Estudo da variação do limite de resistência à tração ao longo da bobina de vergalhão de alumínio 1350 AA

Therebar of aluminum 1350 AA produced by CBA are used inthe manufacture of wires and cables for electric power transmission, which marketshows increasingly favorableto aluminum due to itslow densityand high electrical conductivity, but to ensure that this materialmeets all specifications of projectsfor electricity transmission, it must have homogeneity in the chemicaland mechanicalproperties.One of the points of improvement in the process of rod production isreducing the high variation of the limitof tensile strengthalong the coils, therefore, this work seeks a better understanding of the factors that significantly influence the mechanical properties of rebar, specifically assessing the influence oftemperatureat the output of the coils, which can cause a recovery effect on the material andif thereare relevantdifferences between the two modes of rebar production: auto and manual.Samples of six coils have been specifically produced forthis study, which weresubsequently subjected to different annealing temperatures for one hour and ten minutes, similar to what occurs in the output of the coil from the machine. The tensile tests showed that aluminum 1350 AA is significantly influenced by temperature, whose behavior was very similar to that presented in the literature. It was found that the phenomenon of recovery occurred more significantly at high temperatures. Through the optical electron microscope Zeiss, 18 surface maps were made with 100x magnification for each sample in different conditions and the images were analyzed using entropy and fractal dimension, aiming to relate the condition of surface hardening on mechanical property of the samples in that condition. The results showed that these methods can be applied, provided they do not have any kind of imperfection on the surface, once they can influence the results. The study concluded that a more efficient cooling is required in ... (Complete abstract click electronic access below)

Avaliação dos danos por fluência da serpentina da caldeira da REVAP

The determination of the remaining life of equipment operating at high temperatures has been a great challenge for their owners. The use of safety factors, often conservative, makes the replacement of equipment or of its components at the end of the life of design gets financially unviable. This study aimed to estimate the remaining life of the serpentine of the secondary superheater of one of REVAP’s boilers (Henrique Lage Refinery), through accelerated creep tests and comparison of the results with the techniques based on microstructure and hardness. When conducting a proper assessment it’s possible to increase the equipment reliability, ensuring operational continuity and physical integrity. The tests showed a minimal residual life of 12.7 years (111,252 hours), longer than the design life (100,000 hours), even after a period of operation of approximately 250,000 hours, confirming the conservatism of the project. The techniques based on microstructure and hardness did not show good correlation with the creep test, decreasing the reliability of these techniques in determining the residual life

Espectrometria de massa para análise isotópica dos bio-elementos

Mass spectrometry is an analytical technique widely used in several areas of academic research. It allows the knowledge of the information about the micro-world of atoms leading to significant advances in science today. The analysis of stable isotopes of carbon, hydrogen, oxygen, nitrogen and sulfur, also known as bio-elements, shows itself as a major area of interest in using the proposed method. The development of techniques and equipment coupled with mass spectrometry promises to deliver even greater progress in this field, in particular, for the biological sciences and related areas. The pyrolytic method in reduction of organic compounds at high temperatures provides simultaneous isotopic analysis of bio-elements H and O, by the gases released, H2 and CO after the pyrolitic process, significantly reducing analysis time and the amount of material to sample. This paper presents a review of mass spectrometry with its basic principles of operation, and pyrolytic method for reducing compounds at temperatures above 1400 ° C for isotopic analysis of bio-elements

Melhoria da qualidade de um processo de usinagem utilizando as técnicas de avaliação de Taguchi

Delivering to the customers a product or service with the expected quality associated to the huge competitiveness that exists in the market nowadays, has been making organizations increasingly focus on quality planning using techniques which are directed towards the continuous improvement process and production optimization. Thus, this paper aims to improve a machining process using the techniques of experimental design to the optimization and this also includes the analysis of the measurement system. For this purpose, the alloy Nimonic 80A, a nickel base superalloy, was used in the process due to its widespread use for high temperatures, applying this study the robust method proposed by Genichi Taguchi, determining the influence of the factors considered input variables, cutting speed, feed rate, depth of cut, type of tool, lubrication, and material hardness, in the output or response variable, surface roughness, concluding with the use of Taguchi orthogonal array L16 and by analysis of ANOVA that the factor feed rate is significant and offers greater effect on the response variable studied, should be set to 0,12mm/rev. Moreover, the factor type of tool has more influence on the process when compared to other factors, being CP250 the one more suitable to the process. Lastly, the interaction feed rate x cutting speed provides greater significance in the process regarding to surface roughness variable, being the best match between them 0,12mm/rev to the feed rate and 90m/min to the cutting speed. In order to evaluate the measurement system, it was applied the repeatability and reproducibility method (R&R), through which we saw that the system needs improvement (R & R = 88.04% >>> 30%) as the value found in the study was well above compared to the one that classifies the system as inappropriate

Otimização do processo de usinagem da superliga nimonic 80A utilizando o Método de Taguchi

