987 resultados para SRS-1d


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A new sesquiterpene-substituted benzoic acid has been isolated from the brown Alga Dictyopteris divaricata Okam.. Its structure was elucidated as 3-[(2-hydroxy-2,5,5,8a-tetramethyldecahydro-1-naphthalenyl)methyl]-4-hydroxybenzoic acid, named dictyvaric acid on the basis of spectroscopic methods including IR, HRFABMS, 1D and 2D NMR techniques.

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Two new bromophenols were isolated from Rhodomela confervoides. Their structures were elucidated as 2, 2', 3-tribromo-3', 4, 4', 5-tetrahydroxy-6'-hydroxymethyldiphenylmethane and 2, 2', 3-tribromo-3', 4, 4', 5-tetrahydroxy-6'-ethyloxymethyldiphenylmethane by spectroscopic methods including IR, HREIMS, 1D and 2D NMR techniques.

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A new poly brominated dibenzylphenol named as rhodomevoidin was isolated from Rhodomela confervoides. Its structrue was elucidated as 3-bromo-4, 5-bis (2, 3-dibromo-4, 5-dihydroxybenzyI)pyrocatechol by spectroscopic methods including IR, HRFABMS, 1D and 2D NMR techniques.

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Chemical investigation of the ethanol extract of the marine green alga Chaetomorpha basiretorsa Setchell led to the isolation of a new sterol stigmast-4,28-dien-3 alpha 6 beta-diol 1 in addition to the five known sterols of beta-lawsaritol 2, saringosterol 3, 24-hydroperoxy-24-vinyl - cholesterol 4, beta-stigmasterol 5, 29-hydroxystigmasta-5, 24(28) -dien-3 beta-ol 6. Compounds were isolated by normal phase silica gel and Sephadex LH - 20 gel colum chromatography, reverse phase HPLC and recrystalization. Their structures were elucidated by spectroscopic methods including MS, IR 1D/2D NMR and X-ray analysis. Cytotoxicity of compounds was screened by using the standard WIT method. All these compounds were isolated from the green alga Chaetomorpha basiretorsa Setchell for the first time and they were inactive (50% inhibitory concentration was greater than 10 mu g /cm(3)) against KB, Bel -7402, PC - 3M, Ketr 3 and MCF - 7 cell lines.

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Eight compounds were isolated from red alga Gymnogongrus flabelliformis Harv. In normal phase silica gel, Sephadex LH-20 gel column chromatography, reverse phase HPLC, and recrystallization. Based on MS and 1D NMR spectroscopic data, their structures were determined as: stigmast-4-en-3-one (I), cholest-4-en-3-one (II), cholesterol (III), uracil (IV), uridine (V), adenosine (VI), succinic acid (VII), and 5-hydroxy-4-methyl-5-pentyl-2,5-dihydro-furan-2-on (VIII). All of them were obtained from this species for the first time. Cytotoxicity of these compounds was screened using standard MTT method, but all the compounds were inactive (IC50 > 10 mu g/ml).

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Two new norisoprenoid derivatives have been isolated from the red alga Gymnogongrus flabelliformis. Their structures were elucidated as (3R, 6R, 7E)-(+)-3-O-phenylacetyl-4,7-megastigmadiene-9-one and (3R,7E)-(-)-3-O-phenylacetyl-5,7-megastigmadiene-9-one, respectively, by spectroscopic methods including HRMS, 1D and 2D NMR techniques.

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通过对青海省8个农气观测站的土壤表面始冻期和解冻期连续观测资料的分析,结果表明:青海各地土壤表面始冻期和解冻期存在着明显的地域差异,多数站点的封冻期呈现出缩短的趋势,互助、德令哈略有延长.始冻期变化受气候变化的明显影响,当3-9月平均气温升高1℃,除贵德、诺木洪、互助站响应不明显外,其余站点的始冻期推迟1.5~7.5d,平均推迟2.3d;当3-9月日照时数增多10h,诺木洪地区始冻期提早0.5d,其余站点的响应不明显;当上年10月至当年2月平均气温升高1℃,除门源、德令哈站的解冻期响应不明显外,其余站点提前2~13d,平均提早2.5d;降水量增多10mm,除诺木洪推迟12d,其余站点推迟2~6d,平均推迟2.3d;当上年10月至当年2月平均气温升高1℃,封冻期日数除河南、门源、贵德响应不明显外,其余缩短2.4~23.1d,平均缩短1.8d.

