微重力池沸腾现象中的汽泡行为特性

本文对准稳态加热条件下的微重力核态池沸腾中的汽泡行为特征进行了实验研究，分析了初始核化过程、汽泡数密度、汽泡尺寸及其运动速度等的变化趋势，探讨了过冷度及加热历史等因素对相关特性的影响。实验发现：微重力条件下汽泡生成后沿加热面不停地移动；原生汽泡会聚合形成大汽泡，大汽泡不断捕掠小汽泡而长大，直到大汽泡覆盖整个加热面；汽泡生长速度随过冷度增加而变慢。

气相扩散速率对溶菌酶晶体生长的影响

为研究气相扩散速率对溶菌酶晶体生长的影响,特设计了一种可方便调节气相扩散速率的晶体生长样品池,并用动态光散射法对不同气相扩散速率下晶体生长过程进行了研究.实验结果表明,随着气相扩散速率的增加,晶体生长过程中的成核阶段缩短.气相扩散速率通过影响溶菌酶溶液形成过饱和的速率来影响生长出的晶体的数量和大小.

连续冷却多阶段快速凝固过程起始形核温度的计算

基于快速凝固的瞬态形核理论和对连续冷却条件下整个温度区间的瞬态形核数和晶核体积积分，导出了连续冷却多阶段快速凝固条件下过冷熔体中各析出相起始形核温度的计算方法。假定界面传热处于牛顿冷却方式，对Ni－Al合金平面流铸条带形成过程中析出的化合物相起始形核温度做了计算。

Influence of Evaporation on Marangoni-Benard Instability

Evaporative convection and instability give rise to both scientific and technological interests. Practically, a number of the industrial applications such as thin-film evaporators, boiling technologies and heat pipes concern with the evaporation process of which through the vapor-liquid interface the heat and mass transfer occur. From a physical viewpoint, one of interesting questions is the mechanisms of convection instability in thin-liquid layers induced by the coupling of evaporation phenomenon and Marangoni effect at the mass exchanged interface. Classical theories, including Rayleigh’s and Pearson’s, have only successfully explained convection in a liquid layer heated from below without evaporation. However these theories are unable to explain the convection in an evaporating thin layer, especially liquid layer is cooled from below. In present paper, a new two-sided model is put forward rather than the one-sided model in previous works. In previous works, the vapor is treated as passive gas and dynamics of vapor has been ignored. In this case, the vapor liquid system can be described by one-sided model. In our two-sided model, the dynamics of vapor should be considered. Linear instability analysis of the Marangoni-Bénard convection in the two-layer system with an evaporation interface is performed. We define a new evaporating Biot number which is different from the Biot number in one-sided model and obtain the curves of critical Marangoni number versus wave number. In our theoretical results, the Biot number and the evaporating velocity play a major role in the stability of the vapor-liquid system.

“Deborah Numbers”, Coupling Multiple Space and Time Scales and Governing Damage Evolution to Failure

Two different spatial levels are involved concerning damage accumulation to eventual failure. nucleation and growth rates of microdamage nN* and V*. It is found that the trans-scale length ratio c*/L does not directly affect the process. Instead, two independent dimensionless numbers: the trans-scale one * * ( V*)including the * **5 * N c V including mesoscopic parameters only, play the key role in the process of damage accumulation to failure. The above implies that there are three time scales involved in the process: the macroscopic imposed time scale tim = /a and two meso-scopic time scales, nucleation and growth of damage, (* *4) N N t =1 n c and tV=c*/V*. Clearly, the dimensionless number De*=tV/tim refers to the ratio of microdamage growth time scale over the macroscopically imposed time scale. So, analogous to the definition of Deborah number as the ratio of relaxation time over external one in rheology. Let De be the imposed Deborah number while De represents the competition and coupling between the microdamage growth and the macroscopically imposed wave loading. In stress-wave induced tensile failure (spallation) De* < 1, this means that microdamage has enough time to grow during the macroscopic wave loading. Thus, the microdamage growth appears to be the predominate mechanism governing the failure. Moreover, the dimensionless number D* = tV/tN characterizes the ratio of two intrinsic mesoscopic time scales: growth over nucleation. Similarly let D be the “intrinsic Deborah number”. Both time scales are relevant to intrinsic relaxation rather than imposed one. Furthermore, the intrinsic Deborah number D* implies a certain characteristic damage. In particular, it is derived that D* is a proper indicator of macroscopic critical damage to damage localization, like D* ∼ (10–3~10–2) in spallation. More importantly, we found that this small intrinsic Deborah number D* indicates the energy partition of microdamage dissipation over bulk plastic work. This explains why spallation can not be formulated by macroscopic energy criterion and must be treated by multi-scale analysis.