Atualmente, atender as necessidades dos consumidores é uma das metas mais importantes, os consumidores estão em busca de produtos com qualidade e preços mais acessíveis, para isso, é indispensável que as empresas se atualizem para melhorar seus produtos e serviços. Com este cenário, as superligas estão cada vez mais ganhando mercado, pois possuem ótimas propriedades, principalmente em relação a operar em temperaturas elevadas, podendo proporcionar maior eficiência para motores que necessitam trabalhar em altas temperaturas. Em contra partida a essa vantagem, as superligas possuem uma baixa usinabilidade, sendo importante a análise do processo de usinagem para se tornarem mais aplicáveis. Este trabalho visa à otimização do processo de torneamento cilíndrico da superliga Nimonic 80A, com o intuito de melhorar a qualidade do produto, utilizando o Método de Taguchi, com o arranjo ortogonal L16, sendo o comprimento de corte definido como variável resposta e analisados seis fatores que poderiam influenciar na sua variação, tais fatores são: velocidade de corte, avanço, profundidade de corte, tipo de pastilha, lubrificação e dureza do material. Os resultados obtidos demonstraram que os fatores avanço, tipo de pastilha e lubrificação são significativos e exercem influencia no processo, sendo que o avanço deve ser ajustado no nível de 0,12 mm/rev, a pastilha a ser utilizada deve ser CP250 e a lubrificação deve ser feita de maneira abundante, para a otimização do processo. Com a análise dos resultados, também podemos observar a eficiência e confiabilidade do método utilizado, mostrando resultados coerentes

Leuconostoc mesenteroides SJRP55 isolada de mussarela de búfala: perfil probiótico e bacteriocinogênico

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Análise do comportamento do desgaste de dressadores de ponta única confeccionados com diamantes naturais e sintético piramidais

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Invertase from a Candida stellata strain isolated from grape: production and physico-chemical characterization

Invertases are enzymes which hydrolyze the sucrose and are widely employed in food and pharmaceutical industries. In this work, the screening of autochthonous grape yeasts from Brazil was carried out in order to investigate their invertase production potential. Yeasts belonging to Saccharomyces, Hanseniaspora, Sporidiobolus, Issatchenkia, Candida, Cryptococcus and Pichia genera were analyzed by submerged fermentation (SbmF) using sucrose as substrate. Among them, Candida stellata strain (N5 strain) was selected as the best producer (10.6 U/ml after 48 hours of SbmF). This invertase showed optimal activity at pH 3.0 and 55°C, demonstrating appropriate characters for application in several industrial processes, which includes high temperatures and acid pHs. In addition, this invertase extract presented tolerance to low concentrations of ethanol, suggesting that it could also be suitable for application at the beginning of alcoholic fermentation. These data provide promising prospects of the use of this new invertase in food and ethanol industry.

Avaliação da qualidade de óleos de fritura utilizados em restaurante universitário

Frying is a widely used method of preparing food, because it is a very fast and convenient process, and because it provides specific characteristics of color, flavor, odor, and texture, besides having great consumer acceptance. Therefore, the interest in the physiological effects that oils heated at high temperatures can cause to the human body arises. The aim of this work was to analyze the levels of frying used oil alteration in different kinds of foods served at the university restaurant at “Instituto de Biociências, Letras e Ciências Exatas” (IBILCE), in São José do Rio Preto-SP. In addition, it aims to make the restaurant aware of the good ways to fry and the commitment of providing good quality food to students and professionals of the Institute. With this purpose, determination of total polar compounds, conjugated dienoic acids, peroxide value, and fatty acid profile were analyzed. Two rapid tests were also used: 3M Fat Monitor and Oil Test kit. The results were compared with limits recommended for the disposal of oils and fats used in frying by the Brazilian Health Surveillance Agency (ANVISA), by other countries, and by other researches. Thus, it was concluded that the university restaurant provides the consumers with fried food of good quality, since none of the analyses showed results above recommended, although there is a need of improvement in the quality control of the oil used, in order to avoid unnecessary costs to the university restaurant.

Leuconostoc mesenteroides SJRP55: a bacteriocinogenic strain isolated from Brazilian water buffalo mozzarella cheese

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Caracterização do fator de intensidade de tensão em corpos trincados através do método dos elementos finitos

The industry generally has sought materials with high mechanical resistance, low density, thermal stability and corrosion resistance. In the aerospace industry, for example, the use of aluminum alloys, such as Al 2024-T351 and Al 7075-T7351, have become essential. However, the use of these materials often do not resulted in a satisfactory performance of the component, since the presence of cracks can cause total rupture of the component, even with a tension below the yield stress of the material, unexpectedly. In this work, these aluminum alloys were analyzed and samples were modeled by the finite element method. Moreover, in the models were applied two different types of cracks, central and edge crack, a vertical force was applied to result in a tension 70% of the yield stress of the material analyzed. Through stress asymptotic distribution in the region near the crack tip were calculated the values of the stress intensity factors for each crack length, after the stress intensity factors characterized were compared graphically with the values of fracture toughness found in the available literature

Vinhaça da indústria sucroalcooleira como matéria-prima a carbonização hidrotérmica

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Utilização de metaheurísticas combinada a diferentes métodos de aglutinação para a otimização de um processo de torneamento com múltiplas respostas

Pós-graduação em Engenharia Mecânica - FEG

Burning Graphene Layer-by-Layer

Graphene, in single layer or multi-layer forms, holds great promise for future electronics and high-temperature applications. Resistance to oxidation, an important property for high-temperature applications, has not yet been extensively investigated. Controlled thinning of multi-layer graphene (MLG), e.g., by plasma or laser processing is another challenge, since the existing methods produce non-uniform thinning or introduce undesirable defects in the basal plane. We report here that heating to extremely high temperatures (exceeding 2000 K) and controllable layer-by-layer burning (thinning) can be achieved by low-power laser processing of suspended high-quality MLG in air in "cold-wall" reactor configuration. In contrast, localized laser heating of supported samples results in non-uniform graphene burning at much higher rates. Fully atomistic molecular dynamics simulations were also performed to reveal details of oxidation mechanisms leading to uniform layer-by-layer graphene gasification. The extraordinary resistance of MLG to oxidation paves the way to novel high-temperature applications as continuum light source or scaffolding material.

Hopping-tunneling model to describe electric charge injection at metal/organic semiconductor heterojunctions

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)