Liquid-liquid extraction of Pa-233(V) with Aliquat 336

The extraction of protactinium with Aliquat 336 (methyl-tri-caprylyl ammonium chloride) in toluene, cyclohexane and chloroform from HCl, HNO3, H2SO4, HClO4, HF and mixed HCl-HF media was investigated by radioactive tracer technique. Distribution ratios of protactinium between the aqueous solution and the organic phase were determined as a function of shaking time, concentrations of acid in aqueous solution phase, extractant concentration and type of diluents in the organic phase. Aliquat 336 can almost quantitatively extract protactinium from strong HCl solution. At the same time, small amounts of HF in HCl solutions have a strong effect on Pa distribution.

Thermodynamical versus log-Poisson distribution in turbulence

The thermodynamical model of intermittency in fully developed turbulence due to Castaing (B. Castaing, J. Phys. II France 6 (1996) 105) is investigated and compared with the log-Poisson model (Z-S, She, E. Leveque, Phys. Rev. Lett. 72 (1994) 336). It is shown that the thermodynamical model obeys general scaling laws and corresponds to the degenerate class of scale-invariant statistics. We also find that its structure function shapes have physical behaviors similar to the log-Poisson's one. The only difference between them lies in the convergence of the log-Poisson's structure functions and divergence of the thermodynamical one. As far as the comparison with experiments on intermittency is concerned, they are indifferent.

Measurement Of Fracture Toughness And Interfacial Shear Strength Of Hard And Brittle Cr Coating On Ductile Steel Substrate

The fracture toughness and interfacial adhesion properties of a coating on its substrate are considered to be crucial intrinsic parameters determining performance and reliability of coating-substrate system. In this work, the fracture toughness and interfacial shear strength of a hard and brittle Cr coating on a normal medium carbon steel substrate were investigated by means of a tensile test. The normal medium carbon steel substrate electroplated with a hard and brittle Cr coating was quasi-statically stretched to induce an array of parallel cracks in the coating. An optical microscope was used to observe the cracking of the coating and the interfacial decohesion between the coating and the substrate during the loading. It was found that the cracking of the coating initiated at critical strain, and then the number of the cracks of the coating per unit axial distance increased with the increase in the tensile strain. At another critical strain, the number of the cracks of the coating became saturated, i.e. the number of cracks per unit axial distance became a constant after this critical strain. Based on the experiment result, the fracture toughness of the brittle coating can be determined using a mechanical model. Interestingly, even when the whole specimen fractured completely under an extreme strain of the substrate, the interfacial decohesion or buckling of the coating on its substrate was completely absent. The test result is different from that appeared in the literature though the identical test method and the brittle coating/ductile metal substrate system are taken. It was found that this difference can be attributed to an important mechanism that the Cr coating on the steel substrate has a good adhesion, and the ultimate interfacial shear strength between the Cr coating and the steel substrate has exceeded the maximum shear flow strength level of the steel substrate. This result also indicates that the maximum shear flow strength level of the ductile steel substrate can be only taken as a lower bound estimate on the ultimate shear strength of the interface. This estimation of the ultimate interfacial shear strength is consistent with the theoretical analysis and prediction presented in the literature.

发泡镍对肺冲击伤的防护效果及其机理研究

本研究采用激波管,探讨了发泡镍对肺冲击伤的防护效果和防护机理。结果表明,发泡镍可明显减轻肺冲击伤的程度,降低死亡率。发泡镍的防护作用可能与其降低冲击波超压峰值、延长正压上升时间和缩短正压作用时间有关。结果提示发泡镍是一种较为理想的冲击伤防护材料。

爆炸力学实验技术新进展

本文综述了爆炸力学实验和测试技术的最新进展。

岩石力学性质的研究和爆破技术的改进

<正> 一、前言 炸药爆炸后释放出大量能量,通过爆炸产物气体膨胀对岩石做功,能量以波的形式在岩石中传播,引起岩石变形、破坏、抛掷。爆破工程的任务就是要高效率地利用这种能量对岩石造成理想的块度,抛掷的岩石获得一定的初速,不应破坏的则要完整无损。要做到这些,一方面需对爆炸载荷如何引起岩石的变形、运动和破坏进行系统的实验观察,做出正确的理论分析,加深对爆破机理的认识,为爆破的最优设计打下理论基础,另一方面要有把这种理论变成现实,付诸工程实践的相应技术。

