31 resultados para DCCC
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Mode of access: Internet.
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Mode of access: Internet.
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Mode of access: Internet.
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Droplet counter-current chromatography, rotation locular counter-current chromatography and high-speed counter-current chromatography were applied to the preparative separation of the alkaloid ricinine from the dichloromethane extracts of Ricinus communis leaves. The solvent system used was composed of dichloromethane-methanol-water (93:35:72 v/v/v) and all techniques led to the isolation of large amounts of the alkaloid. The best result was obtained through HSCCC, since the ricinine yield was respectively 50% and 30% higher than when using RLCCC or DCCC.
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Whenever P is a topological property, we say that a topological space is star P if whenever U is an open cover of X, there is a subspace A subset of X with property P such that X = St(A, U). We study the relationships of star P properties for P is an element of {Lindelof, sigma-compact, countable} with other Lindelof type properties. (C) 2010 Elsevier B.V. All rights reserved.
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A general procedure was developed for the simultaneous separation of flavonoids and naphthopyrones from the polar extracts of the capitula from Brazilian everlasting plants is described. The ethanolic extracts of several species from the Paepalanthus genus (Eriocaulaceae) were fractionated by droplet countercurrent chromatography followed by column chromatography on pvp and sephadex LH-20. The isolated compounds were identified by spectrometric analysis and comparison with literature data. This approach led to the isolation of 9-O-β-D-glucopyranosylpaepalantine (1), 9-O-β-D-glucopyranosyl (1→6)allopyranosylpaepalantine (2), along with the flavonoids 6-methoxykaempferol (3), 3-O-β-D-glucopyranosyl-6-methoxykaempferol (4), patuletin (5), 3-Oβ-D-rutinosylpatuletin (6), 7-O-β-D-glucopyranosylquercetagetin (7), 5,7,4'-trihydroxy-6,3'-dimethoxyflavone (8) and 5,7,4'-trihydroxy-6,3'-dimethoxyflavonol (9).
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Appendix, p. [281]-359, contains a list of Union prisoners in Southern prison camps.
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Title vignette.
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Verso of t.p., p. [1]-[2], [6] and [30]-[32] are blank.
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Vol. 9, "Supplementum," incorporating the supplement issued with v. 1, contains: I. Litteras A et B, ab anno M.DCCC.XLIX. ad annum M.DCCC.LXXII. II. Addenda et corrigenda.
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The "elenco" (list of subscribers) in vol. 11 is transcribed in full by Bertelli & Innocenti; see also their remarks on p. cxliv-cxlv.
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Buff printed paper cover has title: "Mr. Sullivan's discourse, delivered at Plymouth."
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Mode of access: Internet.
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Mode of access: Internet.