电感耦合等离子体原子发射光谱法分析稀土元素的研究(Ⅰ)高纯氧化镧中十四种稀土杂质的测定

研究了ICP-AES法测定高纯氧化镧中十四种稀土杂质的方法。利用简单的加热去溶装置成功地测定了99.99％La_2O_3中14种稀土杂质。10mg/ml La_2O_3基体工作曲线下限为(以氧化物百分含量计算)Ce、Pr、Sm_2×10~(-3);Gd、Tb1×10~(-3);Nd,Lu 8×10~(-4),Er,Ho,Dy4×10~(-4); Tm.Eu 2×10~(-4),Yb 8×10~(-5),Y_4×~(-5)。相对标准偏差为2.8—9.7,回收率为85—114％。

控制气氛光谱法测定纯氧化钬中14个稀土杂质元素

本文介绍的是:使溶液干渣样品在Ar/O_2气氛中交流电弧激发,以基体钬为内标,测定高纯氧化钬中微量稀土杂质。其被测元素的测定下限是:铕、镱和钇各为0.0004％,镧、钐、铒,镝和铥各为0.0016％,铈、钕、钆和铽各为0.0031％,镨和镥各为0.0063％,相对标准偏差均小于7.1％。

Cytoglobosins A-G, Cytochalasans from a Marine-Derived Endophytic Fungus, Chaetomium globosum QEN-14

Financial support from the Ministry of Science and Technology of China (2010CB833802 and 2007AA09Z446) and from the National Science Foundation of China (30910103914) is gratefully acknowledged.

Programmed cell death in Laminaria japonica (Phaeophyta) tissues infected with alginic acid decomposing bacterium

TdT-mediated dUTP-biotin nick end labeling (TUNEL) is a sensitive and valid method for detecting DNA cleavage in programmed cell death (PCD). Using this method, DNA cleavage was observed in Laminaria japonica sporophytic tissues, which were infected with alginic acid decomposing bacterium. It was found that DNA cleavage occurred 5 min after the infection, the fragments with 3'-OH groups of cleaved nuclear DNA increased with time of infection and spread from the infection site. Although no typical DNA ladder (200 bp/ 180 bp) was detected by routine agarose gel electrophoresis, the cleavage of nuclear DNA fragments of 97 similar to 48.5 kb could be detected by pulsed field gel electrophoresis (PFGE). By using CaspGLOW(TM) fluorescein active caspase-3 staining method, caspase-3 activity has been detected in response to the infection of alginic acid decomposing bacterium. Our results are similar to the observations in hypersensitive response (HR) of higher plant, suggesting that the rapid cell death of L. japonica infected by alginic acid decomposing bacterium might be involved in PCD, and indicating that the occurrence of PCD is an active defense process against the pathogen's infection.

Cloning and sequencing of the phycocyanin gene from Spirulina maxima and its evolutionary analysis (vol 14, pg 307, 2002)

The geneswere cloned for the two apoprotein subunits, alpha and beta, of phycocyanin from the cyanobacterium Spirulina maxima (=Arthrospira maxima) strain F3. The alpha- and beta-subunit gene-coding regions contain 489 bp and 519 bp, respectively. The beta-subunit gene is upstream from the alpha-subunit gene, with a 111-bp segment separating them. Similarities between the alpha-subunits of S. maxima and nine other cyanobacteria were between 58% and 99%, as were those between the beta-subunits. The maximum similarity between the alpha- and beta-subunits from S. maxima was 27%.

海北高寒草甸生态系统实验站地区的土地覆盖动态变化研究

利用1987和2001年TM卫星遥感数据,在GIS的支持下对海北站土地覆盖变化进行了监测,14年来该区耕地面积增加迅速,高覆盖天然草地面积减少,中、低覆盖天然草地面积增加,湖泊、湿地萎缩,裸岩、沙地、裸土面积扩张,荒漠化程度加剧。

10-14岁超常儿童的亲社会行为特点及影响因素

Is prosocial behavior of supernormal children distinguished from normal children? Is there any difference between the supernormal children’s prosocial behavior from different educational placement? What are the mechanisms underlying the difference? The aim of this study was to examine these issues. With multiple methods of prosocial behavior, including other-rating, self-rating and hypothetical dilemma, we investigated the 10 to 14 year-old children. Firstly, the development of prosocial behavior and its relationship with prosocial behavior was examined. Secondly, we investigated the features of supernormal children’s prosocial behavior and analysed its difference with normal children. Finally, we tried to find the difference of supernormal children’s prosocial behaviour from different educational placement, and the mechanisms underlying the difference, such as social value orientation and peer relation. The results are as follows: 1)The altruistic and compliant prosocial tendency of 14 year-old children was obviously lower than those younger children. Intelligence was positively related with altruistic and emotional prosocial tendency for 10 year-olds, and with prosocial behaviour of peer nominated for 12 year-olds. 2)There was no significant difference of prosocial behaviour between supernormal and normal children. The peer nominated prosocial behaviour of 12 year-old supernormal children was higher than of 11 and 13 years old supernormal children. In addition, girls’ other-rating prosocial behaviour was significantly higher than boys’, but no gender difference was detected in the prosocial behaviour of self-rating and hypothetical dilemma. 3)With regard to the supernormal children’s prosocial behaviour in different educational placement, we found that the prosocial degree of the supernormal children of homogeneous groups was higher than that of heterogeneous groups in the role-change of ultimatum game. 4)The supernormal children from different educational placement had different social value orientation. More supernormal children of homogeneous groups belonged to the type of group enhancement, while more supernormal children of heterogeneous groups belonged to the type of equality. The types of social value orientation did not have impact on the supernormal children’s prosocial behaviour from different educational placement. 5)Peer relation moderated the impact of different educational placement on supernormal children’s prosocial behaviour.

