511 resultados para Líquida


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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

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Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

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The use of pesticides to manage pest problems in agriculture has become a common practice around the world. Pesticides consist in chemical substances or biological agents that act preventing, destroying, repelling or mitigating the damage caused by pests in agriculture. In order to a successful treatment, the correct dosage of pesticide has to be applied for each kind of culture. In this context, this project aims to quantify the levels of the active ingredients Imidacloprid and Chlorpyrifos present in formulated technical products and compare with the reported in the ir commercial leaflets. The analyzes were performed by Ultra Performance Liquid Chromatography coupled to a photodiode array detector (CLUE-DAD). The identification of Imidacloprid and Chlorpyrifos in the samples was realized by comparison of the time of retention and UV spectre of those substances with the commercials patterns, resulting in a excellent method specificity of the method. In the scope of determination of active ingredients in formulated products, the method developed showed good sensitivity in the applied conditions, with suitables limits of detection (4,2.10-² mg L-¹ for Imidacloprid and 1,1.10-¹ mg L-¹ to Chlorpyrifos) and quantitation (1,4.10-¹ mg L-¹ and Imidacloprid 3,6.10-¹ mg L-¹ to Chlorpyrifos) for the concentrations found in matrices analyzed. Furthermore, good results were obtained to the method accuracy with coeficiente of variance values in the range of 0,6 to 0,7% for repeatability (intra-day) and 0,4 to 0,58% for intermediate precision (inter- day). The accuracy of the method was determined by recovery tests, the values were comprised in the range of 98 102%. According to the recommendations of the Associação Brasileira de Normas Técnicas, these values show good accuracy of the method. The concentrations obtained in the quantification of the active ingredients in formulated products showed values within permited by ABNT, 60.1% (w/v) ± 0.6%...

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The use of medicinal plants is common in many Brazil's ethnic groups, because the diversity of plant species in the country is large. But the utilization of these plants as standardized herbal doesn't occur with de same frequency, due the lack of studies related to these therapies, classified as alternatives. Due to the high cost of some synthetic medicines for the treatment of chronic diseases, phytotherapy is a low-cost alternative and efficient, since the phytomedication has proven scientific studies and its production meets strict criteria for manufacturing and quality control to ensure its safety and efficacy. Among the medicinal species used for the treatment of chronic diseases, such as pain and inflammation, is Eugenia speciosa Cambess, popularly known as the bush laranjinha. Against this context, this paper held preliminary studies and developed the chromatographic profile of the hydroalcoholic extract of the leaves of E. speciosa by High Performance Liquid Chromatography coupled to photodiode array detector (CLAE-DAD). Preliminary qualitative results and the chromatographic profile have identified some metabolites classes present and some constituent as: homogentisic acid, homorientina, isovitexin and quercetrin

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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

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The study evaluated the energy balance of the yellow passion fruit (Passiflora edulis Sims) production system in the region of Marilia-SP. There were analyzed the "inputs" of energy originated from biological, fossil, and industrial sources, and the "output" of energy in the form of fruits produced per unit area, as well as five energy indicators. The phytotechnical indices considered were: planting in February (seedling in tubes), production cycle: 18 months, and yield: 20 t/ha. The input energy totaled 173,707.86 MJ/ha. The most representative items corresponded to industrial indirect energy (38%) and to biological (34%). Chemical fertilizers and pesticides accounted for 65% and 31% of indirect energy industry, respectively. The activity generated 391,800.00 MJ per cycle/ha, and the culture productivity, 0.12 MJ/kg. The efficiency of the culture was 2.26. The net cultural energy totaled 218,092.15 MJ/ha. The energy balance was positive (126,050.23 MJ/ha). Energy efficiency was favorable, with a value of 3.64. The direct power consumption of fossil origin is significant in the system evaluated, but it still allows the production of the yellow passion fruit in an environmentally sustainable way.

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The objective of this study was to dimension the economic risks and returns on adopters of genetically modified (GM) maize in one of the major corn producing regions of São Paulo state. We performed analysis of variation of the quantities and prices of insecticides used, productivity gains, and variation in the price differentials between GM maize and conventional hybrids seeds, according to account to the maize prices oscillation during the period studied. The net benefits methodology was used, in other words, the economic gains minus the costs of GM technology under risk conditions were calculated. The net benefits was calculated as a function of four critical variables: 1) GM maize productivity; 2) costs of pest control; 3) maize price; 4) GM seeds cost. The probability distribution functions of these critical variables were estimated and included in the net benefit equation. Using the Monte Carlo simulation methodology, the following indicator sets were estimated: central tendency measurements, variability in net benefits (total benefits minus total costs), sensitivity analysis of the net benefits in relation to the critical variables, and finally, a map of the risk to GM technology adopters. These indicators allow one to design economic scenarios associated with their probability of occurring. The results showed probability of 85% to positive gains to the farmers who adopted the transgenic maize seed cultivation. The variable with the greatest impact on the farmers' income was the reduction in productivity loss, that means, as higher is the maize productivity, higher will be the net income. The average gain was US$ 137,41 (R$ 2.45/US$)per hectare with the adoption of transgenic maize seed when compared to conventional maize seed.

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This study was conducted at University of Marília, São Paulo State, Brazil, aiming to determine the phase of intake transition between exclusively liquid diet (milk) and diet based on milk, grass and/or ration by lambs by δ13C technique. Six Suffolk crossbreeding lambs were distributed in a totally random design (3x2), with two experimental groups and three replications. At the first one, lambs were penned and sucked milk from dams fed with C4 diet. besides, they had access to C3 ration in creep feeding, since their birth. At the second group, lambs were kept on a paddock with Tifton – 85 grass (C4 photosynthetic way) as well as their dams and had access to C3 ration in creep feeding, since their birth. The C3 ration contained soybean meal, ground oat grains, lucerne hay and also mineral salt. The penned lambs’ ration consumption overcame the milk intake at 30-35 days after birth; however, grazing lambs ingested more milk and pasture than ration until 40 days after birth. The δ 13C technique was considered effective on studies of lambs feeding behavior.

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Ginger is a starchy tubers prized for their chemical components. In the production of any kinds of beverages has been added to the extract of ginger. However, in view of the high starch content, a possibility of further development of the agribusiness sector this would be the hydrolysis tuberous rhizomes disqualified for export in order to obtain hydrolysates that would be used in the preparation of fermented beverages. This work aimed to evaluate the production of sugar from rhizomes of ginger. Two α-amylase enzymes were tested in the stage of liquefaction (Liquozyme Supra (T1) and Termamyl 2X (T2)), as well as the effect of time of action of amyloglucosidase (AMG 300L). The hydrolysates were analyzed in liquid chromatography (HPLC) and was also carried out the mass balance of the processes. The results showed higher hydrolysis of starch in the treatment that used Liquozyme Supra in liquefaction. The action time of 18 hours of AMG 300L hydrolyzate which gave an 98% of its chemical components was glucose.