The production of ultrafine ferrite in low-carbon steel by strain-Induced transformation

An investigation into the production of ultrafine (1 µm) equiaxed ferrite (UFF) grains in low-carbon steel was made using laboratory rolling, compression dilatometry, and hot torsion techniques. It was found that the hot rolling of thin strip, with a combination of high shear strain and high undercooling, provided the conditions most suitable for the formation of this type of microstructure. Although high strains could be applied in compression and torsion experiments, large volume fractions of UFF were not observed in those samples, possibly due to the lower level of undercooling achieved. It is thought that ferrite refinement was due to a strain-induced transformation process, and that ferrite grains nucleated on parallel and linear deformation bands that traversed austenite grains. These bands formed during the deformation process, and the undercooling provided by the contact between the strip and the work rolls was sufficient to drive the transformation to homogeneous UFF grains.

Characterization on ferrite microstructure evolution during large strain warm torsion testing of plain low carbon steel

Ferrite grain/subgrain structures evolution during the extended dynamic softening of a plain low carbon steel was investigated throughout the large strain warm deformation by hot torsion. Microstructural analysis with electron back-scattering diffraction (EBSD) scanning electron microscope (FEG/SEM) was carried out on the ferrite microstructural parameters. The results showed that the warm flow stress–strain curves are similar to those affected only by dynamic softening and an extended warm flow softening is seen during large strain deformation up to 30. Furthermore, with an increase in strain up to ~ vert, similar1 the grain size of ferrite, misorientation angle and fraction of high-angle boundaries gradually decrease and fraction of low-angle boundaries increases. With a further increase in the strain beyond ~, vert, similar2, these parameters remain approximately unchanged. No evidence of discontinuous dynamic recrystallisation involving nucleation and growth of new grains was found within ferrite. Therefore, the dynamic softening mechanism observed during large strain ferritic deformation is explained by continuous dynamic recrystallization (CDRX).

In-situ observations of Widmanstätten ferrite formation in a low carbon steel

An in situ laser-scanning confocal microscopy study has been undertaken into Widmanstätten ferrite formation in an Fe–C alloy, in combination with electron backscattered diffraction. It has been found for the first time that the sympathetic nucleation of Widmanstätten ferrite on grain boundary allotriomorphs can exhibit a step wise change in orientation and growth direction until the most favourable growth conditions are achieved.

High-temperature laser-scanning confocal microscopy as a tool to study the interface instability during unsteady-state solidification of low-carbon steel

Solidification microstructure is a defining link between production techniques and the mechanical properties of metals and in particular steel. Due to the difficulty of conducting solidification studies at high temperature, knowledge of the development of solidification microstructure in steel is scarce. In this study, a laser-scanning confocal microscopy (LSCM) has been used to observe in situ and in real-time the planar to cellular to dendritic transition of the progressing solid/liquid interface in low carbon steel. Because the in situ observations in the laser-scanning confocal microscopy are restricted to the surface, the effect of sample thickness on surface observations was determined. Moreover, the effect of cooling rate and alloy composition on the planar to cellular interface transition was investigated. In the low-alloyed, low-carbon steel studied, the cooling rate does not seem to have an effect on the spacing of the cellular microstructure. However, in the presence of copper and manganese, the cell spacing decreased at higher cooling rates. Higher concentrations of copper in steel resulted on an increased cell spacing at the same cooling rates.

Effects of Milling on Surface Integrity of Low-Carbon Steel

This work measured the effect of milling parameters on the surface integrity of low-carbon alloy steel. The Variance Analysis showed that only depth of cut did not influence on the workpiece roughness and the Pearson's Coefficient indicated that cutting speed was more influent than tool feed. All cutting parameters introduced tensile residual stress in workpiece surface. The chip formation mechanism depended specially on cutting speed and influenced on the roughness and residual stress of workpiece.

Effect of citrate ions on the electrochemical behaviour of low-carbon steel in borate buffer solutions

The electrochemical behaviour of cold-rolled low carbon steel was studied on both active and passive potential regions in borate buffer solutions with and without the addition of sodium citrate (NaCit). In the active region anodic charges increased significantly and RCT values decreased with citrate, due to the formation of soluble complexes. In the passive potential region the film formed at +0.4 V in borate buffer solution with and without 0.010 M NaCit is probably enriched by Fe3O4 oxide, while films formed at +0.8 V are probably enriched by gamma-Fe2O3. The equivalent circuit [R-s(R(CT)Q)] fitted all experimental impedance data. (C) 2003 Elsevier Ltd. All rights reserved.

