127 resultados para bake hardening


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A theoretical description of thermo-plastic instability in simple shear is presented in a system of equations describing plastic deformation, the first law of thermodynamics and Fourier's heat transfer rule. Both mechanical and thermodynamical parameters influence instability and it is shown that two different modes of instability may exist. One of them is dominated by thermal softening and has a characteristic time and length, connected to each other by thermal diffusion.A criterion combining thermal softening, current stress, density, specific heat, work-hardening, thermal conductivity and current strain rate is obtained and practical implications are discussed.

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针对激光相变强化搭接带存在的回火软化等问题,对激光强化的球墨铸铁材料QT700-2搭接区的显微硬度、表面粗糙度、物相变化等进行了测试,并分析了强化机理。结果表明:选用合理的搭接率等工艺参数,球墨铸铁激光搭接强化后的硬度可达到50HRC以上,调节搭接宽度可以避免搭接区的回火软化问题。多道搭接强化后表层的马氏体组织呈区域性交错分布,材料表面形成非均匀、多尺度强化结构,强化后的表面具有良好的耐磨性和耐疲劳性。通过上述结果,对材料激光搭接强化的工艺参数进行了合理的优化。

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激光强度空间分布是影响脉冲激光相变硬化效果的重要因素。现有的二维点阵光束按强度均匀分布设计,不能完全满足应用要求。为此提出基于有限元(FE)分析的光强空间分布逆向设计思路,并给出了实现方法。建立脉冲激光相变硬化有限元模型,考虑了材料热物性参数随温度的变化和相变过程,并用实验进行校核。研究了二维点阵分布参数对温度场的影响,从目标温度场和硬化层形貌出发对二维点阵的分布参数进行调整,获得优化的强度空间分布。针对汽车冲压模具表面强化的工艺要求,应用此方法设计出具有实用价值的激光强度空间分布。

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基于人工神经网络基本理论,建立在成形模具表面激光强化中预测材料表面最高温度、强化效果的BP网络模型。借助于MATLAB仿真软件中的神经网络工具箱作为开发平台,将试验样本数据和经过试验验证的数值计算结果作为补充的样本数据用于BP网络的训练,利用训练好的BP网络对非线性的样本数据规律进行拟合,实现激光加工工艺参数的优化,为实际生产和加工提供有效的依据。

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采用MSC.Mare非线性有限元软件,对激光强化过程中的温度场进行数值模拟,分析了能量密度的变化对激光强化效果的影响。通过温度传感器测量激光强化时材料表面温度的变化来验证数值模拟的结果。模拟值与实测值基本吻合。结果表明,数值模拟结果可作为激光加II艺参数选择的依据。

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用大气压非转移弧层流等离子体射流,对W-Mo-Cu铸铁表面进行熔凝相变强化处理,观察和测试了试样经不同弧电流处理后的表面层组织、硬度、耐磨性.结果表明,层流等离子体射流对铸铁表面的局部快速加热熔化和冷却凝固,明显改变了表面层的微观组织,提高了硬度和抗磨损性能.

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<正> The SiCw/6061Al composites were fabricated by squeeze casting method. Varia-tions of thermal residual stresses with quenching temperature, cooling manner, aging time and thethermal-cold cycle process in thin specimens,and the distributions of thermal residual stresses alongthe distances from the surface and changes with heating temperatnres in thick specimens were stud-ied by means of X-ray diffraction (XRD). The effects of residual stresses on the mierostructure, di-mensional stability and age-hardening behavior were studied by SEM, TEM observations, and tensiletest. The results showed that there existed macrostress, microstress and thermal mismatch stress inSiCw/Al compo-site,and the presence of microstress and thermal mismatch stress has no influenceon the measurement of macrostress, but the macrostress can affect the measured value of thermalmismatch stress. Thermal res dual stress induced during the composite fabrication process, will be further in-creased when the composite were subjected to the e

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Pulsed laser beam was used to modify surface processing for ductile iron. The microstructures of processed specimen were observed using optical microscope (OM). Nanoindentation and micro-hardness of microstructures were measured from surface to inner of sample. The experimental results show that, modification zone is consisted of light melted zone, phase transformation hardening area and transient area. The light melt area is made up of coarse dendrite crystalline with a thickness less than 20um, phase transformation hardening area mainly of laminal or acicular martensite, retained austenite and graphite, i.e. M+A prime+ G. The cow-eye microstructure around graphite sphere always is formed in phase transformation hardening area zone, which consisting of a variety structure with the distance from the surface. So, it maybe as a obvious sign distinguishing modification zone border. Finally, the microstructures evolution of laser pulse processed ductile iron was analyzed coupling with beam energy distribution in space and laser pulse heating procession characteristics. The analysis shows that energy distribution of laser pulse has an important effect on microstructure during laser pulse modified ductile iron. Multi-scale and interlace arrangement are the important features for laser pulse modified ductile iron. Of microstructure.

