863 resultados para Propiedades Mecânicas
Resumo:
Tesis, Univ. Central (Madrid), Facultad de Ciencias, 1865.
Resumo:
Mode of access: Internet.
Resumo:
Tesis Universidad Central, 1857.
Resumo:
Mode of access: Internet.
Resumo:
Currently, there is a great search for materials derived from renewable sources. The vegetable fibers as reinforcement for polymer matrixes, has been used as an alternative to replace synthetic fibres, being biodegradable and of low cost. The present work aims to develop a composite material with epoxy resin reinforced with curauá fibre with the addition of alumina trihydrate (aluminum hydroxide, Al(OH)3) as a flame retardant, which was used in proportions of 10 %, 20% and 30% of the total volume of the composite. The curauá fibers have gone through a cleaning process with an alkaline bath of sodium hydroxide (NaOH ), parallelized by hand and cut carding according to the default length . They were molded composites with fibers 30cm. Composites were molded in a Lossy Mold with unidirectional fibres in the proportion of 20% of the total volume of the composite. The composites were prepared in the Chemical Processing Laboratory of the Textile Engineering Department at UFRN. To measure the performance of the material, tests for the resistance to traction and flexion were carried out. with samples that were later analyzed in the Electronic Microscopy Apparatus (SEM ). The composites showed good mechanical properties by the addition of flame retardant and in some cases, leaving the composite more vulnerable to breakage. These mechanical results were analyzed by chi-square statistical test at the 5% significance level to check for possible differences between the composite groups. Flammability testing was conducted based on the standard Underwriters Laboratory 94 and the material showed a satisfactory result taking their average burn rate (mm / min) decreasing with increasing addition of the flame retardant composite.
Resumo:
Composites based on alumina (Al2O3), tungsten carbide (WC) and cobalt (Co) exhibit specific properties such as low density, high oxidation resistance, high melting point and high chemical inertia. That composite shows to be a promising material for application in various fields of engineering. In this work, the mechanical properties of the composite (Al2O3 – WC – Co), particularly density and hardness, were evaluated according to the effects of the variables of powder processing parameters, green compact and sintered. Powder composites with the composition of 80 wt% Al2O3, 18 wt% WC and 2 wt% Co were processed by high energy ball milling in a planetary mill for 50 hours as well as mixed by manual mixing in a glass vessel with the same proportion. Samples were collected (2, 10, 20, 30, 40 and 50 hours) during the milling process. Then, the powders were compacted in a cylindrical die with 5 mm in diameter in a uniaxial press with pressures of 200 and 400 MPa. The sintering was in two stages: first, the solid phase sintering was performed at 1126 and 1300 °C for 1 hour with a heating rate of 10 °C/min in a resistive furnace under argon atmosphere for green samples compacted in 200 and 400 MPa; the second sintering was performed on dilatometer in solid phase at 1300 °C for green sample compacted in 200 MPa, another sintering also was performed on dilatometer, this time in liquid phase at 1550 °C for green samples compacted in 200 and 400 MPa, with the same parameters used in resistive furnace. The raw materials were characterized by X – ray diffraction (XRD), X – ray fluorescence (XRF), scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS) and laser particlemeter. The sintered samples were subjected to microhardness testing. The results showed that high energy milling achieved to the objectives regarding the particle size and the dispersion of composite phases. However, the hardness did not achieve to significant results, this is an indication that the composite has low fracture toughness.
Resumo:
Composites based on alumina (Al2O3), tungsten carbide (WC) and cobalt (Co) exhibit specific properties such as low density, high oxidation resistance, high melting point and high chemical inertia. That composite shows to be a promising material for application in various fields of engineering. In this work, the mechanical properties of the composite (Al2O3 – WC – Co), particularly density and hardness, were evaluated according to the effects of the variables of powder processing parameters, green compact and sintered. Powder composites with the composition of 80 wt% Al2O3, 18 wt% WC and 2 wt% Co were processed by high energy ball milling in a planetary mill for 50 hours as well as mixed by manual mixing in a glass vessel with the same proportion. Samples were collected (2, 10, 20, 30, 40 and 50 hours) during the milling process. Then, the powders were compacted in a cylindrical die with 5 mm in diameter in a uniaxial press with pressures of 200 and 400 MPa. The sintering was in two stages: first, the solid phase sintering was performed at 1126 and 1300 °C for 1 hour with a heating rate of 10 °C/min in a resistive furnace under argon atmosphere for green samples compacted in 200 and 400 MPa; the second sintering was performed on dilatometer in solid phase at 1300 °C for green sample compacted in 200 MPa, another sintering also was performed on dilatometer, this time in liquid phase at 1550 °C for green samples compacted in 200 and 400 MPa, with the same parameters used in resistive furnace. The raw materials were characterized by X – ray diffraction (XRD), X – ray fluorescence (XRF), scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS) and laser particlemeter. The sintered samples were subjected to microhardness testing. The results showed that high energy milling achieved to the objectives regarding the particle size and the dispersion of composite phases. However, the hardness did not achieve to significant results, this is an indication that the composite has low fracture toughness.
