Effect of ceramic etching protocols on resin bond strength to a feldspar ceramic

This study sought to evaluate the resin micro-tensile bond strength (MTBS) stability of a leucite-reinforced ceramic after different ceramic etching protocols. The microtensile test had 40 ceramic blocks (5x5x6 mm) assigned to five groups (n=8), in accordance with the following surface etching protocols: NE nonetched (control); 9HF: hydrofluoric (HF) acid etching (9% HF)+wash/dry; 4HF: 4%HF+wash/dry; 5HF: 5%HF+wash/dry; and 5HF+N: 5%HF+neutralizer+wash/dry+ultrasonic-cleaning. Etched ceramic surfaces were treated with a silane agent. Next, resin cement blocks were built on the prepared ceramic surface and stored for 24 hours in distilled water at 37 degrees C. The specimens were then sectioned to obtain microtensile beams (32/block), which were randomly assigned to the following conditions, nonaged (immediate test) and aged (water storage for 150 days plus 12,000 thermal cycles), before the microtensile test. Bond strength data were submitted to one-way analysis of variance and Tukey test (alpha=0.05). Additional ceramic samples were subjected to the different ceramic etching protocols and evaluated using a scanning electron microscope (n=2) and atomic force microscopy (n=2). Aging led to a statistically significant decrease in the MTBS for all groups, except the untreated one (NE). Among the groups submitted to the same aging conditions, the untreated (NE) revealed inferior MTBS values compared to the 9HF and 4HF groups. The 5HF and 5HF+N groups had intermediate mean values, being statistically similar to the higher values presented by the 9HF and 4HF groups and to the lower value associated with the NE group. The neutralization procedure did not enhance the ceramic/resin cement bond strength. HF acid etching is a crucial step in resin/ceramic bonding.

The effects of heat-moisture treatment on avocado starch granules: thermoanalytical and structural analysis

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Aspectos físicos e fisiológicos de sementes de Fimbristylis dicothoma relacionados à germinação e dormência

In the seeds of pioneer plants, the application of treatments for breaking dormancy, and selection by colour and size, are strategies for obtaining seeds of less dormancy and better germination performance. The aim of this study was to evaluate the effect of the physical and physiological aspects of seeds of the tall fringe-rush (Fimbristylis dichotoma) on germination and dormancy. To do this, the seeds were submitted to the following treatments in three studies: (i) control, immersion in H2SO4 (98%, 36N) for 1 minute, immersion in KNO3 (1, 2 and 3%) for 15 minutes, seeding on a substrate moistened with KNO3 (0.2%) and exposure for 5 and 10 hours in a forced air circulation oven at 40 and 70 degrees C; (ii) classification of the seeds by colour (light and dark) and application of the following treatments: control, immersion of the seeds in H2SO4 (98%, 36N) for 1 and 2 minutes, immersion in KNO3 (5% and 10%) for 15 and 30 minutes and seeding on a substrate moistened with KNO3 (0.2%); (iii) classification by size (0.60, 0.50 and 0.40 mm) and germination on a substrate moistened with KNO3 (0.2%) or distilled H2O. The seeds were evaluated by germination test, first count and germination speed index. Moistening the substrate with KNO3 (0.2%), and heat treatment at 40 degrees C for 10 hours improve performance in seeds of the tall fringe-rush. Light-coloured seeds do not display dormancy. Medium-sized seeds of the tall fringe-rush show better performance in terms of percentage and speed of germination.

Analysis of the effect of wash water reduction on bleached pulp characteristics

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Study on determination and removal of metallic ions from aqueous and alcoholic solutions using a new POSS adsorbent

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Influence of different toothpaste abrasives on the bristle end-rounding quality of toothbrushes

ObjectivesTo evaluate the influence of different toothpaste abrasives on the bristle wear and bristle tip morphology of toothbrushes with different degrees of hardness.Material and methodsNinety samples of bovine incisor teeth were used in this study. The samples were randomly divided into three groups according to the bristle hardness of the toothbrush used: soft bristles (S); extra-soft bristles (ES); hard bristles (H). The toothbrushes of each group were randomly divided into six subgroups with five toothbrushes each, according to the abrasive of the toothpaste used in the simulation: Negative control (distilled water); toothpaste 1 (silica); toothpaste 2 (hydrated silica); toothpaste 3 (calcium carbonate, calcium bicarbonate and silica); toothpaste 4 (tetrapotassium pyrophosphate, silica and titanium dioxide); toothpaste 5 (calcium carbonate). The samples were placed in a toothbrushing simulating machine that simulating three months of brushing. The toothbrush bristles were evaluated by the bristle wear index, and the bristle tips morphology was evaluated by the bristle tip morphology index.ResultsThe ES brush presented the highest bristle wear among the toothbrushes. Additionally, the S brushes showed better morphology of the bristles followed by ES and H brushes. The type of abrasive only influenced the bristle tip morphology of the ES brushes. The toothpaste 3 induced the worse bristle tip morphology than all the other toothpastes.ConclusionsDifferent abrasives have influence only on the bristle tip morphology of the ES brushes.