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在国民经济中占有重要地位的汽车工业中,对于大型覆盖件模具的表面强化处理,最常见的是火焰淬火。火焰淬火对操作人员的要求高,可控性差,效果不理想,但是由于一直没有适合的方法,目前也只能继续使用。而激光表面强化技术结合柔性加工系统正是解决这类问题的新途径。传统的激光表面强化是采用把激光束离焦后进行扫描的方式,这种方法不能充分利用激光功率密度,而且往往要用转镜或振镜形成条形光斑来加快处理速度,这就需要复杂的机械结构,而且产生难以避免的重叠回火。我们提出一种新方法,利用二元光学元件来获得一种新型的周期光强分布,实现其在高功率激光系统中的应用,并设计成为集成到柔性加工系统中的组成部分,能够完成对大、中型模具表面的激光强化处理。本论文的工作主要是有关激光柔性加工系统中的光束传输及变换子系统,不仅包括理论设计、加工制作,同时还包括把该子系统有效的结合到整个系统中。本研究工作广泛涉及激光理论,光束变换和光纤传输,系统中的模块化集成应用技术,金属材料的特殊分布光强表面改性试验研究等等,是跨学科的交叉研究工作。在本论文中,重点是二元光学元件的设计方法的选择、计算机辅助设计的实现、二元光学元件的制作和在高功率激光传输中的应用,以及特殊光强分布应用于金属表面改性中的相关工作。通过把二元光学元件引入到高功率激光加工中,对出现的新现象给出一定的预测和分析,并获得了良好的强化结果,最终实现了系统的集成化,并具有实际生产所要求的可靠性和灵活性。本论文共分六章,主要包括两方面的内容。第一章为绪论,第六章为结论。第一方面内容在第二章到第四章中说明,是用于高功率激光应用中的二元光学元件的原理、设计和制作。第二方面的内容在第五章中,是关于应用前面设计制作的二元光学元件,在实际的金属材料表面处理中的实验研究,给出了相关试验结果。

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The cyclic deformation behavior Of ultrafine-grained (UFG) Ni samples synthesized by the electrodeposition method was studied. Different from those made by severely plastic deformation, the UFG samples used in this study are characterized by large-angle grain boundaries. Behaviors from nanocrystalline Ni and coarse-grained Ni samples were compared with that Of Ultrafine-grained Ni. With in situ neutron diffraction. unusual evolutions of residual lattice strains as well as cyclic hardening and softening behavior were demonstrated during the cyclic deformation. The microstructural changes investigated by TEM are discussed with respect to the unusual lattice strain and cyclic hardening/softening. (C) 2008 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

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利用光束变换技术得到不同光斑形状和不同强度分布的光束,可满足表面硬化所需要的硬化层均匀性等要求.激光硬化在材料表面产生的实际效果与光强分布密切相关,利用特定光强分布的光束进行激光硬化可以得到所需要的温度场及组织分布,直接影响材料表面硬化的效果.对高斯光束圆光束、平顶矩形光束、曲边矩形光束、点阵光斑等不同强度分布的激光表面硬化(LSH)技术进行了介绍.硬化层特定的硬度分布及组织结构等硬化效果是特定光强分布激光束与材料相互作用的结果,要获得所需硬化效果,则需要利用反求方法设计与硬化效果相对应的特定光强分布的光斑.给出了特定光强分布的激光表面硬化技术的发展趋势.

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Determination of the energy range is an important precondition of focus calibration using alignment procedure (FOCAL) test. A new method to determine the energy range of FOCAL off-lined is presented in this paper. Independent of the lithographic tool, the method is time-saving and effective. The influences of some process factors, e.g. resist thickness, post exposure bake (PEB) temperature, PEB time and development time, on the energy range of FOCAL are analyzed.

