Avaliação in vitro da resistência de união de dois sistemas adesivos dentinários à dentina bovina antes e após a termociclagem: teste de cisalhamento e análise estereomicroscópia

Pós-graduação em Odontologia Restauradora - ICT

Resistência ao cisalhamento de diferentes sistemas adesivos no esmalte dental

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Pré tratamento dentinário influência do condicionamento ácido, irradiação laser e hipermineralização na resistência ao cisalhamento de sistema adesivo multi uso

The disadvantages generated by the acid etching of the dentin, such as an increase in its permeability, in the surface moisture and in the potential to denature the external dentinal collagen, the formation of a fragility zone and the citotoxicity of the adhesive monomers; which are all aggravated by the depth of the dentin, have stimulated new and different treatment philosophies of the dentin. The purpose of the present study, therefore, was to investigate the effects of three dentin treatments: laser irradiation, acid etching and hypermineralization, in the shear bond strength of the SMP Plus bonding system. Sixty bovine incisors were extracted and randomly selected immediatly alter the animal's death. They were kept frozen (-18°C) for no longer than 14 days. After buccal dentinal surface had been exposed, X-Rays were taken to control the dentin thickness. The specimens were separated into two groups: (1) Control, kept in distilled water at 4ºC; (2) Mineralized, kept in hypermineralized solution at 4°C for 14 days. Each group was divided into three sub-groups according to the type of dentin treatment used: group F - followed the manufacturer instructions (acid-etching + primer + bond), group AL (acid-etching + primer + bond + laser) and group LA (laser + (laser + acid-etching + primer + bond). A composite resin standard cylinder (Z100-3M) was bond to the dentinal surface and the shear bond strength performed on a Universal lnstron machine 4301, with 500 Kg load and at 0,5mm/min. speed. The analysis of variance (ANOVA) determined that the treatments influenced the shear bond strength values (p<0,05) with the following average shearing load at failure: AL (9,96 MPa), F (7,28MPa) e LA (4,87 MPa). The interaction between the two factors analyzed Group (control and mineralized) and treatment (F, AL, LA) also influenced the shear bond strength (p<0,05). The highest values were obtained...

Força muscular e massa corpórea de ratos Wistar

The use of rats in studies that seek to monitor the effects of physical exercise is fairly common, even in works that make use of overload. However, the correct determination of the training load is critical to success of studies. Thus, with the objective of verifying the correlation of total body mass of the rats with their respective strength, and the correlation of the 1RM test with test repetitions, 40 rats, 90 days old and weighing average 0,49 pounds underwent a program of adaptation to the water and then were subjected to tests to determine the maximal and submaximal loads. After measuring the total body mass and maximal and submaximal strenght, it was possible to observe directly proportional relationship between maximum strenght and total body mass of 0.97 (P ≤ 0.01), being the maximum muscle strength equivalent to 109% of the total body mass. Between muscle strength and mass submaximal muscle strength was also found direct correlation between the variables, allowing to conclude that the submaximal strength test and total body mass are effective tools in determining the training load of rats.

Desenvolvimento de procedimentos e métodos analíticos no campo forense aplicando os princípios da química verde

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Efeito da radiação ionizante, simulando radioterapia, nas propriedades de cerâmicas Y-TZP e cimentos resinosos

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Efeito de diversos protocolos de dessensibilização dentinária na obliteração de túbulos dentinários, resistência de união do sistema adesivo e formação de camada hibrida na dentina cervical

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Caracterização da liga Ti-15Zr visando aplicações biomédicas

With advances in health care, has been na increase of demand for material that could replace the functions of the human body parts, thus evolved biomedic prosthesis which today are responsible for the constant improvement of the quality of life. The Titanium alloys are widely used as implants due to its properties, like high mechanical resistance, biocompatibility and corrosion resistance, and the addition alloying elements like Zirconium, may improve some of those properties. Such properties are related to the microstructure and consequently to the type of processing performed. The purpose of this dissertation was to characterize the experimental alloy Ti15Zr after route of processsing and heat treatment in order to extend the knowledge about this alloy. The latter has been abtained by fusion of pure metals in a arc melting furnace with an inert argon atmosphere. The material has been homogenized in a tube furnace at 950ºC for 24h and cold worked by swaging, after that, bars with 10 mm of diameter were obtained by the process of rotary forging. The samples were solubilized at 900º C for 2 hours and quenched in water. After that, 4 samples were submitted to the aging, at 400º C, 450º C, 500º C and 550º C. The microstructure and phase analysis was done by optical microscopy and X-rays diffraction (XRD), the mechanical characterization was carried out by microhardness test and finally, evaluation of corrosion resistance of the alloy by electrochemical tests. The XRD and the optical microscopy made it possible to analyze that the heat treatment influenced the phase shifting from α to α', and probably affected the alloy hardness, at the first aged sample at 500º Chas been a sudden increase in the value of hardness, probably by appearance of omega phase, unwanted phase to the medical application duo to great fragility, and finally ... (Complete abstract click electronic access below)

