The microstructure evolution and mechanical properties of cryorolled Al alloys

A solutionized Al2024 alloy was subjected to rolling at liquid nitrogen temperature (cryorolling) resulting in an ultra-fine stmcture. The material was also subjected to recovery annealing at 160°C. The ultrafine structured material demonstrated increased strength but very low ductility. The uniform elongation of the material after recovery annealing increased without any sacrifice of strength.

Simultaneously enhanced strength and ductility of titanium via multimodal grain structure

Commercial Ti with a multimodal grain structure was successfully produced using cryorolling, followed by low-temperature annealing. This multimodal grain structure Ti exhibited a combination of high yield strength (926 MPa), a uniform elongation of 11% and a failure elongation of 23%. The strength enhancement was mainly derived from the ultrafine equiaxed grains, while the improved ductility originated from the large fraction of high-angle grain boundaries and the multimodal grain structure.

Cryo-rolling and formability of 2024 aluminium

Sheets of precipitate hardenable 2024 aluminium have been processed by rolling at liquid nitrogen temperature in order to refine the microstructure. A number of different aging/heat treating procedures have been utilised that have resulted in significantly different mechanical properties. The cryo-rolled material was heat treated at 150 °C for varying times and the resulting mechanical properties evaluated as a function of this holding time. The resulting properties were found to be strongly influenced by precipitates that formed either during the aging step, rolling process or the subsequent heat treatment. The formability of the cryo-rolled and heat treated material has been investigated using a limiting dome height test (Erichsen cupping test).

Improved contact load-bearing capacity of ultra-fine grained titanium : Multilayering and grading

The contact load-bearing response and surface damage resistance of multilayered hierarchical structured (MHSed) titanium were determined and compared to monolithic nanostructured titanium. The MHS structure was formed by combining cryorolling with a subsequent Surface Mechanical Attrition Treatment (SMAT) producing a surface structure consisted of an outer amorphous layer containing nanocrystals, an inner nanostructured layer and finally an ultra-fine grained core. The combination of a hard outer layer, a gradual transition layer and a compliant core results in reduced indentation depth, but a deeper and more diffuse sub-surface plastic deformation zone, compared to the monolithic nanostructured Ti. The redistribution of surface loading between the successive layers in the MHS Ti resulted in the suppression of cracking, whereas the monolithic nanograined (NG) Ti exhibited sub-surface cracks at the boundary of the plastic strain field. Finite element models with discrete layers and mechanically graded layersrepresenting the MHS system confirmed the absence of cracking and revealed a 38% decrease in shear stress in the sub-surface plastic strain field, compared to the monolithic NG Ti. Further, the mechanical gradation achieves a more gradual stress distribution which mitigates the interface failure and increases the interfacial toughness, thus providing strong resistance to loading damage. © 2014 Elsevier Ltd.