溶胶-凝胶光波导环形谐振腔的挥发性有机化合物传感特性

采用溶胶-凝胶法制作波导环形谐振腔, 讨论了环形谐振腔器件的传输特性。测量了在不同物质、不同体积分数的挥发性有机化合物(VOC)蒸气气氛下器件的传输光谱的敏感性。结果表明, 谐振波长随甲醇、乙醇、丙醇等醇类化合物, 以及丙酮、甲醛等蒸气体积分数的上升而向长波方向移动, 具有高的灵敏度, 且两者基本呈线性关系。其中, 对丙醇最敏感, 灵敏度达到1.403 pm/10-6。对甲烷和二甲苯也有微弱反应, 但是其灵敏度很低。也测量了水蒸气对传输谱特性的影响。观察到传输谱衬比度对不同挥发性有机化合物物质蒸气的不同敏

143Pm高自旋态和重丰中子新核素的合成及衰变性质研究

本论文从内容上可以分为两大部分：第一部分：对近球形核~(143)Pm高自旋态进行的在束γ研究。这一部分是本文的重点。利用能量为82和90 MeV的~(19)F束流，通过融合蒸发反应~(128)Te (~(19)F,4nγ) ~(143)Pm布局~(143)Pm的高自旋态。利用联合在束装置(JIBGE)的10套带BGO反康的HPGe探测器进行了标准在束γ谱学测量，包括γ射线的激发函数、γ单谱、γ-γ-t符合谱以及DCO测量。在已有工作的基础上，建立了~(143)Pm激发能高达10.5 MeV，自旋约为(61/2)h的高自旋态能级结构。观测到了28条新的跃迁能级和48条新的γ射线。对两个已知的同质异能态寿命进行了提取，并在8 MeV激发能附近进行了高自旋态同质异能态的搜索。以~(142)Nd，~(144)Sm为核实，用零级弱耦合模型对~(143)Pm的晕态能级结构进行了定量的解释。计算表明，直到激发能Ex = 6.77 MeV，自旋宇称J~π = (37/2~+)的晕态能级都可以用弱耦合模型进行很好的解释。但是，对于更高激发能的能级，组态情况要复杂的多，有出现N = 82中子闭壳打破的可能。同时，利用大基壳模型OXBASH程序对其能级结构进行了计算和讨论，其结果支持弱耦合模型的假设。第二部分：利用中能重离子的多核子转移反应，(~(186)W-2p + 2n)，(~(238)U-2p + 2n)对丰中子核~(186)Hf和~(238)Th进行了合成和鉴别。测量它们的半衰期分别为(2.6 ± 1.2) min和 (9.4 ± 2.0) min，与用质子一中子准粒子随机相近似方法的预言值是相符的。同时，对β延发裂变先驱核~(230)Ac进行了实验研究。观测到了它的两个裂变事件，得到~(230)Acβ延发裂变几率为(1.19 ± 0.85) * 10~(-8)。从而使~(230)Ac成为世界上第一种被确认了的基态β延发裂变先驱核。

Structural Evolution and Property Changes in Nd_{60}Al_{10}Fe_{20}Co_{10} Bulk Metallic Glass During Crystallization

The structural evolution and property changes in Nd60Al10Fe20Co10 bulk metallic glass (BMG) upon crystallization are investigated by the ultrasonic method, x-ray diffraction, density measurement, and differential scanning calorimetry. The elastic constants and Debye temperature of the BMG are obtained as a function of annealing temperature. Anomalous changes in ultrasonic velocities, elastic constants, and density are observed between 600–750 K, corresponding to the formation of metastable phases as an intermediate product in the crystallization process. The changes in acoustic velocities, elastic constants, density, and Debye temperature of the BMG relative to its fully crystallized state are much smaller, compared with those of other known BMGs, the differences being attributed to the microstructural feature of the BMG.

Nd_(60)Al_(10)Fe_(20)Co_(10)金属玻璃的变形行为

利用材料测试系统(MTS)、X-Ray 衍射(XRD)和扫描电镜(SEM)等手段研究了Nd 基大块金属玻璃的变形行为和断裂特征。Nd 基大块金属玻璃样品在室温下是脆性断裂,大约在500 K 时变形模式从非均匀变形转变为均匀变形,在523 K 以上表现出显著的塑性变形。在5×10-4 m/s 的应变速率下,这种Nd 基大块金属玻璃材料在523 K~600 K 之间出现明显的屈服应力下降现象,随后进入1 种稳定的粘性流动状态,而且这种屈服下降现象与温度和应变速率有关。这种在过冷液相区的变形行为与其他大块金属玻璃变形特征相似。合金的这种塑性变形行为表明了其存在稳定的过冷液相区,同时对其变形行为的研究有助于进一步了解Nd 基大块金属玻璃的反常热稳定性。

Influence of Surface Stress on Frequency of Microcantilever-Based Biosensors (vol 10, pg 307, 2004)

Microcantilever-based biosensors have been found increasing applications in physical, chemical, and biological fields in recent years. When biosensors are used in those fields, surface stress and mass variations due to bio-molecular binding can cause the microcantilever deform or the shift of frequency. These simple biosensors allow biologists to study surface biochemistry on a micro or nano scale and offer new opportunities in developing microscopic biomedical analysis with unique characteristics. To compare and illustrate the influence of the surface stress on the frequency and avoid unnecessary and complicated numerical solution of the resonance frequency, some dimensionless numbers are derived in this paper by making governing equations dimensionless. Meanwhile, in order to analyze the influence of the general surface stress on the frequency, a new model is put forward, and the frequency of the microcantilever is calculated by using the subspace iteration method and the Rayleigh method. The sensitivity of microcantilever is also discussed. (19 refs.)