Characterization of calcium phosphate coating produced by biomimetic method

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Gallus gallus domesticus are resistant to infection with Neospora caninum tachyzoites of the NC-1 strain

The aim of this study was to experimentally evaluate infection in Gallus gallus domesticus with Neospora caninum tachyzoites of the NC-1 strain. Experimental infection was conducted in 90-day-old chickens, embryonated eggs and bioassays in dogs. In the first experiment, poults were randomly divided into four groups. Groups I and II were provided feed with coccidiostat, whereas groups III and IV received feed without coccidiostat. When the poults from groups I and III reached 90 days of age, they received a subcutaneous inoculation of N. caninum. Once the hens entered their egg-laying period, during the following 30 days, the eggs were collected, identified, weighed and placed in an incubator. On the 70th day after inoculation, all animals, including the chicks, were euthanized. Tissue samples from the adult poultry and chicks were collected for histopathology, immunohistochemistry (IHC) and PCR. Brain tissue and pectoral muscle samples from infected birds were fed to two dogs. Notably, the average weight of the group III eggs was lower than that of the group IV eggs (p <0.05). No changes consistent with infection in adult poultry or chicks were detected by histopathology or IHC; moreover, no amplified parasite DNA was detected in the birds'tissues or dogs'feces. No dog eliminated oocysts. In the second experiment, the embryonated chicken eggs were inoculated with 1 x 10(2) N. caninum tachyzoites, on the 10th day of incubation, and chicks born from these eggs were housed in boxes suitable for the species and received commercial feed and distilled water ad libitum. On the 30th day after infection (DAI), the poultry were euthanized, and their organs were processed as described in experiment I. The amplification of parasite DNA was observed in the spleen and pectoral muscles of one of the birds. The ingestion of bird tissues by dogs did not result in oocyst elimination. These results indicate that the parasite may have been eliminated by the host and that the use of tachyzoites to induce chronic disease might be a poor source for hens. (C) 2014 Elsevier B.V. All rights reserved.

Thin films produced on 5052 aluminum alloy by plasma electrolytic oxydation with red mud-containing electrolytes

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Avaliação de pontas de jato plano na deposição da calda de pulverização com diferentes combinações de plantas de feijão, Brachiaria plantaginea e Bidens pilosa

Objetivou-se com este trabalho avaliar a ponta XR na deposição da calda de pulverização com diferentes combinações de plantas de feijão, Brachiaria plantaginea e Bidens pilosa, em dois volumes de aplicação, com e sem a adição de surfatante Silwet. Foi utilizado como traçador o corante Azul Brilhante FDC -1 na concentração de 500 ppm para quantificar a deposição. Os tratamentos constituíram-se de sete combinações de plantas: (feijão), (B. plantaginea), (B. pilosa), (feijão + B. plantaginea), (feijão + B. pilosa), (B. plantaginea + B. pilosa) e (feijão + B. plantaginea + B. pilosa). O delineamento experimental foi o inteiramente casualizado. Foram avaliadas as pontas de jato plano XR 110015 VS e XR 11002 VS com volumes de aplicação de 150 e 200 L ha-1, respectivamente, com e sem a presença do Silwet a 0,05% v v-1. Após a aplicação, as plantas foram imediatamente coletadas e, em seguida, lavadas em 100 mL de água destilada, para posterior quantificação do traçador em espectrofotômetro. As pontas XR apresentaram comportamento distinto na deposição das gotas de pulverização nas espécies estudadas; a adição de um surfatante à calda de pulverização aumentou a uniformidade da deposição nos alvos e contribuiu para a redução do volume de aplicação.

