Estudo para determinação de uma metodologia para o ensaio de arrancamento que avalia aderência aço/concreto

This work talks about the importance of the steel adhesion to concrete, reinforced concrete structures, their testing and forms of measurement used and how the results are used in the structural design, which uses as a reference the NBR 6118 and NBR 7480. It also deals with the importance of a reliable assessment, discussing failures that the test used, NBR 7477, features in specific circumstances, as discussed under the EC-094. It also presents an initial proposal for simplified pullout test, which aims to analyze the grip on steel bars with diameter less than 10 mm, which results when used standardized testing by ABNT NBT 7477, has shown excessive variability, the main criticism of the trial today used without distinction to be established thick or thin bars. The proposal also presented methodology is in the consolidation phase, given the time and the volume of necessary tests. For this reason it is not possible to make a comparison between the values obtained and the results of the test used on the basis of the standard in force, this can only be done once the front with a continuation of this work

Caracterização da liga Ti-15Zr visando aplicações biomédicas

With advances in health care, has been na increase of demand for material that could replace the functions of the human body parts, thus evolved biomedic prosthesis which today are responsible for the constant improvement of the quality of life. The Titanium alloys are widely used as implants due to its properties, like high mechanical resistance, biocompatibility and corrosion resistance, and the addition alloying elements like Zirconium, may improve some of those properties. Such properties are related to the microstructure and consequently to the type of processing performed. The purpose of this dissertation was to characterize the experimental alloy Ti15Zr after route of processsing and heat treatment in order to extend the knowledge about this alloy. The latter has been abtained by fusion of pure metals in a arc melting furnace with an inert argon atmosphere. The material has been homogenized in a tube furnace at 950ºC for 24h and cold worked by swaging, after that, bars with 10 mm of diameter were obtained by the process of rotary forging. The samples were solubilized at 900º C for 2 hours and quenched in water. After that, 4 samples were submitted to the aging, at 400º C, 450º C, 500º C and 550º C. The microstructure and phase analysis was done by optical microscopy and X-rays diffraction (XRD), the mechanical characterization was carried out by microhardness test and finally, evaluation of corrosion resistance of the alloy by electrochemical tests. The XRD and the optical microscopy made it possible to analyze that the heat treatment influenced the phase shifting from α to α', and probably affected the alloy hardness, at the first aged sample at 500º Chas been a sudden increase in the value of hardness, probably by appearance of omega phase, unwanted phase to the medical application duo to great fragility, and finally ... (Complete abstract click electronic access below)

Estratigrafia do Andar Alagoas na sub-bacia do Tucano Norte, Bahia

Pós-graduação em Geociências e Meio Ambiente - IGCE

EC24-721 Dairy Barns for Nebraska

The increasing interest shown among the farmers thruout this state in the betterment of dairy stock, and the tendency to give more attention to dairying on the farms, is bringing to the Agricultural College a great many requests for plans and suggestions for dairy barn construction. It is impossible to give every one of these inquiries individual attention to the extent of drawing a detailed plan to suit the conditions in each case. It is hoped therefore, that the material contained in this bulletin will offer helpful suggestions and answer many questions in the minds of prospective dairy men and dairy barn builders relative to the arrangement and construction of barns.

Impact of Bottom Flange Confinement Reinforcement on Performance of Prestressed Concrete Bridge Girders

For many years AASHTO provided no recommendation to state DOT’s on bottom flange confinement reinforcement for their bridge superstructures. The 1996 edition of AASHTO Standard Specification for Highway Bridges stated that nominal reinforcement be placed to enclose the prestressing steel from the end of the girder for at least a distance equal to the girder’s height. A few years later the 2004 AASHTO LRFD Bridge Design Specification changed the distance over which the confinement was to be distributed from 1.0h to 1.5h, and gave minimum requirements for the amount of steel to be used, No.3 bars, and their maximum spacing, not to exceed 6”. Research was undertaken to study what impact, if any, confinement reinforcement has on the performance of prestressed concrete bridge girders. Of particular interest was the effect confinement had on the transfer length, development length, and vertical shear capacity of the fore mentioned members. First, an analytical investigation was performed on the subject, and then an experimental investigation followed which consisted of designing, fabricating, and testing eight tee-girders and three NU1100 girders with particular attention paid to the amount and distribution of confinement reinforcement placed at the end of each girder. The results of the study show: 1) neither the amount or distribution of confinement reinforcement had a significant effect on the initial or final transfer length of the prestress strands; 2) at the AASHTO calculated development length, no significant impact from confinement was found on either the nominal flexural capacity of bridge girders or bond capacity of the prestressing steel; 3) the effects from varied confinement reinforcement on the shear resistance of girders tested was negligible, however, distribution of confinement did show to have an impact on the prestressed strands’ bond capacity; 4) confinement distribution across the entire girder did increase ductility and reduced cracking under extreme loading conditions.

