964 resultados para solid-phase crystallization (SPC)
Resumo:
Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
Resumo:
Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
Resumo:
Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
Resumo:
Mixed calcium and copper oxalates, with different proportions of Ca2+ and Cu2+ ions, were precipitated by dimethyl oxalate hydrolysis in homogeneous solution. The compounds were evaluated by means of scanning electron microscopy, energy dispersive X-ray spectroscopy, thermogravimetry (TG), and differential thermal analysis (DTA). The results suggested quantitative precipitation without solid solution formation. From the TG and DTA curves, it was possible to evaluate the Ca2+ ion proportion in the solid phase and to confirm the precipitation of the individual species.