High-performance liquid chromatographic separation and identification of polyphenolic compounds from the infusion of Davilla elliptica St. Hill

The isolation of polyphenolic compounds from an infusion of the Brazilian plant Davilla elliptica (Dilleniaceae), used as tea by virtue of its digestive properties, is described. An improved preparative HPLC method was used in order to isolate pure polyphenols from the complex mixture. Liquid-liquid extraction and solid-phase extraction were employed to minimise the interference of polymeric compounds and to provide an enriched fraction of the compounds of interest. The identification of the isolated compounds was performed using analytical HPLC as well as direct injection electrospray ionisation ion trap tandem mass spectrometry (ESI-IT-MS/MS). The high flavonoid content suggests that D. elliptica may be a promising source of compounds to produce natural phytomedicines. Copyright (C) 2007 John Wiley & Sons, Ltd.

Search for narrow resonances in dilepton mass spectra in pp collisions at root s=7 TeV CMS Collaboration

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Search for resonances in the dijet mass spectrum from 7 TeV pp collisions at CMS

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Measurement of the top-quark mass in t(t)over-bar events with dilepton final states in pp collisions at root s=7 TeV

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Search for high-mass resonances decaying into tau-lepton pairs in pp collisions at root s=7 TeV

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Combined Tevatron upper limit on gg -> H -> W+W- and constraints on the Higgs boson mass in fourth-generation fermion models

We combine results from searches by the CDF and D0 collaborations for a standard model Higgs boson (H) in the process gg -> H -> W+W- in p (p) over bar collisions at the Fermilab Tevatron Collider at root s = 1.96 TeV. With 4.8 fb(-1) of integrated luminosity analyzed at CDF and 5.4 fb(-1) at D0, the 95% confidence level upper limit on sigma(gg -> H) x B(H -> W+W-) is 1.75 pb at m(H) = 120 GeV, 0.38 pb at m(H) = 165 GeV, and 0.83 pb at m(H) = 200 GeV. Assuming the presence of a fourth sequential generation of fermions with large masses, we exclude at the 95% confidence level a standard-model-like Higgs boson with a mass between 131 and 204 GeV.

Search for Signatures of Extra Dimensions in the Diphoton Mass Spectrum at the Large Hadron Collider

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Study of the Dijet Mass Spectrum in pp -> W + jets Events at root s=7 TeV

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Search for resonances in the dilepton mass distribution in pp collisions at root s=7 TeV

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Measurement of the t(t)over-bar production cross section and the top quark mass in the dilepton channel in pp collisions at root s=7 Tev

The t (t) over bar production cross section and top quark mass are measured in proton-proton collisions at root s = 7 TeV in a data sample corresponding to an integrated luminosity of 36 pb(-1) collected by the CMS experiment. The measurements are performed in events with two leptons (electrons or muons) in the final state. Results of the cross section measurement in events with and without b-quark identification are obtained and combined. The measured value is sigma(tt) - 168 +/- 18 (stat:) +/- 14 (syst:) +/- 7 (lumi:) pb, consistent with predictions from the standard model. The top quark mass m(top) is reconstructed with two different methods, a full kinematic analysis and a matrix weighting technique. The combination yields a measurement of m(top) = 175.5 +/- 4.6 (stat:) +/- 4: 6 (syst:) GeV/c(2).

Measurement of the mass difference between top and antitop quarks

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Effect of Jupiter's mass growth on satellite capture

We study the effects of Jupiter mass growth in order to permanently capture prograde satellites. Adopting the restricted three-body problem, Sun-Jupiter-Particle, we performed numerical simulations backward in time while considering the decrease in Jupiter's mass. We considered the particle's initial conditions to be prograde, at pericenter, in the region 100R(4) <= a <= 400R(4) and 0 <= e <= 0.5. The results give Jupiter's mass at the moment when the particle escapes from the planet. Such values give an indication of the conditions that are necessary for capture. An analysis of these results shows that prograde satellite capture is more complex than a retrograde one. It occurs in a two-step process. First, when the particles get inside about 0.85R(Hill) (Hills' radius), they become weakly bound to Jupiter. Then, they keep migrating toward the planet with a strong decrease in eccentricity, while the planet is growing. The radial oscillation of the particles reduces significantly when they reach a radial distance that is less than about 0.45R(Hill) from the planet. Three-dimensional simulations for the known prograde satellites of Jupiter were performed. The results indicate that Leda, Himalia, Lysithea, and Elara could have been permanently captured when Jupiter had between 50% and 60% of its present mass.

Pharmacognostical evaluation of fruits of Solanum lycocarpum A. St.-Hill. (Solanaceae)

This study describes the chemical and physical-chemical profile of plant drug and ethanolic extract obtained from fruits of Solanum lycocarpum A. St.-Hill. (Solanaceae). The physical and chemical analysis involved the granulometry determination, non-compacted apparent density, loss on drying in oven and in infrared scale, pH, ash values and extractive values. The results determined the physical-chemical characteristics of the drug plant. It was also carried out the microbiological control of the plant drug. The preliminary phytochemical screening featured the presence of tannins, flavonoids and saponins in the plant drug and alkaloids and steroids in the ethanolic exctract. The solamargine and solasonine glycoalkaloids were identified through TLC and GC/ MS. The levels of total phenols and tannins were quantified in the extract (8.90% and 6,85% respectively). Such studies contribute to the chemical identification and quality control of S. lycocarpum fruits. © 2010 Phcog.net.

Measurement of the top-quark mass in t̄t events with lepton+jets final states in pp collisions at √s =7 TeV

The mass of the top quark is measured using a sample of t̄t candidate events with one electron or muon and at least four jets in the final state, collected by CMS in pp collisions at √s =7 TeV at the LHC. A total of 5174 candidate events is selected from data corresponding to an integrated luminosity of 5.0 fb-1. For each event the mass is reconstructed from a kinematic fit of the decay products to a t̄t hypothesis. The top-quark mass is determined simultaneously with the jet energy scale (JES), constrained by the known mass of the W boson in q̄q decays, to be 173.49 ± 0.43 (stat. + JES) ±0.98 (syst.) GeV. © 2012 CERN for the benefit of the CMS collaboration.

Study of the mass and spin-parity of the Higgs boson candidate via its decays to Z boson pairs

A study is presented of the mass and spin-parity of the new boson recently observed at the LHC at a mass near 125 GeV. An integrated luminosity of 17.3 fb-1, collected by the CMS experiment in proton-proton collisions at center-of-mass energies of 7 and 8 TeV, is used. The measured mass in the ZZ channel, where both Z bosons decay to e or μ pairs, is 126.2±0.6(stat) ±0.2(syst) GeV. The angular distributions of the lepton pairs in this channel are sensitive to the spin-parity of the boson. Under the assumption of spin 0, the present data are consistent with the pure scalar hypothesis, while disfavoring the pure pseudoscalar hypothesis. © 2013 CERN. Published by the American Physical Society under the terms of the Creative Commons Attribution 3.0 License. Further distribution of this work must maintain attribution to the author(s) and the published article's title, journal citation, and DOI.