensile strength and Mg-5Y-3Nd-0.6Zr alloy showed highest yield strength at room temperature. With increasing amount of Gd, the thermal resistance was improved. The Mg-5Y-3Nd-4Gd-0.6Zr alloy exhibited highest UTS and YS at 250 degrees C, they were about 1.27 times higher than those of Gd-free alloy, which was mainly attributed to the increase of the beta-phase and Mg5RE strengthening phase.

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Bulk novel cemented carbides (W1-xAlx)C-10.1 vol% Co (x = 0.2, 0.33, 0.4, 0.5) are prepared by mechanical alloying and hot-pressing sintering. Hot-pressing (HP) is used to fabricate the bulk bodies of the hard alloys. The novel cemented carbides have good mechanical properties compared with WC-Co. The density and operating cost of the novel material is much lower than a WC-Co system. The material is easy to process and the processing leads to nano-scaled, rounded, particles in the bulk material. The hardness of (W1-xAlx)C-10.1 vol% Co (x = 0.2, 0.33, 0.4, 0.5) hard material is 20.37, 21.16, 21.59 and 22.16 GPa, and the bending strength is 1257, 1238, 1211 and 1293 MPa, with the aluminum content varying from 20% to 50%. The relationship between the microstructure and the mechanical properties of the novel hard alloy is also discussed.

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The new compounds La2-xCaxMo1.7W0.3O9-delta (0 <= x <= 0.2) in which La3+ substituted with Ca2+ were synthesized by dry-chemistry techniques based on the oxygen Ionic conductor La2Mo1.7W0.3O9. The new series were characterized by X-ray Diffraction (XRD), Raman and X-ray Photoelectron Spectroscopy (XPS) and the electrical conductivity of samples were investigated by AC impedance spectroscopy. The lattice parameters were reduced due to the smaller atomic radius of the Ca2+ compared with that of the La3+. Furthermore, Additional oxygen vacancies were introduced into La2Mo1.7W0.3O9 lattice by substitution, and then the oxygen ionic conductivity was increased. At 550 degrees C, the conductivity increased 89.9%, that is, from 0.79 x 10(-4) S center dot cm(-1) (x=0) to 1.5 X 10(-4)S center dot cm(-1) (x=0.16, 0.2).