Genômica e proteômica de Anaplasma marginale: contribuições para o controle da riquétsia.

A anaplasmose bovina é causada pela riquétsia intra-eritrocítica Anaplasma marginale, responsável por importantes prejuízos econômicos, por causa da alta morbidade e mortalidade em rebanhos bovinos suscetíveis. A vacinação tem sido uma forma econômica e eficiente de controlar a enfermidade. No entanto, os métodos de imunização tradicionais apresentam efeitos adversos em algumas categorias de animais. Nas últimas décadas, os estudos sobre imunização contra Anaplasma concentraram-se nas proteínas de superfície MSP1a, 1b, 2, 3, 4 e 5. No entanto, até o momento, os resultados foram pouco promissores, apontando a necessidade de ampliar o conhecimento sobre o rol das proteínas de membrana da riquétsia e das relações estruturais entre elas. Nesse contexto, os estudos do genoma e do proteoma da riquétsia têm contribuído com essa finalidade. Pela análise genômica, 14 genes para novas proteínas de membrana externa foram identificados (omp 1-14), dentre os quais, omp2, 3 e 6 não são transcritos. Esses genes ostraram-se altamente conservados entre isolados da riquétsia. As proteínas OMP4, 7, 10 e 14 foram reconhecidas por soros de bovinos imunizados com membrana de A. marginale, mostrando potencial para desenvolvimento de imunógenos. Além disso, mediante análise proteômica, foi possível detectar novas proteínas de membrana, negligenciadas pela anotação genômica. Dentre elas estão AM097 - conjugal transfer protein, AM956 - PepA citosol amino peptidase, AM254 - fator de elongação Tu e quatro proteínas de função desconhecida: AM127, 197, 387 e 854, as quais também foram reconhecidas por soros de bovinos imunizados com membrana de A. marginale.

Trajectory Mapping ("TM''): A New Non-Metric Scaling Technique

Trajectory Mapping "TM'' is a new scaling technique designed to recover the parameterizations, axes, and paths used to traverse a feature space. Unlike Multidimensional Scaling (MDS), there is no assumption that the space is homogenous or metric. Although some metric ordering information is obtained with TM, the main output is the feature parameterizations that partition the given domain of object samples into different categories. Following an introductory example, the technique is further illustrated using first a set of colors and then a collection of textures taken from Brodatz (1966).

Keeping Secrets in Hardware: the Microsoft Xbox(TM) Case Study

This paper discusses the hardware foundations of the cryptosystem employed by the Xbox(TM) video game console from Microsoft. A secret boot block overlay is buried within a system ASIC. This secret boot block decrypts and verifies portions of an external FLASH-type ROM. The presence of the secret boot block is camouflaged by a decoy boot block in the external ROM. The code contained within the secret boot block is transferred to the CPU in the clear over a set of high-speed busses where it can be extracted using simple custom hardware. The paper concludes with recommendations for improving the Xbox security system. One lesson of this study is that the use of a high-performance bus alone is not a sufficient security measure, given the advent of inexpensive, fast rapid prototyping services and high-performance FPGAs.

Mapeamento e descrição do padráo de uso e cobertura da terra em municípios do sudoeste goiano a partir de imagens orbitais TM/Landsat-5.

A partir dos anos 1970, a ocupação pelo homem do espaço do centro-oeste brasileiro apresentou um elevado crescimento devido a políticas de expansão agrícola. Este fato ocorreu por meio do alto grau de mecanização agrícola e aplicação de fertilizantes, visando elevados níveis de produção em diversas localidades, como o sudoeste do Estado de Goiás. Tal predicado da alta produtividade mantém-se até os dias atuais, indicando a grande intensidade da dinâmica de uso e cobertura das terras nesta região. Desta forma, tornase necessário o conhecimento da dinâmica e distribuição espacial dos padrões de uso e cobertura da terra, podendo fornecer subsídios a ações de planejamento agrícola sobre o espaço em alguns municípios do sudoeste goiano. Para isto, imagens orbitais do satélite Landsat TM-5 foram adquiridas em diferentes períodos do ciclo agrícola ao longo de 2007. Informações complementares acerca do uso regional foram utilizadas para apoiar a interpretação e classificação, principalmente a partir dos dados obtidos em campo. Os mapas de uso e cobertura da terra para os municípios de Rio Verde, Acreúna, Santo Antônio da Barra, Santa Helena de Goiás, Montividiu e Paraúna foram obtidos utilizando ferramentas do programa Spring 4.3.3 como a segmentação de imagens, bem como o classificador semi-automático Bhattacharya Distance, sendo estabelecidas dez classes temáticas, com base na legenda proposta pelo IBGE e Corine. A análise multitemporal, assim como a segmentação mostraram-se eficientes na distinção das classes de uso e cobertura da terra da região. A classe de uso destinada ao plantio da soja apresentou o maior percentual da área, mudando para culturas safrinha, solo exposto ou pousio no inverno. Outras classes também merecem destaque como a Pastagem e a Cana-de-açúcar, que apresentaram distribuição espacial bastante concentrada. Este mapeamento fornece subsídios ao planejamento do uso e ocupação das terras na região, considerando os aspectos ambientais e sociais, assegurando maior produtividade agrícola, visando um manejo sustentável das terras e a qualidade de vida ao homem do campo.

Custo médio de produção de suínos para abate: anexo 14 - dezembro/83.

1983