Desenvolvimento de argamassa para restauração utilizando resíduo do polimento do porcelanato

The coatings mortars are essential elements of building structures because they execute an important role in protecting walls and are particularly exposed to aggressive action responsible for its degradation over time. The importance of wall coverings has been the subject of discussion and analysis in the conservation and rehabilitation of old buildings. Are sometimes removed and replaced with inappropriate solutions of constructive point of view or architecture. The most commonly used coatings on walls of old buildings is based on traditional hydraulic lime mortars. The present study aims at the formulation of new lime- based mortars and aerial fine aggregate, in order to contribute to a better field of conservation and restoration mortar coating of old buildings. Residue was used for polishing porcelain as fine aggregate, replacing the aggregate (sand), in percentages 05-30% by mass. We conducted a thorough evaluation of the mortar properties in fresh and hardened state by comparing the performance of the same with a reference mortar. The residue used was characterized as the density, bulk density, and particle size laser, scanning electron microscopy, X-ray diffraction and X-ray fluorescence. Formulations were produced 7, 6 with residue and one commonly used formulation, which served as a reference. In the formulations of lime mortars air (hydrated lime powder CH-I) has been adopted a stroke volume (1:3) with constant binder, was varied and the water / binder and aggregate and waste. For evaluation of mortars fresh, proceeded to consistency analysis, specific gravity, water retention and air content embedded. In the hardened state assays were performed in specific gravity, water retention, modulus of elasticity, tensile strength in bending, compressive strength, water absorption by capillary action, adhesion, tensile strength, resistance to shrinkage and salts by of crystallization trials with resources chloride solution, nitrate and sulfate all sodium in prismatic at 90 days of age, in addition to the micro structural analysis of mortars. Based on the results we can see that the mortar formulated with 10% content of waste and the reference free retraction feature more stable closer to neutrality. The composition of 10% was obtained better performance against the action of the salt crystallization. The mortar with 15% residue obtained better density, lower air content embedded and high capacity for water retention developing good workability. The replacement of 20% of waste generates a satisfactory utilization of resistance to compression, flexion and traction grip the base. And, finally, it can be seen that the mortar with 10, 15 and 20% residual show, in principle, good suitability as coatings, thus enabling a final result consistent with durability, workability and aesthetics developing therefore a material with better performance to repair or replace existing mortars in old buildings

Avaliação da incorporação combinada dos resíduos de cascalho de perfuração de poço de petróleo e de polimento do porcelanato em cerâmica vermelha

Among the industries, those that produce ceramic porcelain for use in construction industry and oil, during the exploration and production period, play an important role in the production of waste. Much research has been carried out both by academia and the productive sector, sometimes reintroducing them in the same production line that generated them, sometimes in areas unrelated to their generation, as in the production of concrete and mortar for the construction, for example, but each one in an isolated way. In this research, the aim is to study the combined incorporation of the waste drill cuttings of oil well and the residue of the polishing of porcelain, generated in the final stage of finishing of this product in a clay matrix, for the production of red pottery, specifically bricks, ceramic blocks and tiles. The clay comes from the municipality of São Gonçalo, RN, the drilling waste is from the Natal basin, in Rio Grande do Norte, and the residue of the polishing proceeds from a ceramic porcelain of the State of Paraíba. For this purpose, we used a mixture of a plastic clay with a non-plastic, in a ratio of 50% each, settling formulations with the addition of these two residues in this clay matrix. In the formulations, both residues were incorporated with a minimum percentage of 2.5% and maximum of 12.5%, varying from 2.5% each, in each formulation, which the sum of the waste be no more than 15%. It should be noted that the residue of the polishing of ceramic porcelain is a IIa class (not inert). The materials were characterized by XRF, XRD, TG, DTA, laser granulometry and the plasticity index. The technological properties of water absorption, apparent porosity, linear shrinkage of burning, flexural tensile strength and bulk density were evaluated after the sintering of the pieces to 850 °C, 950 °C and 1050 °C, with a burning time of 3 hr, 3 hr and 30 minutes, and 3 hr and 50 minutes, respectively, with a heating rate of 10 °C/minute, for all formulations and landing of 30 minutes. To better understand the influence of each residue and temperature on the evaluated properties, we used the factorial planning and its surfaces of response for the interpretation of the results. It was found that the temperature has no statistical significance at a 95% of reliability level in flexural tensile strength and that it decreases the water absorption and the porosity, but increases the shrinkage and the bulk density. The results showed the feasibility of the desired incorporation, but adjusting the temperature to each product and formulation, and that the temperatures of 850 °C and 950 °C were the one that responded to the largest number of formulations