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目的研究藏药大果大戟Euphorbia wallichii丙酮提取物中的化学成分。方法用溶剂提取,常规硅胶柱色谱分离和葡聚糖凝胶Sephadex LH-20纯化,采用化学方法和现代波谱分析技术(包括IR,HRESIMS,HRSIMS,1D和2DNMR等)鉴定其化学结构。结果从青海产大果大戟根的丙酮提取物中分离得到6个化合物,分别鉴定为:羊毛甾醇(lanosterol,Ⅰ)、巨大戟二萜-20-肉豆蔻酸酯(ingenol-20-myristinate,Ⅱ)、巨大戟二萜-3-肉豆蔻酸酯(ingenol-3-myristinate,Ⅲ)、没食子酸(gallicacid,Ⅳ)、1-O-a-L-阿拉伯糖-(1→6)-β-D-葡萄糖苷-3,7-二甲基-2-烯-7-羟基-辛醇(1-O-a-L-arabinofuranosyl-(1→6)-β-D-glucopyranosyl-3,7-dimethyl-oct-2-en-7-ol,Ⅴ)、1-O-没食子酰葡萄糖苷(1-O-galloyl-β-D-glucose,Ⅵ)。结论巨大戟烷型二萜酯类化合物Ⅱ和Ⅲ为新化合物,其他化合物均为首次从该植物中分离得到,单萜二糖苷类化合物Ⅴ系首次在该属中发现。

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利用硅胶柱层析、Sephadex LH-20和MCI等分离和纯化手段,从产于青海的菊科风毛菊属植物尖苞雪莲的全草中,分离得到5个化合物,经IR、NMR(1D、2D)、MS等现代波谱技术鉴定它们为芦丁、槲皮素-5-O-β-D-葡萄糖苷、丁香苷、胡萝卜苷和β-谷甾醇,其化学成分为首次报道。

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在自然生长状态下 ,用测定在黄头鹡鸰(Motacillacitreola)成鸟产卵期性腺及输卵管蛋的质量变化的方法 ,研究了它们在产卵期间的能量投入及其分配形式 .产卵期 ,雌鸟用于性腺增长和卵形成的能量预算为 6 6 2 4~71 19kJ ,其中用于蛋白质和脂肪的能量分别为 40 42kJ和 2 5 82~ 30 78kJ,占总能量预算的 5 6 8%~ 6 1 0 %和36 3%~ 46 5 % .用于繁殖蛋白的能量分配为 :输卵管 2 77kJ ,卵黄蛋白 12 80kJ ,卵白蛋白 2 4 85kJ.雌鸟耗能最大的是第 0d~ +1d ,达 (13 2 8~ 14 2 6 )kJ/d .产卵期雄鸟耗能 (用于性腺增长 ) 7 98kJ,雌雄亲鸟用于卵的形成和性腺增长共投入能量 74 2 2~ 79 17kJ.雌鸟耗能为雄鸟的 8 3倍~ 8 9倍。

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在黄头鹡鸰(Motacillacitreola)自然生长状态下 ,通过测定雏鸟气体代谢和身体组织能量积累的方法 ,研究了它们在生长期间的能量投入 .最小能量投入在 0~ 1d (d为日龄 ,用t表示 ) ,为 10 82kJ/d . 1只雏鸟需要能量为 414 2 6kJ,其中生产能为 15 3 14kJ,用于维持的能量是 2 6 1 12kJ .

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用脉冲调制荧光仪观测了珊瑚树叶片叶绿素荧光非光化学猝灭(qE)的日变化和季节变化后发现:在晴天,qE及其慢弛豫组分(qE-slow)随着光强的增加而升高,中午达最高值,之后随光强的减弱而下降;阴天时,这两个指标的日变化不明显。在不同季节,相同日时间和同一光照强度下测定珊瑚树叶片的qE和qE-slow,两个指标在冬季明显高于春、秋两季;在短时间(1d)内改变强光下的叶片周围的温度,叶片的qE和qE-slow在高温和低温下均高于过温下测定的结果。

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A new phenyl glycoside, 2-(3'-O-beta-D-glucopyranosyl) benzoyloxygentisic acid (1), along with seven known glycosides 2-8 was isolated from Tibetan herbal medicine Lomatogonium rotatum. The structures of the compounds were elucidated by spectroscopic methods including 1D and 2D NMR techniques and MS data.

