Efeito do acréscimo de nano-hidroxiapatita nas propriedades físico-químicas, mecânicas e antibiofilnme do cimento portland com óxido de zircônio

Pós-graduação em Odontologia - FOAR

Análise de dissipadores de calor com filmes de diamante CVD

Dissipadores de calor recobertos com filmes de diamante CVD foram desenvolvidos para acoplar a semicondutores, utilizando-se do Laboratório de Deposição de Filmes de Diamante CVD, na UNESP - Campus de Guaratinguetá e o Laboratório de Diamantes da Universidade São Francisco, em Itatiba, SP. Analisou-se o filme de diamante CVD sobre o silício, para emprego como dissipador de calor, porque o filme de diamante CVD pode ter o valor da condutividade térmica até cinco vezes superior ao do cobre e de dez vezes a do alumínio. Os filmes foram obtidos via deposição através de reator de filamento quente, trabalhando-se com vários filamentos retilíneos em paralelo, resultando assim em um processo que visou obter um filme mais uniforme e com grande área de deposição. Os dados para análises da composição química superficial dos filmes foram obtidos por Difração de Raios-X, Dispersão de Energia de Raios-X e para a verificação da morfologia e espessura do filme foi utilizada a Microscopia Eletrônica de Varredura. Para a verificação do comportamento da temperatura sobre o dissipador com o filme de diamante CVD foi utilizada uma câmera de imagem termográfica, marca Fluke, modelo Ti 40 FT. Foram obtidos filmes de 2 e 10 ?m sobre o silício. Estas espessuras ainda não oferecem um desempenho mecânico que o torne autosustentado. Do ponto de vista de desempenho térmico as análises mostraram que, mesmo com pequena espessura, o filme de diamante CVD apresentou bom resultado experimental. Os principais desafios de construção para esse dissipador de calor são a obtenção do filme com espessura acima de um mm e a garantia da qualidade do filme com a repetitividade do processo em cujo caso torna-se necessário definir as dimensões do dissipador antes da deposição do filme.

Desempenho adesivo de sistemas de união à dentina aplicados in vivo e in vitro: efeito da pressão intrapulpar e profundidade dentinária

O objetivo do presente estudo foi investigar a influência da pressão intrapulpar e da profundidade dentinária sobre o desempenho adesivo de dois agentes de união à dentina, Single Bond (3M ESPE, St. Paul, MN, EUA) e Clearfil SE Bond (Kuraray, Tokyo, Japão), aplicados in vitro e in vivo. Quarenta e oito prémolares superiores hígidos foram selecionados e os pares pertencentes aos mesmos pacientes foram aleatoriamente distribuídos em 4 grupos experimentais de acordo com o sistema adesivo e a pressão intrapulpar, presente ou ausente. Dos dentes pertencentes ao mesmo par, um foi tratado in vivo e o outro in vitro. A ausência ou presença de pressão intra-pulpar foi determinada in vivo pelo uso de anestésicos locais com ou sem vasoconstritor, respectivamente. In vitro, os dentes foram mantidos sob pressão hidrostática de 15 cm de água por 24 horas. Cavidades de classe I foram preparadas e os sistemas adesivos aplicados de acordo com a recomendação dos fabricantes, seguidos da restauração incremental em resina composta. Para os dentes tratados in vitro, os mesmos procedimentos restauradores foram realizados após 6 meses de armazenagem em solução contendo timol 0,1%. Espécimes com área de secção transversal de 1 mm2 foram obtidos e submetidos ao ensaio mecânico de microtração. In vivo, ambos os sistemas adesivos apresentaram desempenho adesivo comparável, enquanto in vitro, o sistema Single Bond foi superior ao sistema Clearfil SE Bond. Esse último não foi influenciado por nenhuma das variáveis estabelecidas no estudo, ou seja, aplicação in vitro ou in vitro, presença de pressão intrapulpar e profundidade em dentina. O sistema Single Bond aplicado sob pressão intrapulpar positiva sofreu variação significante de resistência de união em função da profundidade da dentina, ou seja, em dentina profunda seu desempenho adesivo... (Resumo completo, clicar acesso eletrônico abaixo)