Estudo de Matérias-Primas do Rio Grande do Norte para Uso em Revestimento Poroso: Influência do teor de dolomita e temperatura de calcinação nas propriedades físico-mecânicas

The state of Rio Grande do Norte presents a great potentiality for the production of ceramic tiles because of having natural raw material in quantity and quality making its economical exploration possible, beyond the great energetic differential of the state, the natural gás. This works aims to study the influence of the dolomite and granulometry concentration and calcinations temperature in the obtaining of formulations for porous coverings which have to be coherent to the project,s specifications. The experiments have involved the physical-chemical and mineralogical characterizations of raw materials and mechanical tests in the dry and burnt proof bodies preceding a mixture experiment planning with the use of the response surface methodology, in order to get the best raw materials combinations to produce a ceramic mass with specific properties. The twelve ceramic masses studied in this work were prepared by the via dry process, characterized, shaped by uniaxial pressing and sinterized in the temperatures of 940ºC, 1000ºC, 1060ºC, 1120ºC and 1180ºC, using a fast burning cycle. The crystalline phases formed during the sintering in the temperatures in study have revealed the presence of anorthite and diopside beyond quartz with a remaining phase. These phases were the main responsible ones by the physical- mechanical properties of the sinterized proof bodies. The proof bodies after the sintering stage have presented water absorption higher than 10% and a good dimensional stability in all studied temperatures. However, the flexural breaking strength results in the temperatures of 940ºC, 1000ºC and 1060ºC, under the temperature zone of the vitrification of ceramic whiteware do not reach the flexural breaking strength specific for the porous wall tile (15 MPa), but in the temperature of 1120ºC next to the vitrification temperature zone, some whiteware ceramic (formulations) has reached the specified value for the porous wall tile. The results of this work have showed that the studied raw materials have great importance for used in the production of porous wall tiles (BIII)

Aproveitamento de resíduo de beneficiamento do caulim na produção de porcelanato cerâmico

Nowadays, industries from all sectors have great concerns over the disposition of the residues generated along the productive process. This is not different in the mineral sector, as this generates great volumes of residues. It was verified that the kaolin improvement industry generates great volumes of residue basically constituted of kaolinite, muscovite mica and quartz, which are basic constitution elements to formularisations of ceramics masses to the production of covering of stoneware tiles type. This happens because the methodology applied to the improvement process is still very rudimentary, what causes a very low yield, only ¼ from all the material volume that enters the improvement process, in the end, is marketable. The disposal of this residue, in a general way, causes a very big negative environmental impact, what has justified the researches efforts aiming to find a rational solution to this problem. In this way, the intention of this present work is the utilization of this residue in the manufacture of products to high quality ceramics covering, stoneware tiles in an industrial scale. For this purpose, the influence of the addition of the residue to a standard ceramics mass used by a ceramics sector company, already established in the market, with the intention of verifying the possibility of use of this residue as the mass complementary raw material and even the possible partial or total substitution of one of the components of the mass for the raw material in evidence will be studied. To the accomplishment of this work, the kaolin improvement residue generated by an industry of exploitation and improvement of kaolin, located in the region of Equador-RN, in the levels 1,2,4,8, 16 and 32% will be added to the standard mass already used for the production of stoneware tiles. The raw materials used, kaolin residue and the standard mass, were characterized through DRX, FRX, DTA, TGA and dilatometry. After the sintering of the bodies of test, tests of water absorption, apparent porosity, post burning linear retraction, apparent specific mass and flexural strength (3 point bending) were realized to determinate the technological properties of these materials. The results show the studied residue can be considered raw material of great potential to the industry of floor and ceramics covering of the stoneware tiles type

