169 resultados para 319.272053


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Dichlorosilane, a gas at normal temperature with a boiling point of 8.3 degrees C, is very difficult to sample and detect using conventional methods. We reduced phosphorus in dichlorosilane to PH3 by hydrogen at high temperature, then PH3 was separated from chlorosilanes by NaOH solution and from other hydrides by chromatographic absorption. Thus the problem of interference of chlorosilanes and other hydrides was overcome and PH, was measured by a double flame photometric detector at 526 nm. This method was sensitive, reliable and convenient and the sensitivity reached as low as 0.04 mu g/l.

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为了生长制作器件所需的外延片,采用低压金属有机物化学气相沉积方法在半绝缘InP衬底上生长了InP/InGaAs异质结双极晶体管(HBT)结构、1.55μm多量子阱激光二极管以及两者集成的光发射光电集成电路材料结构.激光器结构的生长温度为655℃,有源区为5个周期的InGaAsP/ InGaAsP多量子阱(阱区λ=1.6μm,垒区λ=1.28μm);HBT结构则采用550℃低温生长,其中基区采用Zn掺杂,掺杂浓度约为2×1019cm-3.对生长的各种结构分别进行了X射线双晶衍射,光致发光谱和二次离子质谱仪的测试,结果表明所生长的材料结构已满足制作器件的要求.

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提出一种新的牺牲层工艺。先将阳极氧化生成的多孔硅在300℃的氮气氛下进行退火以稳定其多孔结构,然后将其在700℃下氧化成为具有多孔结构的二氧化硅。用氧化的多孔硅材料作为牺牲层材料,既可以保留多孔硅牺牲层材料释放迅速的优点,又克服了多孔硅在释放时的局限性。实验运用氧化的多孔硅材料作牺牲层成功制备了悬空振膜和悬臂梁结构。

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Chinese Academy of Sciences (ISCAS)

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本文通过传统和现代微生物生态学方法,从土壤微生物数量、土壤底物诱导呼吸强度和微生物群落多样性角度,评价了长期污灌所致PAHs污染对土壤微生物特征的影响。结果发现沈抚灌区农田PAHs总量在表层为612.3-6362.81μg•kg-1干土,在亚表层为319.5-4318.51μg•kg-1干土。土壤微生物主要类群、功能群数量、微生物生物量碳和代谢商与土壤PAHs污染程度无明显相关性,土壤底物诱导呼吸强度和所试土壤酶与PAHs含量呈显著正相关,微生物商与PAHs含量呈显著负相关,可以作为土壤PAHs污染评价的敏感生化指标之一。污染稻田土壤细菌群落中优势菌群为β-和γ-变形细菌亚纲的成员,中度PAHs土壤的分支杆菌多样性指数较重度和轻度的略高,PAHs污染使一种或几种分支杆菌得到富集。长期污水灌溉造成土壤固氮细菌种群多样性降低,清水灌溉一段时间后,固氮细菌种群结构得到不同程度的恢复,但是,即使清灌不能使其种群结构得到完全恢复。 通过富集得到一株高效降解芘的细菌N12,经鉴定确认为分支杆菌。经10天培养菌株可将100mg•l-1芘降解97.84%。还可降解菲、苊、芴,不能降解萘、蒽和苯并[a]芘。污染土壤修复实验表明,单一接种菌剂对芘的降解率为57.42%,含N12的混合接种菌剂对芘的降解率为61.11%。

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