Segmented HPGe平面型位置灵敏探测器阵列的γ成像分析；Gamma-ray imaging analysis by using array of segmented planar HPGe detectors

探测器位置分辨能力的高低是实现γ成像的一个重要指标.Segmented HPGe平面型位置灵敏探测器能够很好地给出γ射线与探测器晶体相互作用的作用点位置信息.利用由这种探测器组成的探测器阵列对~(22)Na标准源进行了γ成像实验.结果能够区分出标准源两个不同的摆放位置的细微差别,并与实际情况符合得很好.从而检验了Segmented HPGe平面型位置灵敏探测器的位置分辨能力.

8×8单元CsI(Tl)探测阵列研制；Development of 88 CsI(Tl) array detector

描述了1个8×8单元CsI(Tl)探测阵列的结构和工作原理。探测阵列的每个单元是由1块前表面21 mm×21 mm、后表面23.1 mm×23.1 mm、高50 mm的CsI(Tl)棱台、1块光导和光电倍增管组成。在兰州放射性次级束流线(RIBLL)上对探测阵列进行测试,得到探测阵列对30 MeV质子的能量分辨可达2.7%,对170 MeV7Be可达1.5%,可很好地用于放射性束物理实验中带电粒子的鉴别。

A 3 Tesla Superconducting Magnet for Hall Sensor Calibration

A 3 T superconducting magnet with a 70 mm diameter warm bore and energy storage of 47 kJ has been successfully fabricated and tested, which can be used to calibrate Hall sensors in high magnetic field as well as conduct superconducting experiments. The magnet consists of three solenoid coils and an iron yoke. The homogeneity of the magnetic field in the region of interest (ROI) is +/- 6.0 x 10(-5). The coils of the magnet were fabricated with NbTi-Cu superconducting wire and the stray magnetic field is shielded by an iron yoke. The coils and yoke are fully immersed in a helium vessel. The optimized structural design, stress and quench simulation, fabrication and test results are presented in this paper.

Determination and identification of isoflavonoids in Radix astragali by matrix solid-phase dispersion extraction and high-performance liquid chromatography with photodiode array and mass spectrometric detection

The isoflavonoids in Radix astragali were determined and identified by HPLC-photodiode array detection-MS after extraction employing matrix solid-phase dispersion (MSPD). As a new sample preparation method for R. astragali, the MSPD procedure was optimized, validated and compared with conventional methods including ultrasonic and Soxhlet extraction. The amounts of two major components in this herb, formononetin (6) and ononin (2), were determined based on their authentic standards. Four major isoflavonoids, formononetin (6), ononin (2), calycosin (5) and its glycoside (1), and three minor isoflavonoids, (6aR,11aR)-3-hydroxy-9, 10-dimethoxypterocarpan (7), its glycoside (3), and (3R)-7,2'-dihydroxy-3',4'-dimethoxyisoflavone-7-O-beta-D-glycoside (4), were identified based on their characteristic two-band UV spectra and [M + H](+), [aglycone + H](+) and [A1 + H](+) ions, etc. The combined MSPD and HPLC-DAD-MS method was suitable for quantitative and qualitative determination of the isoflavonoids in R. astragali. (C) 2003 Elsevier B.V. All rights reserved.