丝状加热面池沸腾临界热流尺度效应研究

本文以丝状加热表面上的池沸腾传热现象为主要研究对象，利用地面常重力实验，研究了不同热丝直径、不同过冷度下（(0～40℃）的丝状加热片面FC-72液体和丙酮液体的池沸腾传热特性。 本文利用自主研发的一套可控过冷度池沸腾实验设备，使用纯度为99.99%的铂丝同时作为加热元件和测温元件，加热丝直径分别为0.06mm、0.025mm、0.1mm，长度为30mm。实验采用控制加热电压按阶梯形式增长或下降（时间常数约20s）的稳态加热方式。 实验所得单相自然对流传热数据同Kuehn-Goldstein（1976）换热公式预测结果具有较高的一致性，说明实验设备可靠、实验数据可信。 实验过程中发现，在相同压力条件下，随着过冷度的增加，沸腾传热强化；CHF值在低过冷度时呈线性增加，然后增加趋势变缓。丙酮实验中，0.06mm热丝和0.1mm热丝在低过冷度(2.5～10℃)情况下都出现了从自然对流直接进入双膜态现象，不过，当降低加热电压时，膜态沸腾仍转化为核态沸腾，此时继续增高加热电压，沸腾曲线仍沿常规核态沸腾曲线上升至CHF后，再转换为膜态沸腾。对于同等直径热丝，无论核态沸腾或双膜态沸腾，在丙酮中所产生汽泡尺寸明显偏大。 过冷沸腾中，临界热流随过冷度的增加呈现出非线性依赖关系。在低过冷度线性区，FC-72中实验结果与几种低过冷度线性模型较一致；丙酮中实验结果 随 变化斜率明显高于几种低过冷度线性模型的预测，显示出对尺度的依赖关系。这说明在小Bond数时存在尺度效应对过冷度的影响，即对于小Bond数情况过冷度和尺度效应的耦合作用是非常重要的。 饱和沸腾中，FC-72和丙酮的CHF值随热丝直径的减小而不断增加，其中，FC-72的CHF数值尽管比LD模型预测结果略低，但定性地依然可用LD模型进行描述，尽管相比于LD模型原始的适用范围 已扩大了1~2个数量级；但丙酮的实验数据却远小于LD模型预测结果。综合分析表明，尽管热丝直径相同，但物性的差异使得FC-72和丙酮实验中的数据点分别处于不同的尺度特征区域，反映了小Bond数情形下分区准则的物性依赖性。

Formation of Single and Multiple Deformation Twins in Nanocrystalline fcc Metals

Deformation twins are often observed to meet each other to form multi-fold twins in nanostructured face-centered cubic (fcc) metals.Here we propose two types of mechanism for the nucleation and growth of four different single and multiple twins. These mechanisms provide continuous generation of twinning partials for the growth of the twins after ucleation. A relatively high stress or high strain rate is needed to activate these mechanisms, making them more prevalent in nanocrystalline materials than in their coarse-grained counterparts.Experimental observations that support the proposed mechanisms are presented.

微重力准稳态池沸腾中的气泡动力学研究

本文实验研究了微重力条件下的准稳态核态池沸腾现象中的气泡动力学特征及其对传热特性的影响,发现在低过冷度沸腾中,聚合汽泡表面的强烈振荡促进了整个加热面上的核化过程与核态沸腾传热;而高过冷沸腾中,聚合气泡在表面张力作用下呈球状,难以覆盖整个加热表面,导致核态沸腾向膜态沸腾的过度过程表现为"核态沸腾+局部的干斑扩展"现象,相应的传热曲线没有明显转折.微重力条件下池沸腾临界热流随过冷度和压力的增加而升高,与地面结果定性相符.

微重力池沸腾传热实验研究

本文实验研究了平板加热面FC-72液体的准稳态池沸腾传热现象,利用地面常重力实验、SJ-8卫星搭载微重力实验等手段,分析了不同重力、压力及过冷度条件下平板加热面上的池沸腾传热特性.微重力条件下,相近压力或过冷度时,传热系数和CHF随过冷度或压力增大而增大.相对常重力,传热曲线明显变缓,沸腾起始时的壁面过热度降低,CHF仅为常重力的40%或更低.

微重力池沸腾传热研究

对利用中国返回式卫星搭载开展的两次微重力池沸腾空间实验及地基常重力和落塔短时微重力实验的结果进行了评述.研究发现微重力时丝状加热器沸腾传热会略有强化,而平板力加热器则在高热流条件下明显恶化.微重力时,气泡脱落前存在沿加热面的横向运动,加剧了相邻气泡间的合并,合并气泡会在其表而振荡作用下从加热面脱落.Marangoni效应对于微重力气泡行为有重要影响.

