993 resultados para demerit point loss


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A simple cloud point extraction procedure is presented for the preconcentration of copper in various samples. After complexation by 4-hydroxy-2-mercapto-6-propylpyrimidine (PTU), copper ions are quantitatively extracted into the phase rich in Triton X-114 after centrifugation. Methanol acidified with 0.5 mol L-1 HNO3 was added to the surfactant-rich phase prior to its analysis by flame atomic absorption spectrometry (FAAS). Analytical parameters including concentrations for PTU, Triton X-114 and HNO3, bath temperature, centrifugation rate and time were optimized. The influences of the matrix ions on the recoveries of copper ions were investigated. The detection limits (3SDb/m, n=4) of 1.6 ng mL-1 along with enrichment factors of 30 for Cu were achieved. The proposed procedure was applied to the analysis of environmental samples.

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Työssä tutkitaan kaupallisten lyhyen kantaman radiotekniikoiden ominaisuuksia sekä soveltuvuutta metallisorvin langattomaan ohjaukseen. Ominaisuuksien perusteella valitaan parhaiten sovellukseen käyvä radiotekniikka.

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Työssä vertaillaan kaupallisia lyhyen kantaman radiotekniikoita. Vertailujen pohjalta valitaan parhaiten sovelluskohteeseen soveltuva radiotekniikka.