Determinação de fármacos diuréticos em associação por cromatografia em camada delgada e espectrofotometria

A rapid, sensitive and reliable thin-layer chromatography/spectrophotometry screening procedure was developed for quantitative determination of diuretics associated in pharmaceutical dosage forms. The chromatographic method employed microcrystalline cellulose and butanol : acetic acid : water (4:1:1) or amilic alcohol : ammonium hydroxide 25% (9:1) as mobile phases and detection by U.V. light. The drugs were extracted using a simple procedure and were quantified by U.V. spectrophotometry. Results varied from 97.5 to 102.5% and are similar to those obtained by conventional methods. This method of quantification of diuretics is promising for quality control of drugs.

Estudio digital radiográfico y densitométrico en mandíbulas de cerdos sometidos a osteotomía con alta y baja velocidad, con refrigeración líquida

The influence of the type of rotary cutting instrument on bone repair after osteotomy in swine jaw, was evaluated using digital and densitometric radiographic examinations, at controlled times. Two cross-sectional dissections were made through the base of the right jaw, one using a high speed rotary instrument and the other using low speed, both with liquid cooling. After established periods the animals were sacrificed and their jaws removed for direct and indirect digital radiographic and densitometric studies using the CROMOX, DIGORA and ODR systems. In the initial periods (7 and 28 days) the bone density was higher in osteotomy areas performed with high rotation speeds, and in the final periods (60 and 90 days) the bone density was higher in the osteotomies performed with low rotation, indicating a better final bone repair with the use of low rotation. The qualitative analysis of the repair process was made by the ODR system which obtained three-dimensional and coloured digital images, which enable the bone thickness to be measured using an aluminium wedge. This showed that by twenty-eight days the bone repair was already apparently complete. © 2010 SECOM.

Qualidade fisiológica de sementes de Brachiaria e avaliação da produtividade de massa seca em diferentes sistemas de integração lavoura-pecuária sob irrigação

The speed and magnitude of tropical pastures expansion in Brazil are related to the availability of quality seeds. This research aimed to evaluate the physiological quality of seeds of two Brachiaria species submitted to germination and viability tests and also estimate, for both species, the fresh and dry mass yield, under different irrigated crop-livestock integration systems. For field analysis, the experimental design was a randomized complete block, in subplots, with four intercrops in the plot (Brachiaria brizantha cv. Marandu and Brachiaria ruziziensis simultaneously established with corn and nitrogen fertilization coverage), and four forage cutting times, in the winter/spring season, in subplots, with four replications. In the laboratory, the experimental design was completely randomized, with four replications per treatment/test. The germination and viability tests indicated that B. brizantha seeds showed higher physiological quality, when compared with B. ruziziensis, while the tetrazolium test and germinated seedlings characteristics were similar. The B. ruziziensis, simultaneously intercropped with corn, was the less viable intercrop, due to the lower fresh and dry mass yield and litter deposition on the soil surface. In general, the pasture formation for the second season cultivation, intercropped with corn, was an excellent alternative for crop-livestock integration under a no-tillage system.

Massa seca e composição bromatológica de quatro espécies de braquiárias semeadas na linha ou a lanço, em consórcio com milho no sistema plantio direto na palha

The objective of this research was to evaluate the dry mass yield and chemical composition of four Brachiaria species in different options for sowing, exclusively or in intercrop with corn crop, under a no-tillage system. The experiment was carried out during the growing seasons of 2006 at FEPE (FE/Unesp, Ilha Solteira Campus) located in Selvíria, Mato Grosso do Sul State, Brazil. The soil of the experimental area was classified as distroferric Red Latosol (Oxisol). The experimental design was in randomized blocks, in a factorial scheme (4 × 4), with five replications. The treatments consisted of four Brachiaria species (Brachiaria brizantha cv. Marandu, Brachiaria decumbens, Brachiaria ruziziensis and Mulato II grass) grown in rows and spread on total area, exclusively or intercropped simultaneously with corn crop sowing. The study evaluated the dry mass yield and total digestible nutrients, crude protein, ash, neutral detergent fiber, acid detergent fiber, hemicelluloses, cellulose and lignin content of forage. The spread on total area intercrop of forages with corn crop proved to be viable by presenting similar dry mass yield to exclusive sowing arrangements, conversely to what happened with intercrop in row of corn crop, which decreased such yield. Brachiaria ruziziensis showed superior chemical composition and the intercrops increased energy and crude protein contents, and decreased cell wall components.