绕圆柱体跨声速流场

本文将保角曲线坐标方法应用于绕物体外部的跨声速流动.文中讨论了圆柱体跨声速绕流,计算了来流马赫数M_∞。为亚临界,超临界和M_∞为l的流场.给出了不同来流马赫数下柱面马赫数和压力分布,柱面前端中心流线上马赫数分布.给出了超临界绕流时不同来流马赫数下的声速线和来流马赫数M_∞从0.2,0.3到1的等马赫数线分布.本文部分结果与已有的理论结果进行了比较.本方法计算简单,精度好,是计算厚体跨声速绕流的有效方法,适用于不同形状的柱体和机翼的跨声速绕流.

Equilibrium of isolated magnetostatic flux structure

Two-dimensional magnetostatic models of flux structure confined in stratified atmosphere are discussed in the present paper. The magnetic field in the flux structure is assumed to be force-free at the first step. Numerical solutions for this nonlinear free boundary problem are obtained by finite element method. Results show clearly the relation between the inside fields and outside pressure, especially the influence of atmospheric pressure distribution on the flux structure.

微尺度气体流动

了解微尺度气体流动特点是微机电系统设计和优化的基础。有关的研究可以上溯到20世纪初Knudsen的平面槽道流动质量流量的测量和Millikan的小球阻力系数的测量，实验结果揭示了稀薄气体效应即尺度效应对气体运动的重要影响。由于流动特征长度很小，微尺度气流经常处到滑流区甚至过渡领域，流动的相似参数为Knudsen数和Mach数。因此可以考虑利用相似准则，通过增大几何尺寸、减小压力的途径，解决微机电系统实验观测遇到的困难。为解决直接模拟Monte Carlo方法分析微机电系统中低速稀薄气流遇到的统计涨落困难，我们提出了信息保存法（IP），该方法能够有效克服统计散布，并已成功用于多种微尺度气流。

柱形容器开口泄爆过程中的火焰传播特性

泄爆过程中流动与燃烧的相互作用机制是研究开口泄爆问题的关键.对柱形容器泄爆过程中压力与火焰发展传播过程的观测与分析表明,不同泄爆条件下压力与火焰的发展传播具有明显特点.泄爆诱导流动通过加速火焰传播、加剧火焰变形、增大火焰面积对容器内燃烧产生增强作用,泄爆流动大小主要由泄爆面积决定.小口中低压泄爆过程压力与火焰的发展过程与封闭燃烧中类似;小口高压以及大口泄爆过程中,火焰变形剧烈,传播速度明显上升,并导致压力的回升.

爆炸容器内冲击波系演化及壳体响应的数值研究

对中心装药爆炸后冲击波的产生、传播和壳体动态响应全过程进行了数值研究。认为RDX瞬时爆炸，爆炸近场采用自相似解；冲击波传播和波系演化采用PPM(the Piecewise Parabolic Method)格式求解Euler方程；壳体响应采用有限元方法求解拉氏坐标系下由虚功原理得到的动力学方程。壳体内壁面边界条件分别采用强耦合和弱耦合方法处理。结果表明：（1）当装药量相同时，薄壁壳体振型比厚壁宙体复杂得多，振幅也大；（2）当装药量不同，壳体厚度相同时，爆炸场冲击波的演化过程不同；（3）对少量装药，产生的冲击波强度低，壳体变形小，是否考虑内边界运动，对计算结果的影响不大；（4）在本文条件下，爆炸容器封头顶点所受的载荷最大，是取易发生破坏的地方，侧壁与爆点所在横截面的交线，也易破坏。

离子束外延制备GaAs:Gd薄膜

　室温条件下,用低能离子束外延制备了GaAs∶Gd薄膜,X射线衍射(XRD)结果表明除了GaAs衬底峰没有发现其它新相的衍射峰,并借助于高分辨X射线衍射(HR XRD)进一步分析了晶格常数的变化特点。俄歇电子能谱(AES)分析了样品表面的成分,及元素随深度的分布规律,在60nm深处元素的相对含量发生明显改变,运用原子力显微镜(AFM)揭示了样品表面的形貌特点。