973 resultados para 700


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在封闭的植物培养箱中,通过盆栽实验,研究了红豆草和土壤氮含量对CO2浓度增加的响应.结果表明,与正常CO2浓度(355~370μmol·mol-1)相比,CO2浓度升高(700μmol·mol-1),植物生物量增加25·1%(P<0·01),但植物体氮浓度降低25·3%(P<0·001),植物全氮没有显著的变化.经3个月盆栽实验后,与原始土壤相比,两种CO2浓度处理土壤全N、NO3--N和NH4+-N都有所降低,而土壤微生物氮则显著增加,这可能与植物生长有关.不同CO2浓度处理土壤NH4+-N浓度基本一致,但在高CO2浓度下,土壤NO3--N浓度显著降低,而微生物生物氮显著增加.对整个土壤-植物系统而言,盆栽实验后,整个系统全氮有少量增加,但变化不显著,特别是在高CO2浓度条件下,土壤-植物系统全氮最大,这可能与培养材料红豆草为豆科植物,而且在高CO2浓度下生物量增加,导致氮的固定量增加有关.

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采用田间实验研究了施用氮肥对设施条件下大青菜生长发育和产量,以及对土壤硝酸盐含量累积分布的影响。结果表明,在施氮肥0~500 kg hm-2范围内,氮肥施用量越大,产量越高,但到达一定量时,便不能再促进产量的提高,反而会引起减产。土壤铵态氮含量随着土壤剖面向下不断下降,表层的铵态氮含量较高,土壤硝态氮含量在整个土壤剖面的分布变化较小,但也是从表层向下处于一种缓慢减少的趋势,铵态氮的累积主要集中在上部土壤剖面,硝态氮的累积分布在整个土壤剖面,土壤硝态氮含量随施肥量增加而增加;氮肥施用量对硝酸盐含量有很大影响。在施氮肥0~700kg hm-2范围内,氮肥施用量越多,大青菜硝酸盐含量越高。

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在长白山站以开顶箱方式对4 年生长白松连续4 个生长季进行CO2 处理,包括700 和500 μmolmol-1 高浓度CO2,以及接受空气CO2的对照箱和不扣箱的裸露地条件(约350 μmolmol-1 CO2),通过测定气孔导度(gs),ci/ca比及气孔数量等指标评价气孔对高浓度CO2的响应。气孔导度及ci/ca比的转换实验表明,在各自生长CO2下和在相同测定CO2 下进行比较时,生长在高浓度CO2 下植株的气孔导度要高于空气CO2 下对照组植株的气孔导度(除700 μmol mol-1 CO2 下的植株在生长CO2 浓度下及在350 μmol mol-1 CO2 下测定时的气孔导度低于裸地植株外)。在各自生长CO2浓度下测定时,高浓度CO2下植株的ci/ca比低于对照组植株,但在相同测定CO2浓度下比较时,却是高浓度CO2下植株的ci/ca高于对照组植株的ci/ca比。高浓度CO2下植株与对照组植株在每单位长度气孔数量上无明显差异,但高浓度CO2通过降低气孔线数使长白松当年生针叶的总气孔数量降低,并且改变了气孔在针叶上、下表面的分配模式。表4 参18。

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3年生白桦同时接受3种外源糖溶液(蔗糖、果糖、葡萄糖)和3种高浓度CO2(700、1400、2100μL L-1CO2)处理。处理1个月后,测定了叶片的总糖、蔗糖、果糖和蛋白质含量。结果表明:在700μL L-1和1400μL L-1 CO2下,外源糖溶液增加了叶片的可溶性糖和蛋白质含量,其中外源蔗糖的效果最好;外源糖溶液与2100μL L-1CO2结合,会抑制叶片积累总糖和蛋白质;在700μL L-1和1400μL L-1CO2下,喷施葡萄糖、果糖的叶片在蛋白质含量上没有明显差别;;同700、1400μL L-1CO2相比,除喷施果糖植株外,2100μL L-1CO2明显增加了叶片的总糖、蔗糖、果糖和蛋白质含量;;在喷施同种外源糖溶液的情况下,叶片的糖含量与CO2浓度呈正相关性。图6参7。

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针对现有软件发布方式主要以开发者的角度进行软件开发后生命周期管理所存在的问题,提出了更为合理的以用户的角度进行软件开发后生命周期管理的思想,建立了一种新的软件发布机制体系结构。该发布机制试图解决如下问题:让用户透明地使用软件,即用户不需要显式地进行软件的安装、更新和卸载;支持软件的即点即用和使用态发布,使用态发布指安装了某软件的计算机可以作为该软件的发布源;使得系统重装后能够以较小的代价恢复到指定的状态点。最后,分析了软件动态更新和分布式软件系统发布所应解决的问题。

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The double perovskite oxide Sr2CrNbO6 has a cubic structure according to powder X-ray diffraction. After reducing in CO, Sr2CrNbO6 still exhibited a cubic structure refined by Rietveld technique. The TG analysis indicated that Sr2CrNbO6 loses 0.127 oxygen per formula unit from 400 to 700 degrees C in H-2. The morphology and compositions of this ceramic did not significantly change on reduction

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掺杂的CeO2基固体电解质因其在中低温条件下(500 ̄700℃)具有高氧离子电导率而成为有希望的IT-SOFCs(intermediate temperature-solid oxide fuel

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A series of (alpha-diimine)nickel(II) complexes [ArN = C(Nap)C = NAr]NiBr2 (Nap = 1,8-naphthdiyl, Ar = 2,6-Me2C6H3, 3a; Ar = 2,4,6-Me3C6H2 3b; Ar = 2,6-Me-2-4-tBuC(6)H(2), 3c; Ar 2,6-Me-2-4-BrC6H2, 3d; Ar = 2,6-Me-2-4-ClC6H2, 3e; Ar 2,6-iPr(2)C(6)H(3), 3f; Ar = 2,4,6-iPr(3)C(6)H(2), 3g; Ar = 2,6-iPr-4-BrC6H2, 3h) have been synthesized, characterized, and investigated as precatalysts for ethylene polymerization in the presence of modified methylaluminoxane (MMAO).

