GFAAS Determination of Zinc in Fish Feed and Feces Using Slurry Sampling

This paper presents a simple, fast, and sensitive method to determine zinc in samples of feces and fish feed by electrothermal atomic absorption spectrometry through the direct introduction of slurries of the samples into the spectrometer's graphite tube. The procedure is based on the injection of 10 mu L of an acidified aqueous solution containing 0.50% w/v of feces or feed and 0.50% v/v HNO(3) into graphite tube. The limits of detection and quantification calculated for 20 readings of the blank of the standard slurries (0.50% w/v of feces or feed devoid of zinc) were 0.04 and 0.13 mu g L(-1) for the standard feces slurries and 0.05 and 0.17 mu g L(-1) for the standard feed slurries. The proposed method was applied in studies of digestibility of zinc in different fish feeds, and their results proved compatible with that obtained from samples mineralized by acid digestion using microwave oven.

Analysis of Ant Communities Comparing Two Methods for Sampling Ants in an Urban Park in the City of São Paulo, Brazil

This study aimed to analyze the species composition and functional groups of the ant community and to assess the efficiency of two sampling methods, pitfall and leaf litter sampling, in an urban park. A total of 1,401 ants were collected, which belonged to six subfamilies and 36 species. The predominant species was Wasmannia auropunctata (present in 45.36% of the samples), while the functional group of opportunistic ants were the most frequent (present in 83.75% of the samples) and abundant (95.29% of the total collected specimens) functional group. The Jaccard Similarity Index showed a low similarity between the two sampling methods, as the difference of the number of individuals for each species between these two methods was not significant in only one case (Linepithema sp. 1, p = 0.4561). The fungus-growing and cryptic ants were more collected in leaflitter samples (p<0.0001; p = 0.0348 respectively). Although there was no significant difference (p = 0.6397) between the two sampling methods for the total individuals of opportunistic ants, more species of this group were collected in pitfall traps. This difference was not significant because of the high presence of W. auropunctata, an opportunistic ant, in samples of leaf litter. Due to the predominance of tramp ants in the studied area, this article illustrates the importance of green urban areas in ant control strategies, since these sites could be used as a source of new colonization for these ants. Furthermore, the combination of the two sampling methods seems to be complementary for obtaining a more complete picture of the ant community.

Occurrence and behavior of butyltins in intertidal and shallow subtidal surface sediments of an estuarine beach under different sampling conditions

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Real orthogonal polynomials in frequency analysis

We study the use of para-orthogonal polynomials in solving the frequency analysis problem. Through a transformation of Delsarte and Genin, we present an approach for the frequency analysis by using the zeros and Christoffel numbers of polynomials orthogonal on the real line. This leads to a simple and fast algorithm for the estimation of frequencies. We also provide a new method, faster than the Levinson algorithm, for the determination of the reflection coefficients of the corresponding real Szego polynomials from the given moments.

Connection coefficients and zeros of orthogonal polynomials

We discuss an old theorem of Obrechkoff and some of its applications. Some curious historical facts around this theorem are presented. We make an attempt to look at some known results on connection coefficients, zeros and Wronskians of orthogonal polynomials from the perspective of Obrechkoff's theorem. Necessary conditions for the positivity of the connection coefficients of two families of orthogonal polynomials are provided. Inequalities between the kth zero of an orthogonal polynomial p(n)(x) and the largest (smallest) zero of another orthogonal polynomial q(n)(x) are given in terms of the signs of the connection coefficients of the families {p(n)(x)} and {q(n)(x)}, An inequality between the largest zeros of the Jacobi polynomials P-n((a,b)) (x) and P-n((alpha,beta)) (x) is also established. (C) 2001 Elsevier B.V. B.V. All rights reserved.

Inequalities for zeros of associated polynomials and derivatives of orthogonal polynomials

It is well known and easy to see that the zeros of both the associated polynomial and the derivative of an orthogonal polynomial p(n)(x) interlace with the zeros of p(n)(x) itself. The natural question of how these zeros interlace is under discussion. We give a sufficient condition for the mutual location of kth, 1 less than or equal to k less than or equal to n - 1, zeros of the associated polynomial and the derivative of an orthogonal polynomial in terms of inequalities for the corresponding Cotes numbers. Applications to the zeros of the associated polynomials and the derivatives of the classical orthogonal polynomials are provided. Various inequalities for zeros of higher order associated polynomials and higher order derivatives of orthogonal polynomials are proved. The results involve both classical and discrete orthogonal polynomials, where, in the discrete case, the differential operator is substituted by the difference operator. (C) 2001 IMACS. Published by Elsevier B.V. B.V. All rights reserved.

Monotonicity of zeros of Laguerre-Sobolev-type orthogonal polynomials

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Monotonicity of zeros of Jacobi-Sobolev type orthogonal polynomials

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Sharp bounds for the extreme zeros of classical orthogonal polynomials

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

L-orthogonal polynomials associated with related measures

A positive measure psi defined on [a, b] such that its moments mu(n) = integral(b)(a)t(n) d psi(t) exist for n = 0, +/-1, +/-2. can be called a strong positive measure on [a, b] When 0 <= a < b <= infinity the sequence of polynomials {Q(n)} defined by integral(b)(a) t(-n+s) Q(n)(t) d psi(t) = 0, s = 0, ., n - 1, exist and they are referred here as L-orthogonal polynomials We look at the connection between two sequences of L-orthogonal polynomials {Q(n)((1))} and {Q(n)((0))} associated with two closely related strong positive measures and th defined on [a, b]. To be precise, the measures are related to each other by (t - kappa) d psi(1)(t) = gamma d psi(0)(t). where (t - kappa)/gamma is positive when t is an element of (n, 6). As applications of our study. numerical generation of new L-orthogonal polynomials and monotonicity properties of the zeros of a certain class of L-orthogonal polynomials are looked at. (C) 2010 IMACS Published by Elsevier B V All rights reserved

Convolutions and zeros of orthogonal polynomials

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Asymptotics for Gegenbauer-Sobolev orthogonal polynomials associated with non-coherent pairs of measures

Inner products of the type < f, g >(S) = < f, g >psi(0) + < f', g'>psi(1), where one of the measures psi(0) or psi(1) is the measure associated with the Gegenbauer polynomials, are usually referred to as Gegenbauer-Sobolev inner products. This paper deals with some asymptotic relations for the orthogonal polynomials with respect to a class of Gegenbauer-Sobolev inner products. The inner products are such that the associated pairs of symmetric measures (psi(0), psi(1)) are not within the concept of symmetrically coherent pairs of measures.

Zeros of Gegenbauer-Sobolev Orthogonal Polynomials: Beyond Coherent Pairs

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

BASIC HYPERGEOMETRIC FUNCTIONS and ORTHOGONAL LAURENT POLYNOMIALS

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)