Microstructural Characterization of Ti-6Al-7Nb Alloy After Severe Plastic Deformation

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Comportamento plástico do aço inoxidável austenítico em baixa temperatura

Ensaios de tração uniaxiais foram empregados para deformar aços inoxidáveis austeníticos do tipo 304, em diferentes temperaturas abaixo da ambiente (de 77 K a 300 K). A relação entre a estabilidade da austenita e o encruamento, em função da temperatura de teste, é discutida quanto à transformação martensítica induzida por deformação e ao deslizamento de discordâncias na austenita. em curvas tensão-deformação que assumem a equação de Ludwik sigma = sigmao + képsilonn, na qual sigma é a tensão verdadeira e e a elongação plástica verdadeira, um modo conveniente para analisar o encruamento é por meio do diagrama log dsigma / dépsilon versus log épsilon. O aspecto significativo é a variação da taxa de encruamento dsigma / dépsilon com a elongação plástica verdadeira nas diferentes temperaturas. As mudanças no comportamento do encruamento motivando até três estágios de deformação são associadas a diferentes processos microestruturais. A transformação martensítica pode ser considerada como um processo de deformação que compete com o processo usual de deslizamento. A investigação desses estágios, na região plástica, produz uma referência qualitativa de como diferentes fatores, tais como o grau de deformação, temperatura e composição química da austenita, afetam a transformação austenita-martensita.

Orientation dependence of stored energy of cold work in semi-processed electrical steels after temper rolling

Microhardness measurements were carried out in a low carbon lamination steel after 6% of temper rolling, in order to evaluate local variations of work hardening as a function of crystallographic orientation. EBSD (electron back scattered diffraction) was used to determine grain orientations with respect to individual rolling planes and rolling directions. Hardness was shown to increase with the local Taylor factor. TEM observations and a well-known dislocation hardening model were used to confirm the equivalence between hardness values and the stored energy of cold work. A definite correlation between stored energy and Taylor factors could therefore be established, being more consistent than previous data reported in the literature. The improvement was thought to be related to the rather small plastic deformation, during which Taylor factors could be considered to remain constant. (c) 2006 Elsevier B.V. All rights reserved.

Microstructural Evolution of Ti-6Al-7Nb Alloy During High Pressure Torsion

Ti-6Al-7Nb alloys are being evaluated for biomedical applications, in substitution of the more conventional Ti-6Al-7V. Both types of alloys present a microstructure containing the alpha and the beta phases, which result in good compromise for mechanical applications. In the present work Ti-6Al-7Nb alloys were processed by High Pressure Torsion (HPT), varying the number of revolutions and thus the total imposed strain. X-Ray Diffraction (XRD) results revealed the formation of different crystallographic textures in samples subjected to HPT. Microhardness distribution, across the diameters of the disks, is rather homogeneous for all samples, with higher values for those subjected to 03 and 05 turns. Transmission electron microscopy (TEM) micrographs have showed that an ultra-fine grained microstructure was obtained in all the samples.

Evaluation of immediate bone-cell viability and of drill wear after implant osteotomies: Immunohistochemistry and scanning electron microscopy analysis

Purpose: This study sought to evaluate the effect of repeated implant drilling on the immediate bone-cell viability, and to evaluate drill wear by scanning electron microscopy.Materials and Methods: The tibiae of 10 rabbits were used, divided into 5 groups (G): G1 corresponded to new drills, and G2, G3, G4, and G5 corresponded to drills used 10, 20, 30, and 40 times, respectively. The animals received 10 sequential osteotomies in each tibia. The animals were euthanized immediately after the osteotomies by perfusion with 4% formaldehyde. Samples then underwent immunohistochemistry processing for ordinal qualitative analysis of osteoprotegerin (OPG), the RANK ligant (RANKL; a tumor-related necrosis factor receptor family), and osteocalcin protein immunolabels, as detected by the immunoperoxidase method and revealed with 3,3-diaminobenzidine. Drill wear and plastic deformation were analyzed by scanning electron microscopy (SEM).Results: The proteins were expressed in osteocytes of the superior bone cortical during the 40 drillings. However, in G4 and G5, a discrete increase in the expression of RANKL was observed, when compared with OPG; this increase was statistically significant in G5 (P = .016). The SEM analysis revealed major plastic deformation and drill wear in G4 and G5.Conclusion: Based on the present methodology, it may be concluded that cell viability is preserved if a less traumatic surgical protocol is used. However, the repeated use of drills alters the protein balance as of the thirtieth perforation. (C) 2008 American Association of Oral and Maxillofacial Surgeons.

Influencia da Carga no Comportamento quanto ao Desgaste de um Aco ABNT-1020 Bifasico Revenido a 450°C

The wear rate of the dual-phase steel ABNT-1020 tempered at 450°C sliding against cemented steel ABNT-1020 in function of load value is investigated in wide load range. The alteration in behavior of this function at intermediate load level, like in the case of low hardness steel sliding against high hardness steel, is observed. The analysis by scanning electronic microscope before and after this alteration showed a change of wear mechanism from plastic displacement to embrittlement.

Avaliação da deformação, perda de massa e rugosidade das fresas, após osteotomia para implantes osseointegrados, com diferentes tipos de metais

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Avaliação de um modelo matemático para a determinação do coeficiente de atrito no processo de conformação por dobramento

Pós-graduação em Engenharia Mecânica - FEG

Estudo do alívio das tensões residuais, em peça estampada, pela técnica de vibrações mecânicas

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

A influência da deformação plástica sobre a estabilidade mecânica da Austenita retida em aços 300M

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Estudo do envelhecimento após deformação em um aço complex phase

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Efeito no processo ECAP (EQUAL CHANNEL ANGULAR) na microestrutura e nas propriedades mecânicas de uma liga comercial de alumínio AA3104

Pós-graduação em Engenharia Mecânica - FEG

Investigação da retração plástica e da fissuração da argamassa do concreto auto-adensável

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Desenvolvimento de um programa paramétrico para simulação do processo de estampagem utilizando elementos finitos

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Avaliação do comportamento reológico na retração plástica e na fissuração de argamassas de concreto auto-adensável

This paper investigated the influence of the amount of superplasticizer and mineral adding - silica fume and basaltic filer - in plastic shrinkage and cracking of self-compacting concrete (SCC) mortars. Initially analysis was performed of the rheological behavior of cement paste and mortars phases of the compositions of SCC. Then the deformations of mortars were measured by the effect of shrinkage and evaluation of cracking. On plastic shrinkage and cracking, the composition with silica fume showed superior results, independent of wind and superplasticizer content, relative to the composition with addition of basalt filler. However, the composition with silica fume showed superior results only in the tests with imposed ventilation at vertical plastic deformation. The rheological behavior affected directly the plastic shrinkage and cracking at early ages, fact confirmed by the analysis of capillary pressures of mortars tested.