Insight into differences in nanoindentation properties of bone.

Nanoindentation provides the ideal framework to determine mechanical properties of bone at the tissue scale without being affected by the size, shape, and porosity of the bone. However, the values of tissue level mechanical properties vary significantly between studies. Since the differences in the bone sample, hydration state, and test parameters complicate direct comparisons across the various studies, these discrepancies in values cannot be compared directly. The objective of the current study is to evaluate and compare mechanical properties of the same bones using a broad range of testing parameters. Wild type C56BL6 mice tibiae were embedded following different processes and tested in dry and rehydrated conditions. Spherical and Berkovich indenter probes were used, and data analysis was considered within the elasto-plastic (Oliver-Pharr), viscoelastic and visco-elastic-plastic frameworks. The mean values of plane strain modulus varied significantly depending on the hydration state, probe geometry and analysis method. Indentations in dry bone analyzed using a visco-elastic-plastic approach gave values of 34 GPa. After rehydrating the same bones and indenting them with a spherical tip and utilizing a viscoelastic analysis, the mean modulus value was 4 GPa, nearly an order of magnitude smaller. Results suggest that the hydration state, probe geometry and the limitations and assumptions of each analysis method influence significantly the measured mechanical properties. This is the first time that such a systematic study has been carried out and it has been concluded that the discrepancies in the mechanical properties of bone measured by nanoindentation found in the literature should not be attributed only to the differences between the bones themselves, but also to the testing and analysis protocols.

Mechanics of capillary forming of aligned carbon nanotube assemblies.

Elastocapillary self-assembly is emerging as a versatile technique to manufacture three-dimensional (3D) microstructures and complex surface textures from arrangements of micro- and nanoscale filaments. Understanding the mechanics of capillary self-assembly is essential to engineering of properties such as shape-directed actuation, anisotropic wetting and adhesion, and mechanical energy transfer and dissipation. We study elastocapillary self-assembly (herein called "capillary forming") of carbon nanotube (CNT) microstructures, combining in situ optical imaging, micromechanical testing, and finite element modeling. By imaging, we identify sequential stages of liquid infiltration, evaporation, and solid shrinkage, whose kinetics relate to the size and shape of the CNT microstructure. We couple these observations with measurements of the orthotropic elastic moduli of CNT forests to understand how the dynamic of shrinkage of the vapor-liquid interface is coupled to the compression of the forest. We compare the kinetics of shrinkage to the rate of evporation from liquid droplets having the same size and geometry. Moreover, we show that the amount of shrinkage during evaporation is governed by the ability of the CNTs to slip against one another, which can be manipulated by the deposition of thin conformal coatings on the CNTs by atomic layer deposition (ALD). This insight is confirmed by finite element modeling of pairs of CNTs as corrugated beams in contact and highlights the coupled role of elasticity and friction in shrinkage and stability of nanoporous solids. Overall, this study shows that nanoscale porosity can be tailored via the filament density and adhesion at contact points, which is important to the development of lightweight multifunctional materials.

Mechanical behaviour of electrospun fibre-reinforced hydrogels.

Mechanically robust and biomimicking scaffolds are needed for structural engineering of tissues such as the intervertebral disc, which are prone to failure and incapable of natural healing. Here, the formation of thick, randomly aligned polycaprolactone electrospun fibre structures infiltrated with alginate is reported. The composites are characterised using both indentation and tensile testing and demonstrate substantially different tensile and compressive moduli. The composites are mechanically robust and exhibit large strains-to-failure, exhibiting toughening mechanisms observed in other composite material systems. The method presented here provides a way to create large-scale biomimetic scaffolds that more closely mimic the composite structure of natural tissue, with tuneable tensile and compressive properties via the fibre and matrix phases, respectively.

Mechanical behaviour of electrospun fibre-reinforced hydrogels

Mechanically robust and biomimicking scaffolds are needed for structural engineering of tissues such as the intervertebral disc, which are prone to failure and incapable of natural healing. Here, the formation of thick, randomly aligned polycaprolactone electrospun fibre structures infiltrated with alginate is reported. The composites are characterised using both indentation and tensile testing and demonstrate substantially different tensile and compressive moduli. The composites are mechanically robust and exhibit large strains-to-failure, exhibiting toughening mechanisms observed in other composite material systems. The method presented here provides a way to create large-scale biomimetic scaffolds that more closely mimic the composite structure of natural tissue, with tuneable tensile and compressive properties via the fibre and matrix phases, respectively. © 2014 Springer Science+Business Media New York.

