Fractal behavior throughout stretch zone of 15-5PH steel under elastic-plastic loading conditions

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

MRT letter: Extended depth from focus reconstruction method for stretch zone measurement in 15-5PH steel

The stretch zone width (SZW) data for 15-5PH steel CTOD specimens fractured at -150 degrees C to + 23 degrees C temperature were measured based on focused images and 3D maps obtained by extended depth-of-field reconstruction from light microscopy (LM) image stacks. This LM-based method, with a larger lateral resolution, seems to be as effective for quantitative analysis of SZW as scanning electron microscopy (SEM) or confocal scanning laser microscopy (CSLM), permitting to clearly identify stretch zone boundaries. Despite the worst sharpness of focused images, a robust linear correlation was established to fracture toughness (KC) and SZW data for the 15-5PH steel tested specimens, measured at their center region. The method is an alternative to evaluate the boundaries of stretched zones, at a lower cost of implementation and training, since topographic data from elevation maps can be associated with reconstructed image, which summarizes the original contrast and brightness information. Finally, the extended depth-of-field method is presented here as a valuable tool for failure analysis, as a cheaper alternative to investigate rough surfaces or fracture, compared to scanning electron or confocal light microscopes. Microsc. Res. Tech. 75:11551158, 2012. (C) 2012 Wiley Periodicals, Inc.

Fadiga no aço inox 15-5PH revestido por HVOF: aplicação em trem de pouso

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Fractografia quantitativa de superfícies obtidas em ensaios de propagação de trincas por fadiga em aço inoxidável 15 –5PH

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Influência do tratamento superficial 3IP na vida em fadiga dos aços ABNT 4340 e 15-5PH para aplicação aeronáutica

Pós-graduação em Engenharia Mecânica - FEG

Solution heat treatment of plasma nitrided 15-5PH stainless steel - Part I: Improvement of the corrosion resistance

The results of the investigation on Solution Heat Treatment of Plasma Nitrided (SHTPN) precipitation-hardened steel 15-5PH are presented. The layers have been obtained by the plasma nitriding process followed by solution heat treatment at different temperatures. The influence of the solution heat treatment after nitriding on the dissolution process of the nitrided layer has been considered. The nitrided layers were studied by scanning electron microscopy, X-ray microanalysis (EDX), and X-Ray diffraction. Micro-hardness tests of the nitrided layers and solubilized nitrided layers have been carried out and interpreted by considering the processing conditions. It was found that high nitrogen austenitic cases could be obtained after SHTPN of martensitic precipitation-hardened steel (15-5PH). When Solution Heat Treatment (SHT) was performed at 1100 °C, some precipitates were observed. The amount of precipitates significantly reduced when the temperature increased. The EDX microanalysis indicated that the precipitate may be chromium niobium nitride. When the precipitation on the austenite phase occurred in small amount, the corrosion resistance increased in SHTPN specimens and the pit nucleation potential also increased. The best corrosion result occurred for SHT at 1200 °C.

Correlações entre zona de estiramento e tenacidade à fratura para aço 15-5PH

This work includes a study on the stretch zone and the influence of the toughness conditions at fracture in size and appearance. It was done a literature review about material properties, fracture mechanics concepts, definitions and formation of stretch zone, importance of tenacity for structural calculation, methods and standards to measure the toughness of metallic material fracture and presents the method used in microscopy. After the literature review were carried out identification and measurements of stretch zones of proof bodies were made through confocal optical microscopy and then analyzed the results in order to find relationships between the values obtained with the theory

Correlações entre zona de estiramento e tenacidade à fratura para aço 15-5PH

This work includes a study on the stretch zone and the influence of the toughness conditions at fracture in size and appearance. It was done a literature review about material properties, fracture mechanics concepts, definitions and formation of stretch zone, importance of tenacity for structural calculation, methods and standards to measure the toughness of metallic material fracture and presents the method used in microscopy. After the literature review were carried out identification and measurements of stretch zones of proof bodies were made through confocal optical microscopy and then analyzed the results in order to find relationships between the values obtained with the theory

INFLUENCE OF HVOF COATING ON THE FATIGUE STRENGTH OF 15-5 PH STAINLESS STEEL

Structural component failures due to cyclic loading are associated to surface damage of materials and its interaction with environment. Fatigue failure occurs with stresses below the yield strength of each material and is a result of crack initiation and propagation. In aeronautical components is an important parameter to be considered in project, as well as the corrosion and wear resistance. Thermally sprayed HVOF coatings have been considered to replace galvanic chromium deposits with comparable performance for wear and corrosion resistance. The aim of present research is to study the influence of WC-13Co-4Cr applied by HVOF, on the axial fatigue strength of 15-5 PH stainless steel. The shot peening treatment was used to restore fatigue performance.

