制冷混合工质与替代问题

混合工质是开扩替代工质的一种途径，本文列举各种混合工质的特性，分析讨论。并对混合工质的选用问题作有关论述。

电化学C-V法研究磁性GaMnSb/GaSb单晶的载流子浓度纵向分布

采用电化学C-V方法和Tiron电解液研究了GaMnSb/GaSb单晶载流子浓度的纵向分布，所得结果与Hall测量结果和X射线衍射分析结果一致。研究结果表明GaMnSb单晶中的Mn原子替代了GaSb中部分Ga原子的位置，并在GaSb中形成了浅受主能级。

Microphotoluminescence investigation of InAs quantum dot active region in 1.3 mu m vertical cavity surface emitting laser structure

Microphotoluminescence (mu-PL) investigation has been performed at room temperature on InAs quantum dot (QD) vertical cavity surface emitting laser (VCSEL) structure in order to characterize the QD epitaxial structure which was designed for 1.3 mu m wave band emission. Actual and precise QD emission spectra including distinct ground state (GS) and excited state (ES) transition peaks are obtained by an edge-excitation and edge-emission (EEEE) mu-PL configuration. Conventional photoluminescence methods for QD-VCSELs structure analysis are compared and discussed, which indicate the EEEE mu-PL is a useful tool to determine the optical features of the QD active region in an as-grown VCSEL structure. Some experimental results have been compared with simulation results obtained with the aid of the plane-wave admittance method. After adjustment of epitaxial growth according to EEEE mu-PL measurement results, QD-VCSEL structure wafer with QD GS transition wavelength of 1300 nm and lasing wavelength of 1301 nm was obtained.

啤酒酿造中污染细菌的研究（二）──污染细菌的数量变化规律与快速检测方法

啤酒酿造中污染细菌的研究（二）──污染细菌的数量变化规律与快速检测方法吴文芳，吕安国，曾青，李波（中国科学院沈阳应用生态所）刘钧信，张庆春，蒋志云（铁岭市清河啤酒厂）啤酒酿造过程中污染细菌的类群组成及数量常随着不同的季节、不同的发酵工段与发酵阶段而有...

黄土丘陵区农业可持续发展的科学途径

依据黄土丘陵区生态-经济系统演变过程中的正反两方面事例,分析了制约该区农业、经济可持续发展的主要限制因素,探讨了改善该区生态环境、实现农业持续发展的科学途径。并以此认为,退耕还林还草恢复林草植被,是实行农耕制度革命的重要举措,应该与产业结构调整密切结合,实现生态经济可持续发展。

Enhancement of atmospheric pressure chemical ionization for the determination of free and glycine-conjugated bile acids in human serum

A highly sensitive and accurate method based on the precolumn derivatization of bile acids (BA) with a high ionization efficiency labeling reagent 1,2-benzo-3,4-dihydrocarbazole-9-ethyl-benzenesulfonate (BDEBS) coupled with LC/MS has been developed. After derivatization, BA molecules introduced a weak basic nitrogen atom into the molecular core structure that was readily ionized in commonly used acidic HPLC mobile phases. Derivatives were sufficiently stable to be efficiently analyzed by atmospheric pressure chemical ionization (APCI)-MS/MS in positive-ion mode. The MS/MS spectra of BA derivatives showed an intense protonated molecular ion at m/z [M + H](+). The collision-induced dissociation of the molecular ion produced fragment ions at [MH - H2O](+), [MH - 2H(2)O](+), [MH - 3H(2)O](+). The characteristic fragment ions were at m/z 320.8, 262.8, and 243.7 corresponding to a cleavage of N - CO, O - CO, and C - OCC, respectively, and bonds of derivatized molecules. The selected reaction monitoring, based on the m/z [M + H]+ -> [MH - H2O](+), [MH - H2O](+), [MH - 2H(2)O](+), [MH-3H(2)O](+), 320.8, 262.8, and 243.7 transitions, was highly specific for the BA derivatives. The LODs for APCI in a positive-ion mode, at an S/N of 5, were 44.36-153.6 fmol. The validation results showed high accuracy in the range of 93-107% and the mean interday precision for all standards was < 15% at broad linear dynamic ranges (0.0244-25nmol/mL). Good linear responses were observed with coefficients of > 0.9935 in APCI/MS detection. Therefore, the facile BDEBS derivatization coupled with mass spectrometric analysis allowed the development of a highly sensitive and specific method for the quantitation of trace levels of the free and glycine-conjugated BA from human serum samples.

工业控制设备前端信息集成管理的研究与实现

本文讨论了在连续过程生产中ＣＩＭＳ的应用之一，工业控制设备前端信息集成管理的基本思想，提出了统一格式的操作平台为目的设备前端服务器的框架结构，并在此基础上设计和实现了一个应用于八·五攻关项目应用工厂的设备前端服务器（ＭａｃｈｉｎｅＦｒｏｎｔＥｎｄＳｅｒｖｅｒ简称ＭＦＥ），阐述了该系统的基本结构及开发策略。