倒装焊组装的光电混合集成RCE探测器面阵

报道了一种可用于并行光传输系统的64 * 64光探测器面阵。器件结构采用谐振腔增强型（RCE），吸收区由3层InGaAs/GaAs量子阱构成，谐振腔是由2组多层布拉格反射镜组成，工作波长位于980 nm。该器件利用倒装焊技术，将GaAs基的谐振腔增强型光探测器面阵与相应的Si基标准CMOS集成电路混合集成在一起，形成具备64 * 64路光并行接收及处理的大规模光电集成探测器面阵器件，并对光探测器面阵的主要特性进行了测试，测试结构显示该面阵具有均匀的电特性，反向偏压均大于14 V，暗电流约为10 nA数量级。

快速简便的青霉素效价测定法:Ⅱ.场效应管型青霉素传感器的测定方法和应用

于2010-11-23批量导入

整合素-ICAM-1相互作用的二维反应动力学研究

<正>_2整合素(LFA-1和Mac-1)与其配体细胞间粘附分子-1(ICAM-1)的相互作用在诸如肿瘤转移、炎症反应等许多病理生理过程中起着重要的作用。研究表明,中性粒细胞(PMN)在特定环境下可通过_2整合素与ICAM-1的相互作用而增强黑色素瘤细胞的转移能力,但是其动力学调控机制还不清楚。受体-配体键结合和解离的二维反应动力学定量描述了分子结合的快慢和强弱,是回答_2整合素与ICAM-1相互作用如何调

水蚀条件下不同土壤氮素和有机质流失规律

人工模拟放水冲刷试验研究结果表明 ,随放水冲刷强度的增大 ,不同土壤硝态氮、铵态氮、有机质和全氮流失加剧 ,泥沙全氮和有机质富集程度减少 ;当给不同土壤施等量的硝酸铵时 ,发现随径流流失化肥的铵态氮和硝态氮分别占施入量的 0 .9%～ 3 .5 %和 8.2 %～ 19.7% ,硝酸铵主要随径流流失 ,以泥沙颗粒流失量甚微 ;土壤侵蚀、有机质和全氮流失量与 >2 0 μm团聚体相关系数分别为 -0 .893 5、-0 .792 8和 -0 .815 1,2 0 μm直径的团聚体是区分土壤有机质和全氮流失的标准

21世纪中国经济发展面临的严峻挑战

一、面临的形势在人类文明的车轮辗过数千年后,现已跨入崭新的时代之际,人类的前景却越来越暗淡,环顾当今世界,人口爆炸、粮食紧缺、生态破坏、环境污染、经济危机等社会问题,一个又一个的危机,不仅使人类已有的文明成果黯然失色,而且使人类的未来也越来越充满艰险。英国著名的生态学家爱德华·戈德把全球的生态环境恶化喻为第三次世界大战。他说,由于这场大战,“大自然在崩溃,在衰亡,其速度之快,以致如果让这种趋势继续发展,自然界将很快失去供养人类生存的能力”。这似乎是危言耸听,但严峻的现实却必须引起人们的高度警惕。生态环境的严重破坏,无论是大气污染、温室效应、全球气候变暖和酸雨等,还是各类人为灾害均大大制约着经济的发展。所以人口———环境———经济如何协调发展,是一个全球性的重大课题。80年代以来,联合国许多国际组织,以及绝大多数国家和政府,对此有一种危机感、紧迫感,并做过许多研究和分析,制定相应的政策保护环境。联合国粮农组织将1989年世界粮食日主题定为“粮食与环境”;世界卫生组织将1990年世界卫生日主题定为“环境与健康”;联合国教科文组织将90年代列为“国际环境教育10年”,1992年6月在巴西召开的联合国环境与发展大会,...

浊点萃取-石墨炉原子吸收光谱法测定环境样品中的镉

建立了浊点萃取分离富集石墨炉原子吸收光谱法测定环境样品中痕量镉的方法。浊点萃取选择8-羟基喹啉为螯合剂,Triton X-100为表面活性剂。在pH8～9、0.01%8-羟基喹啉和0.2%-Triton X-100、80℃水浴20 min的优化条件下,所建立方法的检出限为2.5 ng/L;加标回收率为94.6%～106.2%;对样品溶液进行富集的富集因子为17。利用该方法分别测定了2个实际水样和2个国家标准参考物质中的总镉含量,结果令人满意。

Aptamer-based label-free method for hemin recognition and DNA assay by capillary electrophoresis with chemiluminescence detection