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针对室内场景双目立体匹配有别于一般场景立体匹配的特殊性,提出了一种计算简便、准确度高的立体图像匹配算法。该算法首先利用canny算子检测物体的边缘,根据边缘的线性不变矩寻找出目标物体,然后提取出目标物体轮廓的特征点,利用角度直方图计算出左右图像的旋转角度,最后利用角度向量实现左右图像的对应像素点的匹配。线性不变矩有效地将计算复杂度由二维降低到一维,大大降低了计算量。角度向量的提出降低了特征点匹配的复杂度,而且计算简便,准确率高。实验表明,该算法对图像的缩放、旋转、平移均免疫,具有较高的识别精度和良好的抗干扰性,计算效率高于传统方法,有着较高的应用价值。

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随着移动机器人应用范围的日益扩展,在动态、非结构化环境下提高其自主导航能力已经成为移动机器人研究领域迫切需要解决的问题。在机器人自主导航关键技术中,识别技术是最难解决、也是最急需解决的问题。视觉作为导航中的重要传感器,与其他传感器相比具有信息量大、重量轻便、功耗低等诸多优势,因此基于视觉的识别技术也被公认为最具潜力的研究方向。 本文以国防基础研究项目和中科院开放实验室基金项目为依托,以沈阳自动化所自主研发的“轮腿复合结构机器人”和“无人机”为实验平台,针对地面自主机器人和无人机自主导航中迫切需要解决的应用问题,有针对性的展开研究,旨在提高移动机器人在动态、非结构化环境下的适应能力。 本论文的主要内容如下: 首先,为了提高复杂环境下地面移动机器人的自主能力,本文提出了一种基于立体视觉的面向室外非结构化环境障碍物检测算法。文中首先给出了一种可以从V视差图(V-disparity image)中有效估计地面主视差(Main Ground Disparity, MGD)的方法。随后,我们利用由粗到精逐步判断的方式,来识别疑似障碍和最终障碍并对障碍进行定位。最后,该方法已在地面自主移动平台得到实际应用。通过在各种场景下的实验,验证了该方法的准确性和快速性。 其次,以无人机天际线识别为背景,提出了一种准确、实时的天际线识别算法,并由此估计姿态角。通过对天际线建立能量泛函模型,利用变分原理推出相应偏微分方程。在实际应用中出于对实时性的考虑,引入分段直线约束对该模型进行简化,然后利用由粗到精的思想识别天际线。具体做法是:首先,对图像预处理并垂直剖分,然后利用简化的水平直线模型对天际线进行粗识别,通过拟合获得天际线粗识别结果,最后在基于梯度和区域混合开曲线模型约束下精确识别天际线,并由此估计无人机滚动和俯仰姿态角。 第三,通过对红外机场跑道的目标特性进行分析,文中设计了一种新的基于1D Haar 小波的并行的红外图像分割算法的;然后,有针对性的对分割区域提取特征;最后,两种常用的识别方法,支持向量机(SVM)和投票法(Voting)被用于对疑似目标区域进行分类和识别。通过对实际视频和红外仿真图片的测试,验证了本文算法的快速性、可靠性和实时性,该算法每帧平均处理时间为30ms。 最后,针对无人机空中巡逻中对人群进行自动监控所遇到的问题,通过将此类问题简化为固定视角下人流密度监测问题,提出了一种全新的基于速度场估计的越线人流计数和区域内人流密度估计算法。 首先,该算法把越线的人流当成运动的流场,给出了一种有效估计1D速度场的运动估计模型;然后,通过对动态人流进行速度估计和积分,将越线人流的拼接成动态区域;最后,对各个动态区域提取面积和边缘信息,利用回归分析实现对人流密度估计。该方法与以往基于场景学习的方法不同,本文是一种基于角度的学习,因此便于实际应用。