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以硅酸四乙酯(TEOS)和甲基三乙氧基硅烷(MTEOS)为前驱材料,用溶胶-凝胶(sol-gel)方法在钛宝石表面制备得到均匀性良好且具有高激光损伤阈值的有机硅复合凝胶增透膜。膜层在钛宝石激光器输出波段(750~850nm)的增透效果显著,其平均透过率超过98.6%;激光破坏阈值为2.2J/cm^2(800nm,300ps);膜层表面均匀性达到激光波面的要求,在皮秒、飞秒超短脉冲高功率激光领域具有应用价值。溶胶的性能测试结果表明,溶胶粘度和成膜折射率均随溶液中CH3SiO1.5溶胶体含量的增加而增大,而膜

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Porous SiO2 antireflective (AR) coatings are prepared from the colloidal silica solution modified with methyltriethoxysilane (MTES) based on the sol-gel route. The viscosity of modified silica suspensions changes but their stability keeps when MTES is introduced. The refractive indices of modified coatings vary little after bake treatment from 100 to 150 Celsius. The modified silica coatings on Ti:sapphire crystal, owning good homogeneity, display prominent antireflective effect within the laser output waveband (750-850 nm) of Ti:sapphire lasers, with average transmission above 98.6%, and own laser induced damage thresholds (LIDTs) of more than 2.2 J/cm2 at 800 nm with the pulse duration of 300 ps.

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一. 通过对黄瓜类囊体及其基粒片层、间质片层、PS II放氧颗粒和LHC II 复合体脂类成分的分析,得 到以下结果:各膜区均含有类囊体膜的五种脂类成分,在类囊体及其基粒片层、间质片层和PS II放氧颗粒中,MGDG含量最高,分别为42.5%、40.5%、46.3%、和35.7%,其次是DGDG,含量在31-35%之间。值得注意的是黄瓜类囊体间质片层MGDG含量高于基粒片层,而且DGDG/DGDG分子比也较高。这在其它植物材料中还未见报道。在黄瓜LHC II中,PG含量最高,为35.5%,约是类囊体膜PG含量的3倍。从基粒片层、PS II放氧颗粒到LHC II, PG含量呈逐渐增加的趋势,而在间质片层中,PG含量最低。SQDG除在LHC II中含量稍低外,在其它膜区中的分布没有明显的差异。脂类脂肪酸组成分析结果表明:MGDG主要含亚麻酸,含量在90%以上。DGDG也主要含亚麻酸,含量在90%左右,DGDG所含棕榈酸多于MGDG中的含量。SQDG中主要脂肪酸组分为棕榈酸和亚麻酸。不同膜区MGDG、DGDG和SQDG脂肪酸组成没有明显差异在PG中含量最高的脂肪酸是叶绿体特有的反式十六碳一烯酸(trans-16:1)。此外,PG还含有较多的棕榈酸、硬脂酸和油酸。在不同膜区PG的脂肪酸组成有较明显的差异。 根据以上结果,我们推测脂类除了形成膜的流动性基质外,还可能选择性地结合在膜蛋白周转形成特 异的脂质微区,通过膜脂膜蛋白的相互作用,以行使其特殊的生理功能。 二、通过比较两种不同抗寒性小麦品种在低温锻炼前后类囊体脂类及其脂肪酸成分、LHC II复合体及类囊体吸收光谱、低温荧光发射光谱,发现经低温锻炼后:(1)抗寒与不抗寒小麦品种类囊体PG的trans-16:1含量均明显降低,抗寒品种类囊体MGDG/DGDG比值也明显降低,而不抗寒品种这一比值变化不明显。(2)抗寒品种脂/色素比值明显增高,而不抗寒品种滑明显增加。(3)抗寒与不抗寒品种LHC II宏聚体含量均降低而单体含量增加。(4)抗寒与不抗寒品种类囊体吸收光谱四阶导数光谱A_(683)/A_(652)比值均升高。(5)不抗寒品种低温荧光发射光谱F_(685)/F_(738)比值上升,而抗寒品种这一比值没有变化。通过对上述结果的分析,我们认为低温锻炼过程中类囊体膜流动性增强是使抗寒品种抗寒力增强的主要原因之一,此外,MGDG含量降低对膜的稳定性可能起重要作用。trans-16:1含量的降低和LHC II寡聚体解聚可能是植物对于低温的一种适应性反应。