8 resultados para 64101
Resumo:
C-axis-orientated ZnO thin films were prepared on glass substrates by pulsed-laser deposition (PLD) technique in an oxygen-reactive atmosphere, using a metallic Zn target. The effects of growth condition such as laser energy and substrate temperature on the structural and optical properties of ZnO films had been investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission spectra and room-temperature (RT) photoluminescence (PL) measurements. The results showed that the thickness, crystallite size, and compactness of ZnO films increased with the laser energy and substrate temperature. Both the absorption edges and the UV emission peaks of the films exhibited redshift, and UV emission intensity gradually increased as the laser energy and substrate temperature increased. From these results, it was concluded that crystalline quality of ZnO films was improved with increasing laser energy and substrate temperature. (c) 2007 Elsevier B.N. All rights reserved.
Resumo:
In this paper we study the evolution of the kinetic features of the martensitic transition in a Cu-Al-Mn single crystal under thermal cycling. The use of several experimental techniques including optical microscopy, calorimetry, and acoustic emission, has enabled us to perform an analysis at multiple scales. In particular, we have focused on the analysis of avalanche events (associated with the nucleation and growth of martensitic domains), which occur during the transition. There are significant differences between the kinetics at large and small length scales. On the one hand, at small length scales, small avalanche events tend to sum to give new larger events in subsequent loops. On the other hand, at large length scales the large domains tend to split into smaller ones on thermal cycling. We suggest that such different behavior is the necessary ingredient that leads the system to the final critical state corresponding to a power-law distribution of avalanches.
Resumo:
Este recurso trata de un aspecto particular de la enseñanza del inglés como lengua extranjera: la práctica de la fluidez . Sugiere algunas formas en que los estudiantes pueden ser inducidos a hablar en el aula, utilizando el lenguaje de forma creativa, a propósito, y de forma individual. El vehículo de esa utilización se define, en un sentido muy amplio de la palabra, como la discusión. La primera parte del recurso trata acerca de una serie de elementos que son esenciales para una buena discusión: algunos de ellos son bien conocidos: temas interesantes, trabajo en grupo, juego de roles, mientras que otros han sido relativamente descuidados: la como enfocar la tarea, el proceso de la organización. La segunda parte consta de unos cincuenta ejemplos prácticos que van desde lo más sencillo a lo complejo y, por lo tanto, se pueden usar con una amplia gama de estudiantes, desde la enseñanza elemental hasta la enseñanza secundaria y de adultos.
Resumo:
The surface oxidation of UO2 sintered plates at 170-275 ° C was studied in situ by high temperature X-ray diffractometry. At very low oxygen concentration, UO2 is oxidized to U4O9, while at 300°C and argon-20 vol% oxygen it is oxidized up to U3O7. X-ray diffraction profiles of the UO2, U4O9 and U3O7 phases were well characterized during the transformations. The activation energy for the transformation of UO2 to U4O9, obtained from X-ray diffraction data, was found to be 117 ± 9 kJ/mol and 90 ± 14 kJ/mol for the β-(311) and α-(200) reflections, respectively. © 1991.