Fractografia quantitativa: relações entre tenacidade e o comportamento fractal em ligas metálicas

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Avaliação do comportamento de superfícies de fratura por fractais mistos em materiais de diferentes classes

Pós-graduação em Engenharia Mecânica - FEG

Comportamento fractal de superfícies de fadiga em ligas aeronaúticas

Fracture surfaces express sequences of events of energy release with crack propagation in metal alloys, the evolution of topographic features can indicate the lines of load action, failures during the use or processing. The quantitative fractography is an important tool in the study of fracture surfaces, because it allows their interpretation and characterization. In order to evaluate the effectiveness of the characterization of fracture surfaces grounded on concepts such as selfsimilarity and self-affinity, it used the 15-5PH steel that was characterized by metallographic and tensile tests. The metallography allows the microstructural characterization of this steel and proved the presence of the martensite phase in the slats form and a fine-grained, both in the radial and in the axial direction of the dowel. The tensile test (ASTM E8) of this material allowed the determination of the mechanical properties, so based on the obtained results it was possible to affirm that the 15-5PH steel has high mechanical properties and a good stretch. Besides, the specimens also underwent testing of crack propagation, standardized by ASTM E647-00, thus it was obtained the fracture surfaces for characterization under monofractal and multifractal approaches. In front of all the exposed it was possible to conclude that in all measurements the correlation between the crack tip position and the fractal dimension was established in accordance with changes in the thickness and in the fracture micromechanisms presents. Furthermore, the multifractal approach was more sensitive to these variations allowing a more detailed characterization of the morphology

Vibrational spectroscopy of phthalocyanine and naphthalocyanine in sandwich-type (na)phthalocyaninato and porphyrinato rare earth complexes: Part 14. The infrared and Raman characteristics of phthalocyanine in “pinwheel-like” homoleptic bis[1,8,15,22-tetrakis(3-pentyloxy)phthalocyaninato] rare earth(III) double-decker complexes

The infrared (IR) spectroscopic data and Raman spectroscopic properties for a series of 13 “pinwheel-like” homoleptic bis(phthalocyaninato) rare earth complexes M[Pc(α-OC5H11)4]2 [M = Y and Pr–Lu except Pm; H2Pc(α-OC5H11)4 = 1,8,15,22-tetrakis(3-pentyloxy)phthalocyanine] have been collected and comparatively studied. Both the IR and Raman spectra for M[Pc(α-OC5H11)4]2 are more complicated than those of homoleptic bis(phthalocyaninato) rare earth analogues, namely M(Pc)2 and M[Pc(OC8H17)8]2, but resemble (for IR) or are a bit more complicated (for Raman) than those of heteroleptic counterparts M(Pc)[Pc(α-OC5H11)4], revealing the decreased molecular symmetry of these double-decker compounds, namely S8. Except for the obvious splitting of the isoindole breathing band at 1110–1123 cm−1, the IR spectra of M[Pc(α-OC5H11)4]2 are quite similar to those of corresponding M(Pc)[Pc(α-OC5H11)4] and therefore are similarly assigned. With laser excitation at 633 nm, Raman bands derived from isoindole ring and aza stretchings in the range of 1300–1600 cm−1 are selectively intensified. The IR spectra reveal that the frequencies of pyrrole stretching and pyrrole stretching coupled with the symmetrical CH bending of –CH3 groups are sensitive to the rare earth ionic size, while the Raman technique shows that the bands due to the isoindole stretchings and the coupled pyrrole and aza stretchings are similarly affected. Nevertheless, the phthalocyanine monoanion radical Pc′− IR marker band of bis(phthalocyaninato) complexes involving the same rare earth ion is found to shift to lower energy in the order M(Pc)2 > M(Pc)[Pc(α-OC5H11)4] > M[Pc(α-OC5H11)4]2, revealing the weakened π–π interaction between the two phthalocyanine rings in the same order.

Vaughan, Suzi and Armstrong, Wendy (2009) Threads of tension. In: Vaughan, Suzi and Schmidt, Christine Margaret, (eds.) Five Fashion Musings. Post Pressed, Brisbane, Qld, pp. 9-15.

five:fashion musings is an upcoming 2009 publicaton to celebrate the fashion discipline's five-year milestone at the Queensland Unviesity of Technology. it represents a body of work by fashion practitioners, aceademic and educators commissioned to explore their research in fashion theory, practice and pedogogy through five key themes.