Formation of ultra-fine ferrite in hot rolled strip: potential mechanisms for grain refinement

A novel single-pass hot strip rolling process has been developed in which ultra-fine (<2 μm) ferrite grains form at the surface of hot rolled strip in two low carbon steels with average austenite grain sizes above 200 μm. Two experiments were performed on strip that had been re-heated to 1250°C for 300 s and air-cooled to the rolling temperatures. The first involved hot rolling a sample of 0.09 wt.%C–1.68Mn–0.22Si–0.27Mo steel (steel A) at 800°C, which was just above the Ar3 of this sample, while the second involved hot rolling a sample of 0.11C–1.68Mn–0.22Si steel (steel B) at 675°C, which is just below the Ar3 temperature of the sample. After air cooling, the surface regions of strip of both steel A and B consisted of ultra-fine ferrite grains which had formed within the large austenite grains, while the central regions consisted of a bainitic microstructure. In the case of steel B, a network of allotriomorphic ferrite delineated the prior-austenite grain boundaries throughout the strip cross-section. Based on results from optical microscopy and scanning/transmission electron microscopy, as well as bulk X-ray texture analysis and microtextural analysis using Electron Back-Scattered Diffraction (EBSD), it is shown that the ultra-fine ferrite most likely forms by a process of rapid intragranular nucleation during, or immediately after, deformation. This process of inducing intragranular nucleation of ferrite by deformation is referred to as strain-induced transformation.

Grain size in Mg alloys: recrystallization and mechanical consequences

The present paper examines the development of grain size during the recrystallization of magnesium alloys and the influence the grain size has on the mechanical response. In magnesium alloys grain refinement improves the strength-ductility balance. This simultaneous increase in both strength and ductility is ascribed to the impact the grain size has on deformation twinning. The mechanisms by which the grain size is established during hot working are shown to be conventional dynamic recrystallization followed by post-dynamic recrystallization. The role of alloying additionon both of these reactions is briefly considered.

Grain refinement through controlled thermomechanical processing

The major challenge for thermomechanical processing is to extend grain refinement towards lower average grain sizes. However, there is also a need to provide a better understanding of the mechanisms through which the refinement processes proceed. Many recent proposals for advanced thermomechanical processing rely on the dynamic strain induced transformation (DSIT), and the dynamic recrystallisation of austenite as the main refinement mechanisms. These mechanisms are still not fully understood and their clarification can be expected to lead to even greater levels of refinement. The current review examines the roles of ferrite recrystallisation , DSIT and initial austenite grain size. It is shown that although the ferrite recrystallisation mechanism in DSIT has certain similarities with the well known continuous dynamic recrystallisation (CDRX), it is significantly affected by the transformed ferrite grain size. Also, reducing the initial austenite grain size increases the recrystallisation rate in the strain dependent as well as strain independent regions. These results show that the traditional concept of metadynamic recrystallisation is insufficient to explain the changes in grain size following deformation. An alternative explanation is presented.

A rationale for the strong dependence of mechanical twinning on grain size

In metals that yield as a consequence of mechanical twinning, the yield stress is a function of the grain size in much the same way as it is for dislocation glide. However, the sensitivity to grain size is typically greater. The intent of the present communication is to show that this can be understood, at least in part, in terms of a size effect that accompanies twinning. Some confirmatory data from a magnesium alloy are presented.

Dependency of recrystallization mechanism to the initial grain size

The effect of initial grain size on the recrystallization behavior of a type 304 austenitic stainless steel during and following hot deformation was investigated using hot torsion. The refinement of the initial grain size to 8 μm, compared with an initial grain size of 35 μm, had considerable effects on the dynamic recrystallization (DRX) and post-DRX phenomena. For both DRX and post-DRX, microstructural investigations using electron backscattered diffraction confirmed an interesting transition from conventional (discontinuous) to continuous DRX with a decrease in the initial grain size. Also, there were unexpected effects of initial grain size on DRX and post-DRX grain sizes.

Effect of grain size on deformation twinning behaviour of high MN steel

The effect of grain size on the mechanical properties and deformation twinning behaviour in high manganese steel was investigated. In order to generate different grain sizes, the samples were subjected to hot rolling, cold rolling and annealing. Room temperature tensile testing of the steel with different grain sizes (5-50 µm) indicated the occurrence of twinning induced plasticity (TWIP) in all the samples. Also, changes in work-hardening behaviour accompanied changes in the grain size. The results are discussed in terms of the enhanced sensitivity of twinning to the grain size.

Study of the effect of grain size on the dynamic mechanical properties of microalloyed steels

In the present paper the effect of grain refinement on the dynamic response of ultra fine-grained (UFG) structures for C–Mn and HSLA steels is investigated. A physically based flow stress model (Khan-Huang-Liang, KHL) was used to predict the mechanical response of steel structures over a wide range of strain rates and grain sizes. However, the comparison was restricted to the bcc ferrite structures. In previous work [K. Muszka, P.D. Hodgson, J. Majta, A physical based modeling approach for the dynamic behavior of ultra fine-grained structures, J. Mater. Process. Technol. 177 (2006) 456–460] it was shown that the KHL model has better accuracy for structures with a higher level of refinement (below 1 μm) compared to other flow stress models (e.g. Zerrili-Armstrong model). In the present paper, simulation results using the KHL model were compared with experiments. To provide a wide range of the experimental data, a complex thermomechanical processing was applied. The mechanical behavior of the steels was examined utilizing quasi-static tension and dynamic compression tests. The application of the different deformation histories enabled to obtain complex microstructure evolution that was reflected in the level of ferrite refinement.

Effect of transformation mechanism (static or dynamic) on final ferrite grain size

A simple series of test was developed to highlight and compare the difference between the static strain induced transformation (SSIT) and the dynamic strain induced transformation (DSIT) mechanism in grain refinement and also to investigate the origin of the difference between the two mechanisms. The results showed that while the SSIT sets up a two-dimensional impingement among the ferrite grains, it cannot avoid their coarsening (normal growth). However, the DSIT forms a group of grains with a three-dimensional impingement which does not coarsen and maintains their fine size throughout the transformation, thereby, reduces the final average grain size.

Effect of grain size on the performance of extruded magnesium alloy tubes in three-point bending

The performance of extruded AZ31, AZ61 and AM-EX1 tubes was examined in three-point bending. Different extrusion temperatures were used to investigate the effect of grain size on the load-carrying capacity, energy absorption and fracture propensity of the tubes. Results showed that while the peak load increased with a smaller average recrystallised grain size, the retention of large elongated un-recrystallised grains in the microstructure reduced the load. The presence of the large elongated grains also appeared detrimental to the ability of the tube to deform before fracture.

Influence of grain size on twinning in two hcp metals

Deformation twinning behaviour in differently grain sized samples of a commercial pure titanium and a magenisum alloy is investigated. In some aspects the phenomenology of twinning differs between the two materials while in others both materials show a similar response. Nucleation density per unit of nucleating interface and twin aspect ratio scale with applied stress. The impact of grain size on twin volume fraction is modelled analytically.