Moscas-das-frutas na fruticultura de clima temperado: situação atual e perspectivas de controle através do emprego de novas formulações de iscas tóxicas e da captura massal.

2016

Potencial de acúmulo de massa e nutrientes e estádio mais adequado de manejo do sorgo-forrageiro em sistemas de transição agroecológica.

2014

Estudo da formulação de pré-misturas secas para a cimentação de poços em terra

An economical solution for cementing oil wells is the use of pre-prepared dry mixtures containing cement and additives. The mixtures may be formulated, prepared and transported to the well where is added water to be pumped.Using this method, becomes dispensable to prepare the cement mixes containing additives in the cementing operation, reducing the possibility of error. In this way, the aim of this work is to study formulations of cement slurries containing solid additives for primary cementing of oil wells onshore for typical depths of 400, 800 and 1,200 meters. The formulations are comprised of Special Class Portland cement, mineral additions and solids chemical additives.The formulated mixtures have density of 1.67 g / cm ³ (14.0 lb / gal). Their optimization were made through the analysis of the rheological parameters, fluid loss results, free water, thickening time, stability test and mechanical properties.The results showed that mixtures are in conformity the specifications for cementing oil wells onshore studied depths

Uso de espectrometria de massa por ionização e dessorção a laser assistida por matriz : tempo de voo (MALDI-TOF MS) para formação de bibliotecas e caracterização da ocupação nodular em soja por estirpes de Bradyrhizobium

Dissertação (mestrado)—Universidade de Brasília, Instituto de Ciências Biológicas, Programa de Pós-Graduação em Biologia Microbiana, 2016.

Organizações de Massa do PAICV/PAIGC na Primeira República 1975-1990

O presente trabalho académico “As Organizações de Massa do PAIGC/ PAICV na Primeira República, de 1975 a 1990”, insere-se no âmbito do curso de Licenciatura em Ciência Política e Relações Internacionais, pela Universidade do Mindelo, e pretende analisar o papel das organizações de massa, no desenvolvimento do País, durante a Primeira República. O trabalho incide, portanto, na investigação dessas organizações, como surgiram no contexto cabo-verdiano, a contribuição que deram para a organização da sociedade civil e no despertar da consciência cívica da população, e ainda, da relação existente entre elas e o Partido PAIGC (Partido Africano Independente da Guiné-Bissau e Cabo Verde) / PAICV (Partido Africano Independente de Cabo Verde), numa primeira fase. Para depois analisar o impacto do processo democrático do País nas mesmas, visto que elas surgiram num período de partido único, tendo-se verificado um decréscimo na sua dinâmica, após essa mudança política, em que algumas delas acabaram mesmo por desaparecer. Este trabalho contará com a participação das pessoas que fizeram parte dessas organizações e entidades políticas, que, prontamente, disponibilizaram dados para a sua elaboração.

