Deformation behavior of nanostructured aluminum alloy processed by severe plastic deformation

Microstructure and deformation behavior of the commercial aluminum-based Al7.5%Zn–2.7%Mg–2.3%Cu–0.15%Zr alloy subjected to high pressure torsion (HPT) were studied in the present work. A small grain size less than 100 nm, high level of internal stresses and presence of second phase nanoparticles were revealed by transmission electron microscopy (TEM) and X-ray diffraction (XRD). The nanostructured alloy processed by HPT exhibits tensile strength of 800 MPa and ductility of 20% at optimal temperature-strain rate conditions. Unusual influence of a short pre-annealing on tensile strength and ductility of as-processed alloy is discussed.

An investigation of the native oxide of aluminum alloy 7475-T7651 using XPS, AES, TEM, EELS, GDOES, RBS.

The native oxide on the rolled aerospace aluminum alloy 7475-T7651 was characterized using a variety of different techniques, including X-ray Photoelectron Spectrometry (XPS), Auger Electron Spectrometry (AES), Transmission Electron Microscopy (TEM), Electron Energy Loss Spectrometry (EELS), Glow Discharge Optical Emission Spectrometry (GDOES), and Rutherford Backscattered Spectrometry (RBS). All techniques revealed that the native oxide layer is magnesium-rich and is probably a mixture of magnesium and aluminum–magnesium oxides.1 The oxide layer was found to be of nonuniform thickness due to the rolling process involved during the manufacture of this sheet alloy; this complicates analysis using techniques which have poor spatial resolution. Direct thickness measurement from cross-sectional TEM reveals an oxide thickness which varies between 125 and 500 nm. This large variation in thickness was also evident from GDOES and AES depth profiles as well asthe RBS data. Both XPS and RBS also show evidence for the presence of heavy metals in the oxide.

Geometrical effects on residual stresses in 7050-T7451 aluminum alloy rods subject to laser shock peening

Laser shock peening (LSP) is an emerging surface treatment technology for metallic materials, which appears to produce more significant compressive residual stresses than those from the conventional shot peening (SP) for fatigue, corrosion and wear resistance, etc. The finite element method has been applied to simulate the laser shock peening treatment to provide the overall numerical assessment of the characteristic physical processes and transformations. However, the previous researchers mostly focused on metallic specimens with simple geometry, e.g. flat surface. The current work investigates geometrical effects of metallic specimens with curved surface on the residual stress fields produced by LSP process using three-dimensional finite element (3-D FEM) analysis and aluminium alloy rods with a middle scalloped section subject to two-sided laser shock peening. Specimens were numerically studied to determine dynamic and residual stress fields with varying laser parameters and geometrical parameters, e.g. laser power intensity and radius of the middle scalloped section. The results showed that the geometrical effects of the curved target surface greatly influenced residual stress fields.

Geometrical effects on residual stresses in 7050-T7451 aluminum alloy rods subject to laser shock peening

Laser shock peening (LSP) is an emerging surface treatment technology for metallic materials, which appears to produce more significant compressive residual stresses than those from the conventional shot peening (SP) for fatigue, corrosion and wear resistance, etc. The finite element method has been applied to simulate the laser shock peening treatment to provide the overall numerical assessment of the characteristic physical processes and transformations. However, the previous researchers mostly focused on metallic specimens with simple geometry, e.g. flat surface. The current work investigates geometrical effects of metallic specimens with curved surface on the residual stress fields produced by LSP process using three-dimensional finite element (3-D FEM) analysis and aluminium alloy rods with a middle scalloped section subject to two-sided laser shock peening. Specimens were numerically studied to determine dynamic and residual stress fields with varying laser parameters and geometrical parameters, e.g. laser power intensity and radius of the middle scalloped section. The results showed that the geometrical effects of the curved target surface greatly influenced residual stress fields.

Inhibiting localized corrosion of aluminum and aluminum alloy by rare earth metal compounds : behaviors and characteristics observed using an electrochemically integrated multi-electrode array

An electrochemically integrated multi-electrode array namely the wire beam electrode (WBE) has been used to characterize the behavior of cerium chloride (CeCl3) and lanthanum chloride (LaCl3) in inhibiting localized corrosion of AA2024-T3 and AA1100. CeCl3 has been found to inhibit AA2024-T3 corrosion in 0.005 M sodium chloride (NaCl) solution by suppressing galvanic corrosion activities and by creating a large number of insignificant anodes. It has also been shown to inhibit localized corrosion of AA1100 in 0.5 M NaCl solution by promoting the random distribution of minor anodes. LaCl3 has been found to inhibit localized corrosion of AA2024-T3 at 1000 ppm, although its efficiency dropped significantly when its concentration decreased to 500 ppm. The addition of CeCl3 and LaCl3 to corrosion testing cells at later stages was unable to effectively suppress existing corrosion anodes.

Atom probe tomography study of the nanoscale heterostructure around an Al20Mn3Cu2 dispersoid in aluminum alloy 2024.

