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Esta dissertação diz respeito à manufactura por adição, onde são avaliadas as capacidades para diferentes condições de funcionamento de uma impressora 3D por fusão de filamento, de modo a poder quantificar as respectivas vantagens em comparação com outras opções actualmente disponíveis no mercado. Num contexto de inovação tecnológica, este trabalho tem em vista a validação e a possível aplicação deste tipo de equipamentos de fabrico no mercado empresarial e industrial. Realizaram-se ensaios de fabrico que permitem identificar diferentes áreas de aplicação através das características de funcionamento, como o tempo de fabrico, a precisão dimensional, a variação mínima da precisão e a rugosidade de superfícies verticais e horizontais. O equipamento utilizado foi uma impressora Leapfrog Creatr14. Nesta avaliação caracterizaram-se os três tipos de qualidade de impressão disponíveis (baixa, média e alta). Cada componente foi concebido para analisar um único aspecto da qualidade de impressão, mantendo todos os outros constantes. O conhecimento assim adquirido poderá servir como possível base de comparação dos equipamentos de fabrico por fusão de filamento, dado que é uma tecnologia em crescimento e em desenvolvimento constante.

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Contient : Justification par Jean Petit de l'assassinat du duc d'Orléans par le duc de Bourgogne, en 1407. Incomplet du commencement. (Cf. Chronique de Monstrelet, t. I, p. 179-242) ; Réponse à la susdite justification de Jean Petit

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In Charon or the Inspectors we find the ferryman of the underworld on earth, talking to the god Hermes about wealth, happiness, and the vain human striving for material goods. The piece has been considered to be an example of Menippean satire inside the corpus of Lucian"s works. Homeric poetry is always in the background. Lucian uses Homeric verses, or rather, verses structured in the Homeric manner, to formulate his critical view of the mortal world; in addition, he puts these verses into the mouth of a character who must temporarily give up his job as a ferryman in order to practise the art of rhapsody. This paper analyses a textual problem: the two variants in Cont. 7 referring to Homer in the manuscript tradition. In a context in which Lucian wants to make fun not just of foolish humans but also of the Greek poet par excellence, the reading of the ueteres seems more appropriate because it illustrates better Lucian"s parodic intention in recalling Homer and in trying to adapt form and content to the Greek tradition.

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The interface and software for synchronous control of an autosampler and an electrothermal tungsten coil atomizer in atomic absorption spectrophotometry were developed. The control of the power supply, the trigger of the Read function of the spectrophotometer and the automatic operation of the autosampler was performed by software written in "TurboBasic". The system was evaluated by comparison of the repeatability of peak-height absorbances obtained in the atomization of lead by consecutive 10-µl injections of solutions (prepared in 0.2% v/v HNO3) using autosampler and manual sample introduction, and also by long term operation.

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A tungsten coil atomizer was used to investigate the effect of heating programs with constant or variable drying temperatures on the atomization of Al, Cd, Cr and Pb. The variation of the surface temperature in the tungsten coil furnace can occur during each heating step due to the design of the power supply, that may apply constant voltages during a programmed time. For volatile elements (Cd), losses in sensitivity were observed when the program with a variable temperature was used. On the other hand, these effects are negligible for less volatile elements (Al and Cr) and any tested program, in different acidic media, could be used without appreciable changes in sensitivities. The results allow the establishment of proper heating programs for elements with different thermochemical behavior in the tungsten coil atomizer.

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In this review it is presented some aspects of electrothermal atomic absorption spectrometry with tungsten coil (ETAW-AAS) since its beginning until the present days as well as the perspectives for this technique. Some aspects concerning its development and theoretical concepts are discussed. The analytical figures of merit such as limit of detection (LD), characteristic mass (m0), relative standard deviation (RSD), accuracy and precision are evaluated, compared and discussed considering published works. It is also evaluated its advantages, applications, limitations and instrumental development. The use of diode laser as radiation source and its perspectives to ETAW are also discussed.

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It is here discussed the development of a low cost analytical instrument with capacity for metals determination using atomic emission measurements in an electrothermal atomization system with a tungsten coil atomizer. The main goal was to show a new frontier for using this atomizer and to demonstrate that the simple instrumental arrangement here proposed has potential for portability and for solving analytical tasks related to metals determination. Atomic emission of calcium was selected for the adjustment of instrumental parameters and to evaluate the main characteristics of the lab-built instrument. Cobalt was determined in medicines and one alloy to demonstrate its feasibility.

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El nacimiento de la Universitat Oberta de Catalu??a aporta al Sistema educativo actual una forma diferente de entender tanto el proceso de ense??anza-aprendizaje universitarios, como una nueva manera de entender la misma universidad. La Universitat Oberta de Catalu??a es un campus virtual, un campus al que se puede acceder en cualquier momento y desde cualquier lugar. Un campus siempre abierto, que ha de posibilitar una nueva manera de moverse y de estudiar en la universidad.

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Simulación de una entrevista a la televisión. Se exponen las opiniones que ésta respecto a su uso en el seno de las familias: consumo televisivo desmesurado, violencia, manipulación televisiva, influencia de la televisión en las relaciones familiares.

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Resumen basado en el de la publicaci??n

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Incluye Bibliografía