紫外激光诱导近化学计量比钽酸锂晶体铁电畴反转

对紫外激光诱导近化学计量比钽酸锂晶体铁电畴反转进行了实验研究。波长为351 nm的连续紫外激光被聚焦在近化学计量比钽酸锂晶体的-z表面,同时沿与晶体自发极化相反的方向施加均匀外电场。实验证实紫外激光辐照可以有效地降低晶体畴反转所需的矫顽电场,采用数字全息干涉测量技术检测证实在激光辐照区域实现局域畴反转。研究表明采用紫外激光诱导可以实现对近化学计量比钽酸锂晶体铁电畴反转的局域控制。提出了物理机理的理论分析,认为外电场和激光辐照场的共同作用在晶体内部产生高浓度、大尺寸的缺陷结构,缺陷一定程度上降低畴体成核和畴

Red laser-induced domain inversion in MgO-doped lithium niobate crystals

A laser beam at wavelength 647 nm is focused on a sample of 5 mol% MgO-doped lithium niobate crystal for domain inversion by a conventional external electric field. In this case, a reduction of 36% in the electric field required for domain nucleation (nucleation field) is observed. To the best of our knowledge, it is the longest wavelength reported for laser-induced domain inversion. This extends the spectrum of laser inducing, and the experimental results are helpful to understand the nucleation dynamics under laser illumination. The dependence of nucleation fields on intensities of laser beams is analysed in experiments.

Phase mapping of domain kinetics in lithium niobate by digital holographic interferometry

The phase mapping of domain kinetics under the uniform steady-state electric field is achieved and investigated in the LiNbO3 crystals by digital holographic interferometry. We obtained the sequences of reconstructed three-dimensional and two-dimensional wave-field phase distributions during the electric poling in the congruent and near stoichiometric LiNbO3 crystals. The phase mapping of individual domain nucleation and growth in the two crystals are obtained. It is found that both longitudinal and lateral domain growths are not linear during the electric poling. The phase mapping of domain wall motions in the two crystals is also obtained. Both the phase relaxation and the pinning-depinning mechanism are observed during the domain wall motion. The residual phase distribution is observed after the high-speed domain wall motion. The corresponding analyses and discussions are proposed to explain the phenomena.

Temperature dependence of thermal properties of Ag8In14Sb55Te23 phase-change memory materials

The dependence of thermal properties of Ag8In14Sb55Te23 phase-change memory materials in crystalline and amorphous states on temperature was measured and analyzed. The results show that in the crystalline state, the thermal properties monotonically decrease with the temperature and present obvious crystalline semiconductor characteristics. The heat capacity, thermal diffusivity, and thermal conductivity decrease from 0.35 J/g K, 1.85 mm(2)/s, and 4.0 W/m K at 300 K to 0.025 J/g K, 1.475 mm(2)/s, and 0.25 W/m K at 600 K, respectively. In the amorphous state, while the dependence of thermal properties on temperature does not present significant changes, the materials retain the glass-like thermal characteristics. Within the temperature range from 320 K to 440 K, the heat capacity fluctuates between 0.27 J/g K and 0.075 J/g K, the thermal diffusivity basically maintains at 0.525 mm(2)/s, and the thermal conductivity decreases from 1.02 W/m K at 320 K to 0.2 W/m K at 440 K. Whether in the crystalline or amorphous state, Ag8In14Sb55Te23 are more thermally active than Ge2Sb2Te5, that is, the Ag8In14Sb55Te23 composites bear stronger thermal conduction and diffusion than the Ge2Sb2Te5 phase-change memory materials.

Er3+ and Yb3+ codoped phosphate laser glass for high power flashlamp pumping

A novel Vb(3+)-Er-(3+) codoped phosphate glass for high power flashlamp pumping and high repetition rate laser at 1.54 mu m, designated EAT5-2, is developed. The weight-loss rate of is 1.3 x 10(-5) gcm(-2) h(-1) in boiling water, which is comparable to Kigre's QX-Er glass. Some spectroscopic parameters are analysed by Judd-Ofelt theory and McCumber theory The emission cross section is calculated to be 0.73 x 10(-20) cm(2). The thermo-mechanical properties of EAT5-2 are modified after an ion-exchange chemical strengthening process in a KNO3/NaNO3 molten salt bath. The thresholds for optical damage from the flashlamp pumping are tested on glass rods. A repetition rate of 15 Hz is achieved for chemically strengthened glass. The laser experimental results at. 1.54 mu m from flashlamp pumping are also reported.