Nd65Al10Fe25-xCox (x=0,5,10) bulk metallic glasses with wide supercooled liquid regions

Bulk metallic glasses of Nd65Al10Fe25-xCox (x=0,5,10) have been prepared in the form of 3 mm diam rods. Results of differential scanning calrimetry, dynamic mechanical thermal analysis (DMTA), and x-ray diffraction are presented for these alloys. It is shown that the glass transition and crystallization have been observed by DMTA. The reduced glass transition temperature of these glasses, defined as the ratio between the glass transition temperature T-g and the melting temperature T-l is in the range from 0.55 to 0.62. All these glasses have a large supercooled liquid region (SLR), ranging from 80 to 130 K. The high value of reduced glass transition temperature and wide SLR agree with their good glass formation ability.

我国随机振动研究近10年来的进展

该文回顾了中国振动工程学会随机振动专业委员会成立后的10年间我国学者在随机振动领域所进行的理论、应用技术研究方面取得的一些重要进展。着重介绍了随机非线性响应时域积分方法与空间有限元结合的随机动力有限元方法的发展；对随机振动与其他相关学科的交叉渗透进一步发展的前景也作了展望。

Shock tube study of JP-10 ignition delay time

JP-10 (exo-tetrahydrodicyclopentadiene, C10H16) ignition delay times were measured in a preheated shock tube. The vapor pressures of the JP-10 were measured directly by using a high-precision vacuum gauge, to remedy the difficulty in determining the gaseous concentrations of heavy hydrocarbon fuel arising from the adsorption on the wall in shock tube experiments. The whole variation of pressure and emission of the OH or CH radicals were observed in the ignition process by a pressure transducer and a photomultiplier with a monochromator. The emission of the OH or CH radicals was used to identify the time to ignition. Experiments were performed over the pressure range of 151-556 kPa, temperature range of 1000-2100 K, fuel concentrations of 0.1%-0.55% mole fraction, and stoichiometric ratios of 0.25, 0.5, 1.0 and 2.0. The experimental results show that for the lower and higher temperature ranges, there are different dependency relationships of the ignition time on the temperature and the concentrations of JP-10 and oxygen.

10°尖锥标模高超声速动导数的实验测量

在中科院力学所JF-4B高超声速脉冲风洞中，用模型自由飞方法对10~。尖锥开展动态实验测量，并用参数微分法辨识得到了该模型的俯仰阻尼导数。实验结果表明，脉冲风洞中模型自由飞方法得到的10~。尖锥标模高超声速动态气动特性测量值与国外可比数据一致，重复测量精度与弹道靶试验相当。

国际尖端材料技术协会(SAMPE)第24届技术会议和第3届金属及金属加工会议(1992年10月20—22日,加拿大多伦多)

<正> 国际尖端材料技术协会(SAMPE:Society for the Advancement of Material and Process Engineering)于1992年10月20—22月在加拿大多伦多市召开了两个国际学术会议:第24届国际SAMPE技术会议(24th Int.SAMPE Techn。Coaf。)和第3届国际金属与金属加工会议(3rd Int.SAMPE Metals and Metals Processin Conf.)。两个会议同时举行,全体会议(Plenary Session)在一个会场举行。前者的主题是“先进材料迎接经济的挑战”;后者的主题是“合成与加工的新进展”.尽管此二会议是在西方发达国家经济很不景

DG-10型数字光栅测微仪

本文介绍一种0～10mm、分辨率1μm数字光栅测微仪,它是一种具有任意零点、高精度的测长系统,由光栅位移传感器和数显仪两部分组成。介绍了其工作原理、主要技术指标和应用。

在高超声速脉冲风洞中使用的六分量天平测力系统和10°尖锥模型的气动力测量

在中国科学院力学研究所的 JF-4B 高超声速脉冲风洞中,对于半锥角为10°的尖锥模型进行了来流马赫数为7.8和9.9的吹风实验,在不同的α角和β角下使用六分量的压电天平进行了气动力测量。用以鉴定六分量测力系统的可靠性,并检验了新的试验段和α角与β角分别单独可变的模型支架对模型测力实验是否有干扰。实验结果与文献给的结果进行比较表明:六分量压电天平测力系统给出的实验数据是比较可靠的。

DG-10数显光栅测微仪

<正> 由中国科学院力学研究所研制的DG-10数显光栅测微仪,经中国计量科学研究院检定,其主要技术指标: 1.量程0-10mm;2.分度值0.001mm;3.示值误差在全量程内为±0.001mm;4.回程误差0.001mm;5.测杆受径向力作用时示值变化0.001mm。