Microstructure evolution during warm deformation of low carbon steel with dispersed cementite

The microstructure evolution and mechanical behavior during large strain of a 0.16%C-Mn steel has been investigated by warm torsion tests. These experiments were carried out at 685°C at equivalent strain rate of 0.1 s . The initial microstructure composed of a martensite matrix with uniformly dispersed fine cementite particles was attained by quenching and tempering. The microstructure evolution during tempering and straining was performed through interrupted tests. As the material was reheated to testing temperature, well-defined cell structure was created and subgrains within lath martensite were observed by TEM; strong recovery took place, decreasing the dislocation density. After 1 hour at the test temperature and without straining, EBSD technique showed the formation of new grains. The flow stress curves measured had a peculiar shape: rapid work hardening to a hump, followed by an extensive flow-softening region. 65% of the boundaries observed in the sample strained to ε = 1.0 were high angle grain boundaries. After straining to ε = 5.0, average ferrite grain size close to 1.5 μm was found, suggesting that dynamic recrystallization took place. Also, two sets of cementite particles were observed: large particles aligned with straining direction and smaller particles more uniformly dispersed. The fragmentation or grain subdivision that occurred during reheating and tempering time was essential for the formation of ultrafine grained microstructure.

Coatings for the protection of low carbon steel at elevated temperatures /

"Metallurgy and Ceramics."

FeNbP in ultra-low carbon Nb-added steel containing high P

Precipitation of FeTiP is reported to occur in Ti-added IF steels containing high P during thermomechanical processing. An ultra-low carbon (ULC) Nb-added steel ingot containing a higher P content (< 0.8 wt-%) was produced via aluminothermic reduction of Fe2O3 followed by double electron beam melting (EBM). FeNbP coarse precipitates were observed in the as-cast microstructure. After soaking at 1050C for 1 h, the plate was hot rolled from 31 mm down to 7 mm in thickness (total reduction of 77%). During cold rolling of these hot bands we observed embrittlement. We believe that this embrittlement can be attributed to the presence of the FeNbP precipitates. Light optical and scanning electron microscopy (SEM/EDS) were used to characterize the microstructure of this ULC steel. (C) 2000 Elsevier B.V. All rights reserved.

Experimental Study of crack propagation in carbon steel using acoustic emission

Acoustic emission technique has become a significant and powerful structural health monitoring tool for structures. Researches to date have been done on crack location, fatigue crack propagation in materials and severity assessment of failure using acoustic emission technique. Determining severity of failure in steel structures using acoustic emission technique is still a challenge to accurately determine the relationship between the severity of crack propagation and acoustic emission activities. In this study three point bending test on low carbon steel samples along with acoustic emission technique have been used to determine crack propagation and severity. A notch is introduced at the tension face of the loading point to the samples to initiate the crack. The results show that the percentage of load drop of the steel specimen has a reciprocal relationship with the crack opening i.e. crack opening zones are influenced by the loading rate. In post yielding region, common acoustic emission signal parameters such as, signal strength, energy and amplitudes are found to be higher than those at pre-yielding and at yielding.

Recrystallization textures in course grained low carbon and interstitial free steels

The microstructures and textures of coarse grained cold rolled, partially recrystallized and fully recrystallized low carbon and interstitial free steel were examined by optical microscopy, scanning electron microscopy (SEM) and electron backscatter diffraction (EBSD). The recrystallization textures of the two grades are markedly different, with the low carbon steel having a predominantly Goss {11O}<OOl> texture and the interstitial free steel having a <1ll>/1ND texture with a strong {III }<112> component. One possible explanation for the texture difference is that less severe localization of flow during deformation of interstitial free steels causes less Goss nuclei to be generated. While some support for this view is provided by the results presented in this paper, the results suggest that another mechanism may be at least partially responsible. Examination of micro
shear bands on the surface of pre-polished samples showed that a higher proportion of micro shear bands remained active at high rolling reductions in the low carbon steel, compared with the interstitial free grade. Regions of Goss orientation within bands that have ceased to operate rotate to
near-{ III }<112> orientations with further deformation. Consequently, the recrystallization texture of coarse grained interstitial free steels can be rationalized by a reduction in the availability of Goss nuclei and an increase in the availability of {Ill }<112> nuclei due to a "Goss to {Ill }<112>" rotation within micro shear bands that have ceased to operate.