Resumo:
As the degraded products of chitosan, chitooligosaccharides (COS) have recently been produced by several methods, such as enzymatic an acidic hydrolysis. Chitosans are a family of biocompatible and biodegradable biopolymers obtained by N-deacetylation of chitin, the most abundant natural polymer after cellulose, consisting of two monomeric units, N-acetyl-2- amino-2-deoxi-D-glucose (A units) and 2-amino-2-deoxi-D-glucose (D units) linked by β (1→4) links. The degraded products COS, have a smaller molecular weight and therefore have better solubility and lower viscosity under physiological conditions because of shorter chain lengths and free amino groups in D-glucosamine units. The study of COS has been increasing not only because they come from a natural source, but also because of their biological compatibility and effectiveness. There are numerous reports on the biological activities of COS and their potential applications in food industry, pharmacy, agricultural or biomedicine. Nevertheless, in these studies it is difficult to find well defined COS in terms of physicochemical parametres, because these samples are usually poorly characterized. This makes it difficult to compare the results and to understand their mecanism of action. Degradation of the O-glycosidic linkages of chitosan by different methods, results in COS with different numbers and sequences of A and D units as well as different degrees of polymerisation (DP). Over the past few years, several technological approaches have been taken in preparing COS, including acid hydrolysis or enzymatic methods, among others. Therefore, in order to obtain COS with different physicochemical properties, different preparation methods of COS have been developed in this work. Then, the study of the relationship between physicochemical properties of these COS and their biological activities such as natural antioxidants, antibacterial agents, mucoadhesive and anti-inflammatory effects have been studied...
Resumo:
Las mecánicas patrimoniales se han basado tradicionalmente en factores racionales, marginando aquellos de carácter más emotivo o relacional. Además, en los últimos tiempos el sesgo economicista las ha obligado a buscar la rentabilidad y participar en el juego de la oferta y la demanda, con unos resultados muy poco esperanzadores. Cambiar ese estado de cosas pasa por cambiar radicalmente las estrategias puestas en marcha, basarse en la interlocución, conocer las relaciones entre el patrimonio y los colectivos sociales y, sobre todo, cambiar nuestra manera de pensar en el patrimonio.
Resumo:
Las Tecnologías de la Información y las Comunicaciones (TICs) y la WWW deben ser una fuente de oportunidades para la integración, el aprendizaje, el empleo y no un conjunto de nuevas barreras que aumente la exclusión y la discriminación. Aplicando herramientas de evaluación es posible identificar y revertir estas barreras en productos existentes, propiciando el acceso y la interacción a las personas, independientemente de sus capacidades diferentes y/o especiales. Pero el desafío real es aportar a un escenario más proactivo, que tenga en cuenta estas barreras al momento de concebir y desarrollar nuevos sitios y aplicaciones. Enfocados en personas con discapacidad motora y/o cognitiva y considerando estándares nacionales e internacionales vigentes, en este trabajo se realiza un análisis de los problemas que enfrenta este grupo crítico de usuarios de interés para comunicarse con los demás y el mundo que los rodea, y cómo pueden contribuir a esta comunicación la tecnología y la Web. La identificación de barreras se utiliza para proponer el diseño de sistemas Web personalizados de comunicación aumentativo y alternativo, que puedan enriquecerse dentro de una comunidad, compartiendo pictogramas descriptivos en un entorno de interacción usable y accesible.
Resumo:
El objetivo fue analizar las propiedades psicométricas del Sexuality and the Mental Retardation Attitude Inventory (SMRAI) en una muestra de 144 estudiantes universitarios de la carrera de psicología de una universidad privada de Lima Metropolitana, del 2do al 9no ciclo, de los cuales 44 fueron varones (30.6%) y 100 mujeres (69.4%), con edades comprendidas entre 17 y 43 años (M: 21.9). El análisis factorial confirmatorio realizado revela que dicha prueba presenta una estructura de dos factores con índices de ajuste adecuados. Por otro lado, con relación a la confiabilidad del constructo mediante el coeficiente Rho se obtuvo un indicador de .80. Se concluye que la SMRAI cuenta con propiedades psicométricas adecuadas para implementarlo en estudios orientados a conocer más facetas de las actitudes hacia la sexualidad de las personas con discapacidad intelectual.
Resumo:
El instrumento ADHD Rating Scale IV (ADHD RS IV) es un cuestionario de 18 ítems que permite valorar el déficit de atención, la hiperactividad e impulsividad que conforman el trastorno por déficit de atención con hiperactividad (TDAH). El aporte del presente estudio a la línea de investigación del TDAH se basa en el análisis de las propiedades psicométricas del instrumento en una adaptación en formato de auto-reporte, además, se trata de un estudio no realizado previamente en el contexto ecuatoriano.