Análise microestrutural e caracterização mecânica do aço AISI 4350 submetido a diferentes tratamentos térmicos

The multiphase steels are gaining increasing attention in scientific studies because of the different mechanical and microstructural properties that the material can achieve under different thermomechanical and heat treatments that can be submitted. In the present study, it was made a microstructural study thru the triple attack technic associated with optical microscopy and mechanical characterization of medium carbon AISI 4350 steel thru a tensile strength test, subjected to three routes of heat treatment: annealing, quenching and tempering and isothermal annealing. It was verified the predominance of ferrite-perlite constituent in the specimen annealed, martensitic in the quenched and tempered specimen and bainitic in the annealed isothermally specimen. The annealed material showed a higher ductility, while the hardened and tempered specimen showed the highest hardness and ultimately the bainitic specimen showed a combination of the two abovementioned mechanical properties. Thus, we proved that the multiphase steel SAE 4350 can be a versatile material with great potential for various industrial applications

O efeito da contração muscular de membros superiores sobre o sistema nervoso autonômico de pessoas com fatores de risco cardiovascular

Pós-graduação em Desenvolvimento Humano e Tecnologias - IBRC

Efeito de diversos protocolos de dessensibilização dentinária na obliteração de túbulos dentinários, resistência de união do sistema adesivo e formação de camada hibrida na dentina cervical

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Caracterização da liga Ti-15Zr visando aplicações biomédicas

With advances in health care, has been na increase of demand for material that could replace the functions of the human body parts, thus evolved biomedic prosthesis which today are responsible for the constant improvement of the quality of life. The Titanium alloys are widely used as implants due to its properties, like high mechanical resistance, biocompatibility and corrosion resistance, and the addition alloying elements like Zirconium, may improve some of those properties. Such properties are related to the microstructure and consequently to the type of processing performed. The purpose of this dissertation was to characterize the experimental alloy Ti15Zr after route of processsing and heat treatment in order to extend the knowledge about this alloy. The latter has been abtained by fusion of pure metals in a arc melting furnace with an inert argon atmosphere. The material has been homogenized in a tube furnace at 950ºC for 24h and cold worked by swaging, after that, bars with 10 mm of diameter were obtained by the process of rotary forging. The samples were solubilized at 900º C for 2 hours and quenched in water. After that, 4 samples were submitted to the aging, at 400º C, 450º C, 500º C and 550º C. The microstructure and phase analysis was done by optical microscopy and X-rays diffraction (XRD), the mechanical characterization was carried out by microhardness test and finally, evaluation of corrosion resistance of the alloy by electrochemical tests. The XRD and the optical microscopy made it possible to analyze that the heat treatment influenced the phase shifting from α to α', and probably affected the alloy hardness, at the first aged sample at 500º Chas been a sudden increase in the value of hardness, probably by appearance of omega phase, unwanted phase to the medical application duo to great fragility, and finally ... (Complete abstract click electronic access below)

Análise microestrutural e caracterização mecânica do aço AISI 4350 submetido a diferentes tratamentos térmicos

The multiphase steels are gaining increasing attention in scientific studies because of the different mechanical and microstructural properties that the material can achieve under different thermomechanical and heat treatments that can be submitted. In the present study, it was made a microstructural study thru the triple attack technic associated with optical microscopy and mechanical characterization of medium carbon AISI 4350 steel thru a tensile strength test, subjected to three routes of heat treatment: annealing, quenching and tempering and isothermal annealing. It was verified the predominance of ferrite-perlite constituent in the specimen annealed, martensitic in the quenched and tempered specimen and bainitic in the annealed isothermally specimen. The annealed material showed a higher ductility, while the hardened and tempered specimen showed the highest hardness and ultimately the bainitic specimen showed a combination of the two abovementioned mechanical properties. Thus, we proved that the multiphase steel SAE 4350 can be a versatile material with great potential for various industrial applications