Atom probe tomography (APT) has been used to investigate the surface and sub-surface microstructures of aluminum alloy 2024 (AA2024) in the T3 condition (solution heat treated, cold worked, and naturally aged to a substantially stable condition). This study revealed surface Cu enrichment on the alloy matrix, local chemical structure around a dispersoid Al20Mn3Cu2 particle including a Cu-rich particle and S-phase particle on its external surface. Moreover, there was a significant level of hydrogen within the dispersoid, indicating that it is a hydrogen sink. These observations of the nanoscale structure around the dispersoid particle have considerable implications for understanding both corrosion and hydrogen embrittlement in high-strength aluminum alloys.

Anisotropic behavior in plasticity and ductile fracture of an aluminum alloy

Anisotropic mechanical behavior is investigated for an aluminum alloy of 6K21-IH T4 both in plastic deformation and ductile fracture. Anisotropic plastic deformation is characterized by uniaxial tensile tests of dog-bone specimens, while anisotropy in ductile fracture is illustrated with specimens with a central hole, notched specimens and shear specimens. All these specimens are cut off at every 15º from the rolling direction. The r-values and uniaxial tensile yield stresses are measured from the tensile tests of dog-bone specimens. Then the anisotropic plasticity is modeled by a newly proposed J2-J3 criterion under non-associate flow rule (non-AFR). The testing processes of specimens for ductile fracture analysis are simulated to extract the maximum plastic strain at fracture strokes as well as the evolution of the stress triaxiality and the Lode parameter in different testing directions. The measured fracture behavior is described by a shear-controlled ductile fracture criterion proposed by Lou et al. (2014. Modeling of shear ductile fracture considering a changeable cut-off value for stress triaxiality. Int. J. Plasticity 54, 56-80) for different loading directions. It is demonstrated that the anisotropic plastic deformation is described by the J2-J3 criterion with high accuracy in various loading conditions including shear, uniaxial tension and plane strain tension. Moreover, the anisotropy in ductile fracture is not negligible and cannot be modeled by isotropic ductile fracture criteria. Thus, an anisotropic model must be proposed to accurately illustrate the directionality in ductile fracture.

A comparison of continuous SPD processes for improving the mechanical properties of aluminum alloy 6111

Microstructure evolution, mechanical properties, formability, and texture development were determined for AA6111 samples processed by asymmetric rolling (ASR) with different roll friction, velocity, or diameters, conventional rolling (CR), and equal-channel-angular pressing (ECAP). Highly elongated or sheared grain structures were developed during ASR/CR and ECAP, respectively. ASR led to improved r-values and formability compared with CR primarily as a result of the development of moderate shear-texture components analogous to those developed during ECAP of billet material. ASR based on different roll diameters gave the best combination of strength, ductility, and formability.

Non-equal channel angular pressing of aluminum alloy

Strain history, microstructure and texture were studied in an aluminum alloy processed by the recently proposed process of non-equal channel angular pressing (NECAP). Comparison with alloy processed by equal channel angular pressing (ECAP) has been performed. A much finer microstructure was obtained in NECAP, showing that in this modified ECAP test the grain-refinement process was more efficient. The results indicate that the NECAP test has some interesting features that may be of interest for further research.

Enhanced tensile ductility of an ultra-fine-grained aluminium alloy

Aluminum alloy 6082 was subjected to equal-channel angular pressing (ECAP), which resulted in an ultra-fine-grained (UFG) microstructure with an average grain size of 0.2–0.4 μm. There was a pronounced effect of the grain refinement on the strain-rate sensitivity and tensile ductility. The Hart criterion of tensile necking fails to explain the observed ductility of the UFG material at low strain rates. A correlation between the observed stronger-than-expected ductility and a tendency to microshear band formation at low strain rates was established.

Magnesium alloy applications in automotive structures

The energy absorbed by magnesium alloys (high-pressure die-cast (HPDC) AM20, AM50, AM60, and extruded AZ31) in a buckling test was significantly greater than the aluminum alloy 6061 T6 and particularly mild steel of a similar weight, but was less than that of the aluminum alloy and steel for the same thickness (Figure 6).26 This indicates that mass savings can be achieved by the substitution with magnesium alloys to achieve similar energy-absorbing characteristics.

Development of the sheared edge in the trimming of steel and light metal sheet, part 1 - experimental observations

Trimming experiments were conducted on sheet metals including two drawing steels, an aluminum alloy and a magnesium alloy, using a specially designed die in a mechanical press. The punch-die clearance was varied and data obtained on the rollover and burr height as a function of the clearance. Samples were also partially trimmed to examine crack initiation, the generation of the fracture surface profile and mechanism of burr formation. The results showed that while the burr height and rollover depth generally increased with increasing clearance for all examined materials, there were differences in the fracture surface profile shape, the burr shape, and the mechanism of burr formation, between the two steels and the two light alloys. The major cause of these differences appeared to be the rate of crack propagation through the sheet material.