Vibration of pressurised, elastic, spherical shells

Balloons are one example of pressurised, elastic, spherical shells. Whilst analytical solutions exist for the vibration of pressurised spheres, these models only incorporate constant tension in the membrane. For elastic shells, changes in curvature will result in restoring forces that are proportional to the elasticity in the membrane; hence the assumption of constant tension is not valid. This paper describes an analytical solution for the natural frequencies of an elastic spherical shell subject to internal pressure. When the membrane tension is set to zero, the results are shown to converge to the analytical solution for a spherical shell, and when the skin elasticity is neglected, the results converge to the constant-tension solution. This analytical solution is used to predict the natural frequencies of a small balloon, based on a value for the elastic modulus that is determined using biaxial tensile testing. These predictions are compared to experimental measurements of balloon vibrations using impact hammer testing, and good agreement is seen.

聚合通信模型的测试与分析

聚合通信的性能影响着大规模并行数值计算软件的整体效率,它是基于点对点消息传递实现的。可以通过选择点对点通信模型来描述聚合通信。一个恰当的模型可以为聚合通信算法提供精确的定量分析,有助于算法的设计与研究。论文通过对若干聚合通信典型算法的测试与分析,尝试比较与定量分析两种点对点通信模型对聚合通信的描述精度。

关于蜕变测试和特殊用例测试的实例研究

提出了基于蜕变测试方法的集成测试环境MTest,进而为检验蜕变测试方法的能力和效率,以稀疏矩阵乘法程序为例设计了一组实验.该实验基于变异分析技术,分别以mutation score和错误发现率为度量指标,定量地分析和对比了特殊用例测试,以特殊测试用例和随机测试用例为源测试用例的蜕变测试这3种方法的测试能力和效率.该实验可在MTest测试环境下自动完成.实验结果表明,蜕变测试与特殊用例测试之间是互补的,而且就蜕变测试的源测试用例而言,随机测试用例在测试能力和效率上优于特殊测试用例.

Persistent Photoconductivity in n-type GaN

The persistent photoconductivity（PPC） phenomena in n-type GaN Films grown by metalorganic chemical vapor deposition（MOCVD） have been studied. After using some testing and analysis methods, such as the double crystal X-ray diffraction（DCXRD）, the photolumineseence（PL） spectra, etc, it is found that the issue which influences PPC in n-type GaN is not relative to the dislocations and yellow band （YB）, and is caused by the doping level of Si most likely.

A quantitative HPLC method for determining lactide content using hydrolytic kinetics

A new method for quantitative analysis of lactide has been developed by applying chemical kinetics to a HPLC system. The most important advance is its practical approach to the quantification of analytes that are unstable in the HPLC mobile phase. In HPLC analysis, anhydrous mobile phases cannot separate lactide from impurities, and only mixtures of water and organic solvent can achieve effective separation. By selecting conditions for testing and studying the kinetics of lactide hydrolysis, extensive experiments revealed that lactide degradation can be treated as a pseudo-first-order reaction under the given HPLC conditions, and lactide content or purity can be quantitatively determined. This method is practical for measuring the purity of the intermediate lactide in polylactic acid (PLA) production and the lactide content in PLA.

