Magnetic Purification of Curcumin from Curcuma longa Rhizome by Novel Naked Maghemite Nanoparticles

Naked maghemite nanoparticles, namely, surface active maghemite nanoparticles (SAMNs), characterized by a diameter of about 10 nm, possessing peculiar colloidal stability, surface chemistry, and superparamagnetism, present fundamental requisites for the development of effective magnetic purification processes for biomolecules in complex matrices. Polyphenolic molecules presenting functionalities with different proclivities toward iron chelation were studied as probes for testing SAMN suitability for magnetic purification. Thus, the binding efficiency and reversibility on SAMNs of phenolic compounds of interest in the pharmaceutical and food industries, namely, catechin, tyrosine, hydroxytyrosine, ferulic acid, coumaric acid, rosmarinic acid, naringenin, curcumin, and cyanidin-3-glucoside, were evaluated. Curcumin emerged as an elective compound, suitable for magnetic purification by SAMNs from complex matrices. A combination of curcumin, demethoxycurcumin, and bis-demethoxycurcumin was recovered by a single magnetic purification step from extracts of Curcuma longa rhizomes, with a purity >98% and a purification yield of 45%, curcumin being >80% of the total purified curcuminoids.

Biologia comparada de populações da lagarta–do–cartucho em folhas de milho e mandioca

The fall armyworm is a pest that feeds on various botanies species. The objective of this experiment was to study the biology of this pest in corn and cassava leaves. Caterpillars were collected in area under cultivation with cassava and maintained on artificial diet for two generations. Under controlled conditions in a climatic chamber (B.O.D) in the laboratory (25 degrees, 60 +/- 10% RH and photophase 14 hours) were evaluated daily 50 caterpillars in corn treatments and 50 in cassava, where duration and viability of the larval phase and pupal, weight of pupas were observed after 24 hours, deformation percentage of pupas and adults, longevity, fecundity and total life cycle. The viability of larvae fed on leaves of maize and cassava was 74% and 60%, respectively. The larval period of the insects was shorter in maize 16.89 days (seven instars) and cassava 20.08 days (six instars). The pupal phase lasted 11.42 days in cassava treatment and 10.87 in the maize. The pupal weight of females and males was higher in corn 204.91 mg and 198.97 mg, respectively. The biological cycle varied depending on the ingested food. Adult longevity lasted 9.88 days for insects fed on cassava leaves. Therefore, cassava affected the development of S. frugiperda.

Aspectos biológicos e tabela de vida de fertilidade de Aphis gossypii Glover (Hemiptera: Aphididae) em cultivares de algodoeiro DeltaOPAL e NuOPAL

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Effect of beta 1,3 glucan in stress responses of the pencilfish (Nannostomus trifasciatus) during transport within the rio Negro basin

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Administração de maltodextrina em cavalos submetidos a teste de exercício progressivo e a exercícios sequenciais de alta intensidade e curta duração em esteira

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Estudo comparativo entre traçados cefalométricos predictivo e pós operatório imediato de pacientes que foram submetidos à cirurgia ortognática para correção da síndrome da face longa

The aim of this research was to verify the accuracy of the prediction trace. Records in 15 patients admitted for orthognathic surgical treatment were analysed. Predictive and postoperative positíons of maxilla were compared with linear measurements. Statistically significant difference between predicted and postoperative position were demonstrated, but the prediction trace revealed to be very useful to help in decision of direction of movements, easy to do at low cost

Elaboração de um material didático aplicado ao ensino de física para utilização do experimento virtual da dupla fenda

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Automação do fornecimento de ração para organismos aquáticos

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

O efeito da estrutura da matriz na percepção de aves na paisagem

Pós-graduação em Ciências Biológicas (Zoologia) - IBRC

Física Moderna no Ensino Médio: um experimento para abordar o efeito fotoelétrico

Considering the importance of the inclusion of Modern and Contemporary Physics in the curriculum of Physics in High School, it is proposed in this work an experimental activity, made with low- cost materials, which presents the photoelectric effect. This activity can be used articulating this phenomenon with some technological applications experienced by the students in their daily lives. When working the experiment, the teacher can encourage students to investigate what happens during its execution and, through questions, get them to express their ideas in the previous attempt to explain its operation. This articulation linked to social interaction in the classroom can arouse the students’curiosity and motivation of students to learn the subject taught in classroom.

Variáveis determinantes do desempenho em provas de curta duração em nadadores masters

Twenty-four masters swimmers participated in the study (42.0 ± 7.4 years, 1.74 ± 0.09 m, 74.8 ± 14.1 kg). Countermovement jump (CMJ) and 3 kg medicinal ball throwing (BM) were performed. At a 25 m swimming pool, each subject completed a maximal 50 m front crawl swim with in water start, 25 and 50 m performances (T25, T50) were recorded. Anaerobic critical velocity (AnCV) was determined by the slope of the distance-time relationship (Dd-t) in the two swimming distances. T25 and T50 (respectively 19.0 ± 2.7-sec and 38.8 ± 6.4-sec) were correlated with CMJ (27.2 ± 5.0 m) (respectively, r = -0.78 and -0.73, p < 0.01), and BM (4.3 ± 1.0 m) (r = -0.68 and - 0.58, p < 0.01). AnCV25,50 (1.31 ± 0.23 m.s-1 ) was correlated with T25 (r = -0.92, p < 0.01 ) and T50 (r = -0.98, p < 0.01). The strength parameters turn out to be important in aquatic performance in masters swimmers and AnCV may be relevant in the training of masters swimmers.

Interferência das plantas daninhas na produtividade e na qualidade tecnológica da cana-de-açúcar no manejo cana-crua e queimada

Pós-graduação em Agronomia (Produção Vegetal) - FCAV

Protocolos para o uso combinado de monensina sódica e virginiamicina em dietas de bovinos Nelore confinados

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)