An aptamer-based label-free approach to hemin recognition and DNA assay using capillary electrophoresis with chemiluminescence detection is introduced here. Two guanine-rich DNA aptamers were used as the recognition element and target DNA, respectively. In the presence of potassium ions, the two aptamers folded into the G-quartet structures, binding hemin with high specificity and affinity. Based on the G-quartet-hemin interactions, the ligand molecule was specifically recognized with a K (d)approximate to 73 nM, and the target DNA could be detected at 0.1 mu M. In phosphate buffer of pH 11.0, hemin catalyzed the H2O2-mediated oxidation of luminol to generate strong chemiluminescence signal; thus the target molecule itself served as an indicator for the molecule-aptamer interaction, which made the labeling and/or modification of aptamers or target molecules unnecessary. This label-free method for molecular recognition and DNA detection is therefore simple, easy, and effective.

反相高效液相色谱表征无定型聚芳醚酮（砜）成环解聚产物

建立了一种反相高效液相色谱表征无定型聚芳醚酮（砜）成环解聚产物的新方法.采用岛津VP-ODS C18反相色谱柱（150 mm×4.6 mm; 5 μm, i.d.）,以四氢呋喃/水为流动相,流速1.0 mL/min, 梯度淋洗方式;254 nm紫外检测,由此方法可将全部同系物组分有效地分离并可准确给出产物中各环状低聚体组分的百分含量.分析结果表明,酚酞聚醚酮、酚酞聚醚砜、双酚A聚砜经成环解聚反应高产率得到环状聚合体,最高成环率达97.57%.通过与激光质谱的比较证实了HPLC方法更适合于对成环解聚产物体系的表征.

In situ electrochemical SERS studies on electrodeposition of aniline on 4-ATP/Au surface

The electrochemical polymerization of 0.01 M aniline in 1 M H2SO4 aqueous solution on roughened Au surface modified with a self-assembled monolayer (SAM) of 4-aminothiophenol (4-ATP) has been investigated by in situ electrochemical surface-enhanced Raman scattering spectroscopy (SERS). The repeat units and possible structures of the electrodeposited polyaniline (PANI) film were proposed; i.e., aniline monomer is coupled in head-to-tail predominately at the C-4 of aniline and amine of 4-ATP, and the thin PANI film is orientated vertically to substrate surface. Simultaneous Raman spectra during potential scanning indicate clearly that the ultrathin PANI film (in initial growth of the film) consists of semiquinone radical cation (IP+), para-disubstituted benzene (IP and IP+) and quinine diimine (NP) while it is oxidized, and without quinine diimine and semiquinone radical cation while reduced. Meanwhile, the results confirm that 4-ATP monolayer shows a strong promotion on the electrodeposition of aniline monomer, and a possible polymerization mechanism was proposed.

Synthesis, structure and reactive mechanism of intermetallic W3Mg

Assisted by mechanical alloying and high-pressure technique, a new W3Mg intermetallic was formed. W3Mg amorphous mixture was obtained by mechanically alloying the pure metal powder mixtures at designated composition for 20 h. A new compound was found after the Subsequent high pressure and high temperature treatment. W3Mg intermetallic was identified as a tetragonal structure and the lattice parameter was a = 0.7880 nm, c = 0.7070 nm. The synthesis mechanism is also discussed in this paper.

Synthesis of a new aryl ether ketone polymer

The synthesis of a new aryl ether ketone polymer with an advantageous ratio of glass transition temperature to melting temperature is reported.

The phase inversion and morphology of nylon 1010 polypropylene blends

Noncompatibilized and compatibilized blends of nylon 1010/PP blends having five different viscosity ratios were prepared by melt extrusion. Glycidyl methacrylate-grafted-polypropylene (PP-g-GMA) was used as the compatibilizer to enbance the adhesion between the two polymers and to stabilize the blend morphology. The effect of the viscosity ratio on the morphology of nylon 1010/polypropylene blends was investigated, with primary attention to the phase-inversion behavior and the average particle size of the dispersed phase. The relationship between the mechanical properties and the phase-inversion composition was investigated as well. Investigation of the morphology of the blends by microscopy indicated that the smaller the viscosity ratio (eta(PP)/eta(PA)) the smaller was the polypropylene concentration at which the phase inversion took place and polypropylene became the continuous phase. The compatibilizer induced a sharp reduction of particle size, but did not have a major effect on the phase-inversion point. An improvement :in the mechanical properties was found when nylon 1010 provided the matrix phase. (C) 1996 John Wiley & Sons, Inc.