Shape memory effect of poly(L-lactide)-based polyurethanes with different hard segments

A series of biodegradable polylactide-based polyurethanes (PLAUs) were synthesized using PLA diol (M-n = 3200) as soft segment, 4,4 '-diphenylmethane diisocyanate (MDI), 2,4-toluene diisocyanate (TDI), and isophorone diisocyanate (IPDI) as hard segment, and 1,4-butanediol as chain extender. The structures and properties of these PLAUs were studied using infrared spectroscopy, differential scanning calorimetry, tensile testing, and thermomechanical analysis. Among them, the MDI-based PLAU has the highest T-g, maximum tensile strength, and restoration force, the TDI-based PLAU has the lowest T-g, and the IPDI-based PLAU has the highest tensile modulus and elongation at break. They are all amorphous. The shape recovery of the three PLAUs is almost complete in a tensile elongation of 150% or a twofold compression. They can keep their temporary shape easily at room temperature (20 degrees C). More importantly, they can deform and recover at a temperature below their T-g values. Therefore, by selecting the appropriate hard segment and adjusting the ratio of hard to soft segments, they can meet different practical demands for shape memory medical devices.

载人潜器半物理虚拟仿真系统及其性能分析

为了缩短深海载人潜器控制系统的开发周期,测试系统性能,根据载人潜器的自身特点,构建和实现了载人潜器所有传感器、执行器设备模拟,以及潜器在海底实景的运动状态的半物理虚拟仿真系统。首先,以仿真系统的硬件架构和数据流程为基础,重点介绍了潜器设备模拟的软件体系结构;其次,在仿真平台上测试了各种网络数据的传输延迟,分析了其整体性能;最后,得出了潜器控制器设计的时间约束。现阶段整个系统已经开发成功,并投入运行到潜器控制系统的安装调试中。

海洋机器人用水下电机的深水密封研究

本文研究了海洋机器人用水下电机各个部分的密封方法，同时介绍了一个先进的动密封装置以及检验密封性能的水压试验方法．经测试及实际使用表明该密封方法和动密封装置完全满足水下机器人在深水中运行的密封要求

在51单片机上移植uC/OS—II关键问题的解决

由于MCS-51系列微控制器存在着硬件堆栈小的结构缺陷,无法满足多任务环境下进行任务切换的需求,因此很难将uC/OS—II移植到MCS-51系列微控制器上。本文给出的"堆栈映射"方式很好的解决了这个问题。同时还对uC/OS—II移植过程中一些关键性问题给予了详细的论述。包括:uC/OS—II可移植的条件、内核配置和裁剪以及内核调试。

基于labview的变速箱振动测试分析系统

文章介绍了一个基于虚拟仪器技术开发的变速箱振动测试与分析系统。该系统实现了汽车变速箱振动信号的检测、分析、处理和显示存储,满足对测试过程高精度、自动化、智能化等各项测试要求。

东濮凹陷低阻油层形成机理与评价方法研究

In order to effectively identify and accurately evaluate low resistivity reservoir in Dongpu depression, using various logging data synthetically, geological and logging characteristics are summarized in term of different blocks on the basis of core analysis, cutting logging, oil testing and commissioning data. The formation mechanism of low resistivity reservoir is studied, and the main factors that cause low resistivity reservoir are discovered. The first factor is fine lithology, high shale content and hydrophilic rock. The second factor is high salinity formation water. The third factor is light oil, high gas quantity dissolved and large difference density of oil-water. The last factor is low amplitude structure of reservoir and low differential degree of oil-water. According to the characteristics of low resistivity reservoir, the method of compound lithology, the method of movable fluid, the method of phase permeability and the method of nuclear magnetic resonance logging are put forward. The compound lithology criterion of distinguishing hydrocarbon is founded in term of different blocks on the basis of electrical efficiency. The evaluation models of reservoir parameters are founded; whose core is oil saturation and phase permeability. In order to calculate oil saturation, the compound lithology model on the basis of electrical efficiency theory is chosen on condition that there is only the combination logging data of acoustic and induction; the W-S model is chosen on condition that there is all-around logging data. The calculational precision of oil saturation in low resistivity reservoir of work area is enhanced when the selection method is utilized. There are 1212 layers of reservoir newly added by the old well reexamination in the ten oil areas. The coincidence rate of logging interpretation reaches 83.2 percent according to the 74 well-times of oil testing or commissioning, which indicates that the distinguishing method and evaluation models of low resistivity reservoir above are feasible.By the reexamination, a ten million tons of proved reserves related to the low resistivity reservoir are newly added, consequently, the groundwork is established to increase reserve and production of old oilfields in the east of China and new livingness is added for the petroleum exploration and development in Dongpu depression.