O efeito protetor contra o dano muscular: alternativas às contrações excêntricas máximas

Já é bem estabelecido que, após a realização de exercícios aos quais não se está acostumado, principalmente se esses envolverem contrações excêntricas, ocorre um processo conhecido como dano muscular (DM). Esse processo consiste na desorganização e/ou rompimento de células musculares graças a elevados níveis de estresse mecânico e/ou metabólico. Esse processo pode ser identificado pela manifestação de sintomas clássicos como dor muscular, diminuição da amplitude de movimento, perda de força e extravasamento de proteínas intracelulares para a corrente sanguínea, entre outros. Sabe-se que, após a ocorrência do DM, o músculo acometido se recupera e passa a ser mais resistente a esse fenômeno, apresentando respostas atenuadas desses sintomas. Recentemente, diferentes estratégias de proteção contra o DM que não envolvem a realização de contrações excêntricas máximas vêm sendo apresentadas, como a realização de contrações excêntricas submáximas, contrações isométricas, treinamento de flexibilidade e aumento da temperatura muscular previamente ao exercício. O objetivo do presente estudo foi revisar essas estratégias de proteção contra o DM para melhor entender esse fenômeno. Foram realizadas pesquisas em importantes bases de dados e, os artigos encontrados que forem relevantes ao tema serão revisados e didaticamente explanados ao longo do trabalho

Análise granulométrica do compósito cimentício produzido com adição de resíduos de madeira e escória

Since the early twenty-first century, the construction sector has been the second largest on the rise in the Brazilian industrial sector, with a growth of 1.4% in 2012, and is likely to remain at this level for a long time. However, unlike decades ago, the industry has been seeking in its manufacturing process, sustainable materials, encompassing in their works the concept of sustainability. Thus, the timber sector seeks to satisfy a market increasingly demanding, innovating techniques and utilization being less aggressive to the environment. The purpose of this study was to produce and evaluate the mechanical strength of the composite cement with the addition of wood residues and slag low oven. Therefore, it was made 42 specimen cement-slag-wood, carried out in two steps. Since at the first, it was varied only the slag particle size, and at the second, through the best result of the previous step, it was varied the wood particles granulometry. The mechanical performance of the composite was evaluated by the results obtained in the compression test and the physical test for determining the density of the material. In the first step of the process can be concluded that the best result was achieved with the use of slag particles retained on the 60 mesh sieve. In the second phase of the study concluded that the best results were achieved with wood particles with the large particles, i.e. particles retained on the 10 mesh sieve. Both in the first and in the second step it can be seen that there has been the influence of the particle size of the waste materials. With the obtained results, could be evaluated that the use of waste for the production of cement-slag-wood composite showed lower performance when compared to the results obtained in studies without the use of waste. However, some applications are feasible to be performed with the use of composite wood-cement-slag

Gestão ambiental aplicada a prevenção, controle e recuperação de erosão linear acelerada no município de Ipeúna-SP

The erosion is a natural process of detachment, transport and deposition of soil and rock particles from one place to another. Human activities with no previous planning may accelerate this process, causing several damages to the environment and to society. In order to control the acceleration of these erosion processes caused by humans, prevention and improvement initiatives emerge. Regarding works which interfere directly in some of the natural resources, these initiatives must respect the intrinsic physical properties of the area of interest, if they aim to obtain effective results. Based on this scenario, this work proposes a few methods of accelerated linear erosion prevention, control and recovery in a specific area of the municipal district of Ipeúna (SP). For that matter, this study is based on a method of physiographic compartmentalization of the area, considering and integrating soil, relief, geology and the use and land cover properties of the study area. Plus, a flowchart with general orientations regarding management of eroded areas was produced, focused on the control and recovery of linear erosion. The result demonstrates the importance of careful erosion control, respecting the physical properties of each physiographic unit. The vegetative and mechanical conservationists methods, and the discipline of water flow, have found wide applicability in the study area.