Avaliação da resistência à corrosão da liga Ti-30Ta submetida a diferentes taxas de deformação visando aplicações biomédicas

This study aims to evaluate the corrosion resistance of Ti-30Ta alloy when subjected to different strain rates. Samples of the alloy Ti-30Ta were obtained from the melting of pure elements in the arc furnace in inert atmosphere (argon gas). Then, the samples were subjected to a thermal treatment and to cold worked to obtain bars. After forging, the samples were machined in accordance with ASTME9-09 standard for carried out compression tests. To microstructural characterization, samples were sectioned longitudinal and transversally and embedded in resin. After, the wet sanding and polishing were performed, followed by a chemical attack, in order to study the microstructure under an optical microscope. Microhardness was measured on the samples that were subjected to microstructural characterization by using microhardness tester. Phases were evaluated by x-rays diffraction. Corrosion tests were carried out to evaluate the influence of deformation on the corrosion resistance. Results show that microstructure was not influenced by deformation

Estudo para determinação de uma metodologia para o ensaio de arrancamento que avalia aderência aço/concreto

This work talks about the importance of the steel adhesion to concrete, reinforced concrete structures, their testing and forms of measurement used and how the results are used in the structural design, which uses as a reference the NBR 6118 and NBR 7480. It also deals with the importance of a reliable assessment, discussing failures that the test used, NBR 7477, features in specific circumstances, as discussed under the EC-094. It also presents an initial proposal for simplified pullout test, which aims to analyze the grip on steel bars with diameter less than 10 mm, which results when used standardized testing by ABNT NBT 7477, has shown excessive variability, the main criticism of the trial today used without distinction to be established thick or thin bars. The proposal also presented methodology is in the consolidation phase, given the time and the volume of necessary tests. For this reason it is not possible to make a comparison between the values obtained and the results of the test used on the basis of the standard in force, this can only be done once the front with a continuation of this work

Caracterização da liga Ti-15Zr visando aplicações biomédicas

With advances in health care, has been na increase of demand for material that could replace the functions of the human body parts, thus evolved biomedic prosthesis which today are responsible for the constant improvement of the quality of life. The Titanium alloys are widely used as implants due to its properties, like high mechanical resistance, biocompatibility and corrosion resistance, and the addition alloying elements like Zirconium, may improve some of those properties. Such properties are related to the microstructure and consequently to the type of processing performed. The purpose of this dissertation was to characterize the experimental alloy Ti15Zr after route of processsing and heat treatment in order to extend the knowledge about this alloy. The latter has been abtained by fusion of pure metals in a arc melting furnace with an inert argon atmosphere. The material has been homogenized in a tube furnace at 950ºC for 24h and cold worked by swaging, after that, bars with 10 mm of diameter were obtained by the process of rotary forging. The samples were solubilized at 900º C for 2 hours and quenched in water. After that, 4 samples were submitted to the aging, at 400º C, 450º C, 500º C and 550º C. The microstructure and phase analysis was done by optical microscopy and X-rays diffraction (XRD), the mechanical characterization was carried out by microhardness test and finally, evaluation of corrosion resistance of the alloy by electrochemical tests. The XRD and the optical microscopy made it possible to analyze that the heat treatment influenced the phase shifting from α to α', and probably affected the alloy hardness, at the first aged sample at 500º Chas been a sudden increase in the value of hardness, probably by appearance of omega phase, unwanted phase to the medical application duo to great fragility, and finally ... (Complete abstract click electronic access below)

Estratigrafia do Andar Alagoas na sub-bacia do Tucano Norte, Bahia

Pós-graduação em Geociências e Meio Ambiente - IGCE

A novel HS-SBSE system coupled with gas chromatography and mass spectrometry for the analysis of organochlorine pesticides in water samples

