982 resultados para Chemical Analysis
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Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)
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Pós-graduação em Agronomia (Produção Vegetal) - FCAV
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Pós-graduação em Engenharia Mecânica - FEIS
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Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
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Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
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Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
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Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
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Pós-graduação em Agronomia (Horticultura) - FCA
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Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
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Chemical analysis of leaves is an effective tool for detecting nutritional imbalances and providing data for fertilizer recommendations. Therefore, it is extremely important to establish criteria for interpreting these results. The DRIS (Diagnosis and Recommendation Integrated System) method is an alternative to the interpretation of results of leaf analysis as it allows the calculation of indexes for each nutrient, using its relations with others and comparing them with a reference population. Thus, we aimed to establish preliminary DRIS norms, by both Beaufils's and Jones's methods, and to derive critical levels and nutrient sufficiency ranges in the leaf tissue for Pera orange, by studying a commercial crop in the growing conditions of the Sao Paulo state. The methods (Beaufils and Jones) differed in the limiting nutrients in the Pera orange orchard. The use of regional norms must be prioritized because of differences between the management methods applied. In the methods used, the nutrients that had a greater number of concordant cases in decreasing order: Mn > Mg > B > N > Cu > Fe > Zn > K > P > Ca. Amplitudes related to the DRIS methods used were narrower than the conventional literature.
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The present work deals with the study on the evaluation of the human health risks caused by the leaching of hydrocarbon products from a gas station in Sumaré-SP. First, a geoenvironmental diagnosis had to be done, where information such as: history of the area, chemicals involved, geological characteristics, transport, chemical analysis, were used to make it. The geoenvironmental diagnosis was used in the software RBCA tier 2 which established the risks by all possible pathways. The results indicated that there are risks for groundwater ingestion for commercial (on site and off site) and residential receptors and 10 that there´s risk for inhalation of vapors in enclosed space for the commercial receptor on site. The evaluation also calculated the specific target levels that the area needs to show, in order not to harm human beings and the environment. That makes RBCA a great tool that can helps the remediation actions needed to be done so that the human being and the environment remain secure.
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This work consists of preparation and characterization of glasses containing transition noble metals and the study of optical properties of such materials. The glasses were prepared by quenching of the glass melt followed by heat treatment and polishing of the monoliths. The structural characterization of glasses was made using differential thermal analysis, X-ray, Raman and infrared spectroscopies, while the optical properties were studied by UV-Vis and M-Lines spectroscopies. Preliminary results have shown that the color of the glasses is dependent on both concentration of silver and the melting temperature of the melt. Controlled heat treatments have been used to induce the crystallization of Ag nanoparticles within the glass. The study of crystallization was accompanied by electron microscopy and UV-Vis spectroscopy. Data from electron diffraction, as well as chemical analysis, EDX, were obtained using a transmission electron microscope. EDX data have shown that the atomic percentage of Ag is higher on the nanoparticle. X-ray diffraction was used in order to characterize the composition of the crystals and cubic AgCl was identified as the main crystallized nanophase obtained after annealing
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In order to to research, the region of Perau, base metal mineralization, Grupo Votorantim Metals conducted a soil sampling on targets predetermined holding its chemical analysis. These reviews have been provided by the company for this work was to evaluate the potential use of these data pedogeochemical multi-element for refinement of the work of geological mapping. We selected six targets: Varginha, Salvador, Guararema Taquara Lisa and Coffin of Mendes, in the municipalities of Adrianople, Cerro Azul and Tunas do Paraná, located in Vale do Ribeira (PR). Both have about 10 km2 and situated in the geological context of the Fold Belt Terrane and the Massif de Joinville. The main rock types are present metasedimentary rocks of low to medium grade metamorphic, interspersed the amphibolites ortoderivados, both belonging to the Complex Perau, gneisses and migmatitic Complex. Applied to the geochemical data descriptive statistical techniques (variogram, kriging and histogram). From the correlation between the distributions of elements with the geological data, we could assess the potential of the proposed methodology.
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This study aimed to produce beer, using different botanical origins of honeys (orange, eucalyptus and wild), as malt adjuncts, and their Physical-chemical and sensorial characterizations. The production was made with malt, water, hops and honey. All musts were adjusted to 12 Brix, and the concentration of honey in the formulation was 45% (based on the extract), except for the control (0%). The physical and chemical analysis were performed on malt (extract content), honey (pH, free acidity, lactonic acidity, total acidity, color, turbidity, extract content, moisture content, reducing sugar, total reducing sugar and sucrose) in wort (content extract, pH, color, turbidity, fermentability ,bitterness and total acidity) and beer apparent extract, apparent fermentability, real extract, real fermentability, alcohol content, pH, total acidity, total foam, foam density , bitterness, carbon dioxide, color and turbidity). Sensory analysis was performed by nine-points hedonic scale testing. The attributes evaluated were appearance, aroma, flavor and overall. The results were submitted to ANOVA and means compared by Tukey testing at a 5% of probability. Beer with honey as adjuncts’ had high fermentability and low content of fat, compared to the pure malt beer. The addition of honey as an adjunct did not affect the majority of the physical-chemical parameters, except for turbidity, whereas beer with honey showed the highest value for this feature, in addition, it has also presented their biterness differences the values for beer with honey were lower. The different types of honeys did not affect the acceptability of beer, however, the beer with honey showed greater acceptance between beer with malt and honey
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Infrared spectroscopy (IR spectroscopy) explores the infrared region of the electromagnetic spectrum. Like any other spectroscopic technique, it can be used to identify a compound or the composition of investigate a sample. Spectroscopy (IR) is a very important technique in qualitative chemical analysis, widely used in the chemistry of natural products, organic synthesis and transformations. In this work we study of the theoretical foundations of infrared spectroscopy, the different vibration modes, experimental techniques, and the identification and characterization of solids. Were studied as applications: their use in thermograph and remote sensing satellites