Influência do uso de hipoclorito de sódio 2,5% e extrato glicólico de sálvia 20% durante o preparo biomecânico sobre a resistência adesiva de retentores intra- radiculares: avaliação através do teste de push-out

The aim of this study it was to evaluate the use of irrigating solution used during root canal preparation on the adhesive cementation of prefabricated fiberglass pins. The bond strength between different regions of the root and the fiberglass pins cemented into the root canal were evaluated by push-out assay. For this study, 36 human teeth were used, all equally prepared. The irrigating solutions used for biomechanical preparation were: saline solution, sodium hypochlorite 2,5% and glycolic extract of salvia 20%. The dual cure resin cement was used for cementation of pins. After cementation, specimens were sectioned to give 3 slices of approximately 2 mm each (cervical, middle and apical), which were submitted to mechanical push-out test. Were performed ANOVA and Tukey's test with a significance level of 5%, for the analysis of mechanical test. Comparing the thirds we observed that the only solution that presented statistical difference in the bond strength was sodium hypochlorite, which showed higher values for the middle and apical third compared with the cervical third, but when compared without taking into consideration the dental thirds, solutions studied showed no differences in bond strength. Therefore, it was concluded that the solutions studied can be used during endodontic treatment without causing harmful effects on the final adhesive restoration

Otimização do braço inferior da suspensão dianteira do veículo Baja utilizando o método dos elementos finitos

Mass reduction coupled with the mechanical performance in service has been the goal of many projects related to the transport area, considering the advantages that mass reduction can bring. However, make a simple material substitution without design a new geometry to corroborate for the best component performance, often makes the replacement unviable. In this study, it was investigated the advantages of replacing the prototype BAJA SAE front suspension lower arm of Equipe Piratas do Vale de BAJA SAE - Universidade Paulista, Campus Guaratinguetá, actually produced with steel, for a new component made of carbon fiber composite. The new geometry has been developed to provide the best possible performance for this component and your easy manufacturing. The study was done using the 3D modeling tools and computer simulations via finite element method. The first stage of this work consisted on calculation of the estimated maximum contact force tire / soil in a prototype landing after jump at one meter high, drop test in the laboratory with the current vehicle, current front suspension lower arm 3D modeling, finite element simulation and analysis of critical regions. After all current component analysis, a new geometry for the part in study was designed and simulated in order to reduce the component mass and provide a technological innovation using composite materials. With this work it was possible to obtain a theoretical component mass reduction of 25,15% maintaining the mechanical strength necessary for the appropriated component performance when incited

Estudo comparativo de dois tipos de painéis de MDP: com adição de papel impregnado e lâminas de bambu

This work is the production of two types of particle boards reconstructed MDP (Medium Density Particleboard), the first with the addition, in the inner layer of particles of impregnated paper, the ratios of 0%, 1%, 5% and 20 %. In the second type of panel MDP was inserted with blades of bamboo species Dendrocalumus giganteus as coatings and structural reinforcement. The MDP panel, used as a basis for both cases has the composition of three layers, two external particles with smaller particle size and an inner layer composed of particles of larger particle sizes. Assays were performed based on physical and mechanical NBR 14.810/2006 for the determination of the board density, thickness swelling, water absorption, moisture content, bending, tension parallel and perpendicular, and testing of particle sizes of the particles did not exists in standard references. The results were analyzed and compared the results of the commercial boards made from 100% eucalyptus, based on the limits specified by the ABNT NBR 14.810/2006. The values of the tests showed similar results indicating normative specifications in a positive way, the possibility of production of MDP with the use of waste paper impregnated. As for the panel with bamboo blades, the tests showed a mechanical performance far superior to MDP market, explaining the study and possible implementation of the bamboo for use where the MDP will suffer greater mechanical stress, such as doors, tops and benches tables

Analise mecânica e microestrutural em estruturas tubulares aeronáuticas soldadas de aço ABNT 4130

Airplane Motor Cradles have a complex geometry, since they require different conbinations between different tubes and TIG welded in several angles. In T-25 aircraft and Universal T-27 Tucano (EMBRAER / FAB), besides having to bear the engine balance, these components maintain fixed the nose landing gear in another extremity. They are considered critical to flight safety, and for this reason, the aviation standards are extremely rigid in their production, imposing a zero index” of defects on the final weld metal quality. These structures may be containing an historical of welding repairs, whose effects on their structural integrity are not computed. In this work we analyzed the standardised AISI 4130 steel and the raw steel of tubes to the Airplane Motor Cradles. First of all, microscopy and microanalysis of the base steel, then we analyzed the effects of the TIG weld. Tensile testing was conducted to measure the difference between the mechanical properties of standardised steel and without this treatment

