Desenvolvimento de um secador spray para obtenção de pós finos de precursores de nióbio

This work presents a spray-dryer designed to oxalate-niobate precursors and suitable for the production of Niobium Carbide. The dryer was intended to produce powders of controlled particle size. First, the precursor is dissolved in water to produce a solution of known concentration and then it is atomized on the spray-dryer to produce the powder. This equipment consists of a 304 stainless steel chamber, 0.48 m x 1.9 m (diameter x length), with a conical shape at the lower portion, which is assembled on a vertical platform. The chamber is heated by three 4 kW electrical resistances. In this process, drying air is heated as it flows inside a serpentine surrounding the chamber, in contrary to more traditional processes in which the hot drying air is used to heat the component. The air enters the chamber at the same temperature of the chamber, thus avoiding adherence of particles on the internal surface. The low speed flow is concurrent, directed from the top to the bottom portion of the chamber. Powders are deposited on a 0.4 m diameter tray, which separates the cylindrical portion from the conical portion of the chamber. The humid air is discharged though a plug placed underneath the collecting tray. A factorial experimental planning was prepared to study the influence of five parameters (concentration, input flow, operation temperature, drying air flow and spray air flow) on the characteristics of the powders produced. Particle size distribution and shape were measured by laser granulometry and scanning electronic microscopy. Then, the powders are submitted to reaction in a CH4 / H2 atmosphere to compare the characteristics of spray-dried powders with powders synthetizided by conventional methods

Protótipo de rastreador solar de um eixo baseado em microcontrolador

The increase in the efficiency of photo-voltaic systems has been the object of various studies the past few years. One possible way to increase the power extracted by a photovoltaic panel is the solar tracking, performing its movement in order to follow the sun’s path. One way to activate the tracking system is using an electric induction motor, which should have sufficient torque and low speed, ensuring tracking accuracy. With the use of voltage source inverters and logic devices that generate the appropriate switching is possible to obtain the torque and speed required for the system to operate. This paper proposes the implementation of a angular position sensor and a driver to be applied in solar tracker built at a Power Electronics and Renewable Energies Laboratory, located in UFRN. The speed variation of the motor is performed via a voltage source inverter whose PWM command to actuate their keys will be implemented in an FPGA (Field Programmable Gate Array) device and a TM4C microcontroller. A platform test with an AC induction machine of 1.5 CV was assembled for the comparative testing. The angular position sensor of the panel is implemented in a ATMega328 microcontroller coupled to an accelerometer, commanded by an Arduino prototyping board. The solar position is also calculated by the microcontroller from the geographic coordinates of the site where it was placed, and the local time and date obtained from an RTC (Real-Time Clock) device. A prototype of a solar tracker polar axis moved by a DC motor was assembled to certify the operation of the sensor and to check the tracking efficiency.