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Liquid polybutadiene with desirable 1,2-units content was synthesized by Co(naph)(2)-Al-2(C2H5)(3)Cl-3-P(OPh)(3) catalyst system. It was shown that liquid polybutadiene having adequate 1,2-unit content (vinvl =35%-40%) molecular weight(M-n = 700-3500), and acceptabele conversion(>= 55%) can synthesized after optimizing polymerization conditions.

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采用两步加热高温固相法合成了掺杂Nd3+的LiFe1-xNdxPO4/C复合材料(x=0,0.01,0.02,0.04,0.06,0.08)。用TG-DSC对前驱体进行分析和SQUID(超导量子干涉仪)对样品中Fe3+的磁性测定,优化了合成工艺条件;采用XRD、FE-SEM、EDS等方法分析了样品的结构并对其电化学性能进行了测试。结果表明:LiFe1-xNdxPO4/C复合材料具有橄榄石型结构;当Nd3+的掺杂量6%(物质的量分数)、煅烧温度700℃、煅烧时间16 h时,样品在0.2C(1C=170.0 mA.g-1)电流密度下的最大放电比容量可达165.2 mAh.g-1,循环100次后的容量保持率仍为92.8%,在1C、2C、5C下的最大放电比容量分别为146.8、125.7和114.8 mAh.g-1。通过测定样品在不同较低倍率下的放电比容量,采用外推法得出制备样品的实测理论比容量为168.7 mAh.g-1。

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Starburst-substituted hexaazatriphenylene Compounds have been designed and synthesized by introducing various peripheral aryl substituents to the central heterocyclic core. The effects of various substituent groups on the photophysical and electrochemical properties of the substituted hexaazatriphenylene have been investigated. Significant red-shifts of the absorption peak (from 413 nm to 530 nm) and emission peak (from 432 nm to 700 nm) were observed when the electron-donating ability of the aryl substituents was increased, corresponding to a decrease in the band gap from 2.90 eV to 2.05 eV. Introducing bulky substituents with weak electron-donating ability enhances the fluorescence quantum yield from 23% to 87%. In contrast, incorporating aryl substituents with strong electron-donating ability decreases the fluorescence quantum yield.

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A simultaneous electrochemiluminescence (ECL) and electrochemical (EC) detection scheme for NACE was presented for fast analysis of tertiary amines. Both ECL and EC signals were generated at the same Pt electrode. Triethylamine (TEA), tripropylamine (TPrA), chlorpromazine, promethazine, and dioxopromethazine (DPZ) were selected to validate NACE-ECL/EC dual detection strategy. The linear ranges for TEA and TPrA were 0.01-500 and 0.01-10 mu M with the detection limits of 8.0 and 5.0 nM (S/N=3), respectively. The RSDs (n = 6) of the migration time and the ECL intensity for 1 mu M TEA and 0.5 mu M TPrA were 0.1 and 2.8%, and 0.2 and 1.8% with theoretical plate numbers of 180 000 and 700 000 per meter, respectively. These two analytes could be separated within 92 s and the Pt electrode did not need reactivation during the experiments.

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Carbon black and titanium dioxide supported iron tetraphenylporphyrin (FeTPP/TiO2/C) catalysts for oxygen reduction reaction (ORR) were prepared by sol-gel and precipitation methods followed by a heat-treatment at temperatures of 400-1000 degrees C. The FeTPP/C and TiO2/C were also studied for comparison. The FeTPP/TiO2/C pyrolyzed at 700 degrees C exhibits significantly improved stability while maintaining high activity towards ORR in comparison with the FeTPP/C counterpart. The electrochemical study combined with XRD, XPS, and SEM/EDX analyses revealed that the appropriate dispersion of TiO2 on the surface of FeTPP/TiO2/C catalysts, which depending on heat-treatment temperature, plays a crucial role in determining the activity and stability of catalysts.

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One-dimensional Mn2+-doped ZnGa2O4 nanofibers were prepared by a simple and cost-effective electrospinning process. X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), thermogravimetric and differential thermal analysis (TG-DTA), scanning electron microscopy (SEM), energy-dispersive X-ray spectrum (EDS), transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), photoluminescence (PL) and cathodoluminescence (CL) spectra as well as kinetic decays were used to characterize the samples. SEM results indicated that the as-formed precursor fibers and those annealed at 700 degrees C are uniform with length of several tens to hundred micrometers, and the diameters of the fibers decrease greatly after being heated at 700 degrees C. Under ultraviolet excitation (246 nm) and low-voltage electron beams (1-3 kV) excitation, the ZnGa2O4:Mn2+ nanofibers presents the blue emission band of the ZnGa2O4 host lattice and the strong green emission with a peak at 505 nm corresponding to the T-4(1)-(6)A(1) transition of Mn2+ ion.