Desempenho estrutural de vigas em madeira laminada colada armada

The objective of the present work was to evaluate Pinus’ glued laminated timber (glulam) beams and steel reinforced glulam beams, using PU mono-component adhesive in lamination step and epoxy adhesive to bond steel bars. The mechanical performance was verified through bending test, and the adopted method based on homogenized section, to considerate the differences between wood and steel mechanical properties. The homogenization section method proved itself effective in obtaining the stiffness of the parts in MLCA. The stiffness of reinforced beams increased 91% in comparison with glulam beams, differing only 5.5 % from value of stiffness calculated

Fractografia quantitativa e o conceito de tenacidade à fratura para a análise do efeitodo choque térmicos em TiO2

The present study evaluated the use of semicircular bending test (SCB) as an alternative to conventional bending test to examine the effect of thermal shock. Still, studies the behavior of fracture surfaces generated by monofractal behavior analysis, which allows us to evaluate the contributions of the microstructure and the mechanical context in forming reliefs during the crack propagation. The fractal analysis is made from elevation maps obtained by reconstruction method by extension of the focus stacks of digital images acquired in microscope. The specimens used were samples semicircular pressed TiO2 (rutile) with and without heat shock, prepared for testing mode I loading. Were also produced, specimens in the form of bars for Weibull statistical analysis. From the three-point bending test, we found the variation of fracture toughness between the samples after the heat shock and natural condition. The SCB test was feasible for the analysis of thermal shock resistance. The results showed that the value of the fracture toughness decreases as the heat shock treatment

Revestimento interno de tubulação por um processo de centrifugação utilizando resina éster-vinílica com adição de cargas

Being the corrosion one of the great problems facing the industry today, specifically the internal corrosion of pipes in chemical and petrochemical industries, hence this work proposes a new type of internal coating in order to avoid fouling and decrease the pressure loss in the flow. For this, we use a composition of vinyl ester resins and manometric loads, which after cleaning and preparation of the internal surface of the tube will be applied through a process of centrifugation, adjusted by a lathe. After curing the resin, a test of roughness will be realized in order to analyze the reduction of friction factor and thus be able to conclude whether there was a significant decrease in pressure drop. With test results in hand, we hope to obtain a coating that meets most of the properties required by the industry and to provide a reduction in operating costs and a visible improvement in the conditions of use of the pipe

Uma análise da eficiência de uma transmissão CVT

This undergraduate thesis evaluates the effects of temperature variation of the air inside the CVT gearbox on the performance of a Continuously Variable Transmission (CVT). The CVT used in the tests was manufactured by Gaged Engineering (GX9 model) and is currently used in a Baja prototype. It’s a mechanically operated CVT, which the movement of the pulley plates varies according to the drive shaft rotation, shifting the belt along the diameter, and varying the transmission ratio. The purpose of this work is to analyze the change in the slip factor, coefficient that compares the variation between the actual transmission ratio and the ratio of geometric transmission, and its correlation with the power variation. A test bench was built and some tests were performed, indicating that was possible to achieve output power ratios of 1.75 [ℎ

Avaliação da colagem de suportes utilizados para fixar cabos elétricos em aeronaves

The most usual method to fix supports that hold the vast majority of electrical cables on an aircraft is accomplished by using, for this purpose, rivets. However, this procedure may some cause some inconveniences such as the need of effecting holes in the structure that is intended to fix these supports, thus decreasing resistance of the structure. In order to have an alternative to seek an increase in the performance of structured materials, the aircraft industry, like other industries, have been studying the use of collage as a method of replacing this usual forms. Against this backdrop, this paper aims to assess the strength and durability of a joint bonded using the adhesive EA9394, manufactured by company Henkel Corporation, and perform a careful survey of the mechanical performance of riveted structures, taking into account different types of conditioning environment and thus create a database that can be used by the aerospace industry