Influence of storage times on bond strength of resin cements to root canal

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Influência do agente de união na resistência ao cisalhamento da interface titânio/polímero de vidro

There is little information regarding bond strengths of polyglass to metal alloys. This study evaluated the influence of bonding system on shear bond strength of a composite resin (Artglass/Heraeus Kulzer) to cast titanium (Ti). Twenty metallic structures (4mm in diameter, 5mm thick) of titanium grade I were cast shaped and abraded with 250mm aluminum oxide and separated into two groups. For each group was applied one bonding system (Siloc or Retention Flow) before opaque and dentin polymer superposition. This procedure was managed using teflon matrices. They were manipulated and polymerized according to the manufacturer's recommendations. The samples were stored in distilled water for 24 hours at 37º and thermocycled (5º and 55ºC/500 cycles). Shear bond strength tests were performed by using an Instron Universal testing machine at a crosshead speed of 5mm/min. Results were analyzed statistically with one-way ANOVA (a=0,5) and they indicated that the Retention Flow system was statistically better than Siloc (20.74 MPa and 11.65 MPa , respectively). It was possible to conclude that the bonding agent influenced the adhesion between polymer and cast titanium.

Study of thermocycling effect on the bond strength between an aluminous ceramic and a resin cement

This study evaluated the effect of thermocycling on the bond strength between Procera AllCeram (Nobel-Biocare) and a resin cement (Panavia F, Kuraray CO). Nine ceramic blocks with dimensions of 5x6x6mm were conditioned at one face with Rocatec System (Espe). After, they were luted with Panavia F to composite resin blocks (Clearfil AP-X, Kuraray CO). The nine groups formed by ceramic, cement and composite resin were split up obtaining 75 samples with dimensions of 12x1x1mm and adhesive surface presenting 1mm2±0.1mm2 of area. The samples were divided into 3 groups (n=25): G1 - 14 days in distilled water at 37ºC; G2 – 6,000 cycles in water (5ºC - 55ºC – 30s); G3 – 12,000 cycles in water (5ºC - 55ºC – 30s). The samples were tested in a universal testing machine (EMIC) at a crosshead speed of 1mm/min. Data were analyzed by ANOVA and Tukey tests. The results indicated that mean values of rupture tension (MPa) of G1 (10.71 ± 3.54) did not differ statistically (p <5%) from G2 (9.01 ± 3.90), however there was statistical difference between G1 and G3 (7.28 ± 3.00). It was concluded that thermocycling significantly reduced the bond strength values when samples were submitted to 12,000 cycles.

Effect of whitening and desensitizing dentifrices on composite surfaces treated with surface sealants

This study evaluated the effect of different dentifrices on the microhardness and surface roughness of composite surfaces covered by surface sealants. Samples of Filtek P60 were made and divided into groups, in accordance with surface treatments: G1 - Fortify; G2 - Fortify Plus; G3 - control (none). For Knoop microhardness evaluation, the specimens were placed in a microdurometer, under a load of 50 g for 15 sec. The analyses of surface roughness were carried out individually in a profilometer. The specimens were submitted to toothbrushing using dentifrices: Colgate Maximum Protection Anti-caries, Colgate Whitening or Sensodyne, diluted in distilled water (1:3) for 30 000 cycles. The results showed that the control group (G3) presented the highest microhardness values. The control group presented, before toothbrushing, the lowest surface roughness values, and after toothbrushing there were no differences among the experimental groups. The maintenance of the lowest values of microhardness demonstrated the effectiveness of these sealant materials to support the abrasive wear.

Abrasion resistance of direct and indirect resins as a function of a sealant veneer

Abrasive wear is one of the most common type of wear that not only affect teeth, as also dental restorations. Thus to investigate one of the etiological factors as tooth brushing procedure is clinical relevant in order to select the best material combination that may prevent damage of resin dental restoration's abrasion. This study evaluated the influence of tooth brushing on mass loss and surface roughness of direct Venus (Vs) and indirect Signum (Sg) resin composites, with and without a surface sealant, Fortify (F). Twenty-four specimens were prepared with each resin composite, using their proprietary curing units, according to manufacturer's instructions. All the specimens were polished and ultrasonically cleaned in distilled water for 5 minutes. Half of the specimens of each resin (n = 12) were covered with F (Vs F and Sg F ), except for the control (C) specimens (Vs C and Sg C ), which were not sealed. Mass loss (ML) as well as surface roughness (Ra ) was measured for all the specimens. Then, the specimens were subjected to toothbrush-dentifrice abrasion, using a testing machine for 67.000 brushing strokes, in an abrasive slurry. After brushing simulation, the specimens were removed from the holder, rinsed thoroughly and blot dried with soft absorbent paper. The abrasion of the material was quantitatively determined with final measurements of ML and surface roughness, using the method described above. ML data were analyzed by two-way analysis of variance (ANOVA) and the analysis indicated that resin composites were not statistically different; however, the specimens sealed with F showed higher ML. Ra mean values of the groups Vs F and Sg F significantly increased. Tooth brushing affects mainly the roughness of the direct and indirect resin composites veneered with a sealant.