Contribuição da variedade e da fermentação maloláctica para o perfil em compostos fenólicos de baixa massa molecular de vinhos varietais alentejanos

O presente trabalho teve como objectivo identificar a influência da variedade e o impacto da fermentação maloláctica, no perfil em compostos fenólicos de baixa massa molecular de vinhos varietais do Alentejo. Para o efeito, foram doseados alguns compostos fenólicos (aldeído protocatéquico e ácidos gálico, protocatéquico, caftárico, vanílico, fertárico, siringico, cafeíco, p-coumárico, ferúlico e coutárico) em 81 vinhos varietais produzidos na Adega Experimental da Universidade de Évora, 48 da casta Trincadeira, e os restantes das castas Aragonez, Cabernet Sauvignon, Alfrocheiro, Castelão e Touriga Nacional. A análise dos dados obtidos, através do método da partição de variância, permitiu identificar a variedade como a variável que mais influência teve no perfil em compostos fenólicos de baixa massa molecular dos vinhos varietais

Processos de recrutamento, seleção e admissão, em massa, de trabalhadores agrícolas numa média empresa

O presente relatório surge do seguimento do estágio curricular em contexto do trabalho final do Mestrado em Gestão – Recursos Humanos, realizado no período de seis meses na organização Vale da Rosa, especificamente no departamento de Recursos Humanos. Este trabalho tem como principal objetivo identificar e descrever pormenorizadamente todo o procedimento efetuado, em contexto profissional, os processos de recrutamento, seleção e admissão de trabalhadores agrícolas. Esta experiência serviu para o desenvolvimento e aquisição de novas competências, onde a mestranda conjugou a base teórica com a prática. As atividades desenvolvidas durante o estágio curricular, como foi referido anteriormente, foram o recrutamento, a seleção e a admissão de trabalhadores agrícolas na entidade acolhedora. Estes processos foram feitos em grande escala devido ao número de indivíduos que são colocados durante o período da colheita, que é aproximadamente cinco meses, para abranger os 250 hectares de vinha. São processamentos adaptados para a área em questão, área de viticultura, o que implica serem utilizados métodos pouco idênticos aos que são referidos pelos diferentes autores; ABSTRACT: Recruitment Processes, Selection and Admission, Mass, Farm Workers in Medium Enterprises This report arises from the follow-up of the curricular internship in the context of the final work of the Masters in Management - Human Resources, carried out during the six-month period in the Vale da Rosa organization, specifically in the Human Resources department. The main objective of this work is to identify and describe in detail the entire procedure carried out, in a professional context, the recruitment, selection and admission processes of agricultural workers. This experience served to develop and acquire new skills, where the master student combined the theoretical base with the practice. The activities developed during the curricular internship, as mentioned previously, were the recruitment, selection and admission of agricultural workers to the welcoming entity. These processes were carried out on a large scale due to the number of individuals being placed during the harvest period, which is approximately five months, to cover the 250 hectares of vineyard. They are adapted processes for the area in question, area of viticulture, which implies using methods not very similar to those that are mentioned by different authors.

Efeito de formulações de iscas tóxicas sobre Anastrepha fraterculus e Ceratitis capitata (Diptera: Tephritidae).

2016

Suco de maçã: elaboração de formulações.

cadeia produtiva de maçã no Brasil está estruturada apenas para comercialização ?in natura?. Visando aproveitar/valorizar os frutos considerados impróprios ao consumo ?in natura?, objetivou-se desenvolver formulações de sucos de maçã com e sem a adição individual de amora, framboesa e morango.

Avaliação do gene psec de Corynebacterium pseudotuberculosis como candidato a duas formulações vacinais contra linfadenite caseosa

2015

Formulações dietéticas para cordeiros Morada Nova e Santa Inês em confinamento, usando o NRC (2007): pesos e rendimentos de cortes comerciais.

Os pesos e rendimentos de cortes comerciais de ovinos podem ser influenciados pela dieta, especialmente se levarmos em conta os grupos genéticos envolvidos, com diferentes graus de maturidade e, ainda, condições de restrição nutricional em períodos críticos de escassez de alimentos. Com o presente trabalho objetivou-se determinar os pesos e rendimentos de cortes comerciais de cordeiros Morada Nova e Santa Inês alimentados com dietas formuladas conforme o NRC de 2007 para maturidade tardia e precoce sem restrição de nutrientes.