Determinação da massa seca, teor de nutrientes e cobertura do solo de espécies semeadas no outono-inverno

Culture options for the autumn-winter season are a major problem for production systems under low rainfall. The aim of this study was to evaluate the effect of the sowing season on dry matter yield, nutrient content of the shoot and soil covering percentage of coverage plants on the soil on the intercrop: grain sorghum, rattlepods, pearl millet brachiaria grass and an area with weeds (fallow). The experiment was conducted under field conditions on an Oxisol (Haplustox), clay texture, in Selvíria, Mato Grosso do Sul, Brazil. The experimental design was a randomized block design with eight replications, two sowing seasons and five coverage treatments. When the sorghum culture of the first sowing season reached the harvest stage, the dry matter yield on the other treatments was evaluated. Results showed that sowing in March results in higher dry mass yield and higher soil coverage percentage in the studied species. In the first sowing season, Brachiaria brizantha presents higher dry matter yield and macronutrients extraction.

Nitrogênio, fósforo e potássio na produção de massa seca e no acúmulo de nutrientes em mudas de limeira ácida 'tahiti'

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Composição química e digestibilidade in vitro da massa seca de cana-de-açúcar acrescida de ureia em diferentes tempos de estocagem

The objective of this research was to evaluate the chemical composition and in vitro dry mass (DM) digestibility of sugar cane with urea, maintained in the shade and sun, at different storage times. The utilized design was the completely randomized in a factorial scheme 6x2, that is, six storage times after the mixing (0; 2; 4; 6; 12 and 24 hours) and two storage location (shade and sun), with three replicates. The sugarcane utilized presented 12 months of development and was disintegrated for application of mixture (nine parts of urea for one of ammonium sulfate) to 1.0kg/100.0kg of fresh sugarcane. The samples taken with 12 hours of storage indicated that was an increase in the content of DM and crude protein (CP) of sugar cane compared to the moment of the mixture (307.6 vs. 294.2g/kg of DM and 115.2 vs. 99.3 g/kg of DM, respectively), and the smaller content of neutral detergent fiber (NDF) was observed around of 12 hours of storage (465.0g/kg of DM). The coefficients of in vitro dry mass digestibility (IVDMD) ranged of 0.558 to 0.612 in the times 0 and 12 hours, respectively. The length of storage changes the chemical composition of sugar cane plus urea. The storage location changes the dry mass content and pH values.

Estudio histológico comparativo de la reparación ósea entre hueso alveolar y extra-alveolar en los cerdos sometidos a osteotomía con alta y baja velocidad, con refrigeración líquida

Taking into account the bone repair process in pigs has shown a greater similarity among the histological variables studied compared to other biological models, the present study has as its aim to evaluate the histological bone repair process of osteotomy performed on alveolar and extra-alveolar bones, using drilling tools with liquid refrigeration. Material and method: Eighteen Large White pigs weighing between 20 and 25 Kg were divided into three groups of six animals in order to evaluate the osteotomy repairs with low and high speed in the alveolar bone and threes in the extra-alveolar area, study periods of 7, 14 and 28 days. Results: It was observed that in the alveolar bone at the postoperative times of 14 and 28 days, the best repair results were in the osteotomy performed with low speed, while in the 7 day postoperative period, the results with high speed were slightly better, in alveolar areas as well as extra-alveolar areas. There no statistically significant differences between the alveolar and extra-alveolar bone repair process. Conclusions: The repair process, by means of microscopic analysis in the alveolar and extra-alveolar areas, are similar with better results observed in osteotomies performed with low speed drills in the 14 and 28 day study periods, and at 7 days postoperative the results with high speed drills and refrigeration were slightly better. Research works using pigs as an animal model are perfectly viable. © 2011 SECOM.

Unidade amostral para determinação de massa média de frutos em lichieira em sistema orgânico e convencional

The experimental unit of measurement is a suitable technique to estimate the average character in evaluation, and experimentation should be well understood and executed, because the precision characterizes the quality of the inferences of the results. This research aimed to analyze the possibility to obtaining the quantity of fruit required for sampling of lychee plants, to determining the average mass of the fruits, with less sampling error. One hundred fruits were collected, in a hectare, in two cropping systems, conventional and organic, being one fruit per plant. From the data of fruit mass was used the Excel® to calculate the average fruit mass and number of fruits samples needed to represent the area of the producer. The results show that to achieve a sampling error of 10% for determining the average mass of fruit, 400 fruits should be collected for organic system and 370 for the conventional, while for 20% sampling error, it is necessary to collect 250 fruits per hectare in organic system and 220 in the conventional.

Eficiência de herbicidas inibidores da ALS e PROTOX sob condições de déficit hídrico no comportamento bioquímico de plantas daninhas

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Crescimento e produtividade da mamoneira iac 2028 na safrinha em função da população de plantas em espaçamento reduzido

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Eficiência agronômica de fertilizantes organominerais sólidos e fluidos em relação à disponibilidade de fósforo

Pós-graduação em Agronomia (Agricultura) - FCA

Efeito de treinamentos resistidos sobre marcadores inflamatórios, força e massa magra corporal de pacientes com doença pulmonar obstrutiva crônica

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Influência do treinamento físico de alta intensidade sobre o metabolismo de ratos espontaneamente hipertensos (SHR)

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Estudo físico-químico de nanopartículas de DNA com derivado de quitosana contendo grupos fosforilcolina

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)