A methodology to analyze organochlorine pesticides (OCPs) in water samples has been accomplished by using headspace stir bar sorptive extraction (HS-SBSE). The bars were in house coated with a thick film of PDMS in order to properly work in the headspace mode. Sampling was done by a novel HS-SBSE system whereas the analysis was performed by capillary GC coupled mass spectrometric detection (HS-SBSE-GC-MS). The extraction optimization, using different experimental parameters has been established by a standard equilibrium time of 120 min at 85 degrees C. A mixture of ACN/toluene as back extraction solvent promoted a good performance to remove the OCPs sorbed in the bar. Reproducibility between 2.1 and 14.8% and linearity between 0.96 and 1.0 were obtained for pesticides spiked in a linear range between 5 and 17 ng/g in water samples during the bar evaluation.

Porcelain monolayers and porcelain/alumina bilayers reinforced by Al2O3/GdAlO3 fibers

Aim. This work tested the effect of the addition of Al2O3/GdAlO3 longitudinal fibers in different contents to veneering porcelain of two dental all ceramic systems. Methods: Fibers (0.5 mm diameter) obtained by the Laser Heated Pedestal Growth (LHPG) method were added to bar-shaped specimens made by veneer porcelain (monolayers) or both the veneer and the core ceramic (bilayers) of two all-ceramic systems: In-Ceram Alumina - glass infiltrated alumina composite (GIA) and In-Ceram 2000 AL Cubes - alumina polycrystal (AP) (VITA Zahnfabrik). The longitudinal fibers were added to veneering porcelain (VM7) in two different proportions: 10 or 17 vol%. The bars were divided into nine experimental conditions (n = 10) according to material used: VM7 porcelain monolayers, VM7/GIA, VM7/AP; and according to the amount of fibers within the porcelain layer: no fibers, 10 vol% or 17 vol%. After grinding and polishing the specimens were submitted to a three point bending test (crosshead speed = 0.5 mm/min) with porcelain positioned at tensile side. Data were analyzed by means of one-way ANOVA and a Tukey's test (alpha = 5%). Scanning electronic microscopy (SEM) was conducted for fractographic analysis. Results. Regarding the groups without fiber addition, VM7/AP showed the highest flexural strength (MPa), followed by VM7/GIA and VM7 monolayers. The addition of fibers led to a numerical increase in flexural strength for all groups. For VM7/GIA bilayers the addition of 17 vol% of fibers resulted in a significant 48% increase in the flexural strength compared to the control group. Fractographic analysis revealed that the crack initiation site was in porcelain at the tensile surface. Cracks also propagated between fibers before heading for the alumina core. Conclusions. The addition of 17 vol% of Al2O3/GdAlO3 longitudinal fibers to porcelain/glass infiltrated alumina bilayers significantly improved its flexural strength. 10 vol% or 17 vol% of fibers inclusion increased the flexural strength for all groups. (C) 2011 Elsevier Ltd. All rights reserved.

Conservative Treatment of Comminuted Mandibular Fracture Involving Maxillomandibular Fixation With Miniplates

Bars and steel wires are the most commonly used methods to achieve maxillomandibular fixation, although there are numerous alternatives described for this same purpose. In cases of edentulous candidates for the conservative treatment of facial fractures, none of the conventional methods can be instituted for maxillomandibular fixation. Fixation in such cases is achieved with the aid of the total dentures of the patient or the confection of splints, but these methods lead to eating and oral hygiene problems. This article reports the case of an edentulous patient with a comminuted mandible fracture treated with a rarely described technique in which intermaxillary fixation was achieved with titanium miniplates.

