Synthesis, spectral and structural studies of oxovanadium(IV/V) complexes derived from 2-hydroxyacetophenone-3-hydroxy- 2-naphthoylhydrazone: polymorphs of oxovanadium(V) complex [VOL(OCH3)]


Autoria(s): Prathapachandra Kurup, M R; Seena, E B; Mini, Kuriakose
Data(s)

14/07/2014

14/07/2014

09/02/2010

Resumo

Oxovanadium(IV/V) complexes of 2-hydroxyacetophenone- 3-hydroxy-2-naphthoylhydrazone (H2L) have been synthesized and characterized. The complexes were characterized by elemental analyses, IR, electronic and EPR spectra. The oxovanadium(V) complex [VOL (OCH3)] is crystallized in two polymorphic forms, denoted by 1a and 1b, with space groups Pn21a and P 1, respectively. Both have distorted square pyramidal structures.

Struct Chem (2010) 21:599–605 DOI 10.1007/s11224-010-9589-7

Cochin University of Science and Technology

Identificador

http://dyuthi.cusat.ac.in/purl/4003

Idioma(s)

en

Publicador

Springer

Palavras-Chave #Oxovanadium(IV/V) complexes #2-Hydroxyacetophenone #3-Hydroxy-2-naphthoylhydrazide #Crystal structures
Tipo

Article