Footprints of a trypanosomatid RNA world: pre-small subunit rRNA processing by spliced leader addition trans-splicing

The addition of a capped mini-exon [spliced leader (SL)] through trans-splicing is essential for the maturation of RNA polymerase (pol) II-transcribed polycistronic pre-mRNAs in all members of the Trypanosomatidae family. This process is an inter-molecular splicing reaction that follows the same basic rules of cis-splicing reactions. In this study, we demonstrated that mini-exons were added to precursor ribosomal RNA (pre-rRNA) are transcribed by RNA pol I, including the 5' external transcribed spacer (ETS) region. Additionally, we detected the SL-5' ETS molecule using three distinct methods and located the acceptor site between two known 5' ETS rRNA processing sites (A' and A1) in four different trypanosomatids. Moreover, we detected a polyadenylated 5' ETS upstream of the trans-splicing acceptor site, which also occurs in pre-mRNA trans-splicing. After treatment with an indirect trans-splicing inhibitor (sinefungin), we observed SL-5' ETS decay. However, treatment with 5-fluorouracil (a precursor of RNA synthesis that inhibits the degradation of pre-rRNA) led to the accumulation of SL-5' ETS, suggesting that the molecule may play a role in rRNA degradation. The detection of trans-splicing in these molecules may indicate broad RNA-joining properties, regardless of the polymerase used for transcription.

Bosentan, an endothelin receptor antagonist, ameliorates collagen-induced arthritis: the role of TNF-alpha in the induction of endothelin system genes

Endothelins (ETs) are involved in several inflammatory events. The present study investigated the efficacy of bosentan, a dual ETA/ETB receptor antagonist, in collagen-induced arthritis (CIA) in mice. CIA was induced in DBA/1J mice. Arthritic mice were treated with bosentan (100 mg/kg) once a day, starting from the day when arthritis was clinically detectable. CIA progression was assessed by measurements of visual clinical score, paw swelling and hypernociception. Histological changes, neutrophil infiltration and pro-inflammatory cytokines were evaluated in the joints. Gene expression in the lymph nodes of arthritic mice was evaluated by microarray technology. PreproET-1 mRNA expression in the lymph nodes of mice and in peripheral blood mononuclear cells (PBMCs) was evaluated by real-time PCR. The differences were evaluated by one-way ANOVA or Student's t test. Oral treatment with bosentan markedly ameliorated the clinical aspects of CIA (visual clinical score, paw swelling and hyperalgesia). Bosentan treatment also reduced joint damage, leukocyte infiltration and pro-inflammatory cytokine levels (IL-1 beta, TNF alpha and IL-17) in the joint tissues. Changes in gene expression in the lymph nodes of arthritic mice returned to the levels of the control mice after bosentan treatment. PreproET mRNA expression increased in PBMCs from rheumatoid arthritis (RA) patients but returned to basal level in PBMCs from patients under anti-TNF therapy. In-vitro treatment of PBMCs with TNF alpha upregulated ET system genes. These findings indicate that ET receptor antagonists, such as bosentan, might be useful in controlling RA. Moreover, it seems that ET mediation of arthritis is triggered by TNF alpha.

ENVIRONMENTAL TOBACCO SMOKE INDUCES OXIDATIVE STRESS IN DISTINCT BRAIN REGIONS OF INFANT MICE

Environmental tobacco smoke (ETS) leads to the death of 600,000 nonsmokers annually and is associated with disturbances in antioxidant enzyme capacity in the adult rodent brain. However, little is known regarding the influence of ETS on brain development. The aim of this study was to determine levels of malonaldehyde (MDA) and 3-nitrotyrosine (3-NT), as well as enzymatic antioxidant activities of glutathione peroxidase (GPx), glutathione reductase (GR), glutathione S-transferase (GST), and superoxide dismutase (SOD), in distinct brain structures. BALB/c mice were exposed to ETS twice daily for 1 h from postnatal day 5 through postnatal day 18. Acute exposure was performed for 1 h on postnatal day 18. Mice were euthanized either immediately (0) or 3 h after the last exposure. Immediately after an acute exposure there were higher GR and GST activities and MDA levels in the hippocampus, higher GPx and SOD activities in the prefrontal cortex, and higher GST activity and MDA levels in the striatum and cerebellum. Three hours later there was an increase in SOD activity and MDA levels in the hippocampus and a decrease in the activity of all enzymes in the prefrontal cortex. Immediately after final repeated exposure there were elevated levels of GST and GR activity and decreased GPx activity in the hippocampus. Moreover, a rise was found in GPx and GST activities in the prefrontal cortex and increased GST and GPx activity in the striatum and cerebellum, respectively. After 3 h the prefrontal cortex showed elevated GR and GST activities, and the striatum displayed enhanced GST activity. Data showed that enzymatic antioxidant system in the central nervous system responds to ETS differently in different regions of the brain and that a form of adaptation occurs after several days of exposure.