Multivariate Development and Validation of a Stability-Indicating HPLC Method for the Determination of Glimepiride in Tablets

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Cádmio em Latossolo Vermelho cultivado com milho em colunas: mobilidade e biodisponibilidade

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Impact of the Textile Dye Acid Blue 40 on the Periphyton of a Simulated Microecosystem

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Analises paramétricas de colunas granulares encamisadas com tecido geossintético através de software Ringtrac

This study attempts a preliminary assessment of the behavior of a soil improvement system with the use of encased columns of granular material with geosynthetic (columns Ringtrac ® ). This evaluation was performed using the software Ringtrac ® (developed by Huesker GmbH, Germany), which required different parameters such as soil Oedometric Module, friction angle of soil, thickness of soft soil and the embankment height .In each analysis, one parameter was varied and the other different parameters considered were fixed, resulting in a total of 726 results. Were considered valid only the results where the radial deformation of the geosynthetic encased column did not exceed the value of 4%, which is the maximum radial deformation of the geosynthetic adopted by the Ringtrac ® program. The analysis results are shown graphically in this study, evaluating the tension values in the column and obtained settlements in each analysis. It’s proven in this preliminary study that the variation of the soft soil friction angle in the Ringtrac ® column, will not significantly affect the values of strain on the tension in the column and settlements on the ground. Furthermore, the variation of Oedometric Module on the soil, will significantly affect the tension values in the column and the settlements in the soil

Entre o acadêmico e o jornalístico: análise da coluna de crítica literária Prosa de Sábado, do suplemento Sabático

The literary criticism was developed in Brazil in the period that comprehends the end of the 19th century and the beginning of the 20th century. During that time, the mean of dissemination of the criticism were the footnotes of the newspapers, places in which literature was discussed and the critics expressed their personal impressions about literary works with the objective of orientating the good taste of the readers. With the progressive evolution of journalism and of the newspaper's audience, the criticism columns became incompatible with the informative part of the periodicals, being transferred to the literary supplements, during a transition phase, until it was concentrated in the universitary field. This change in the paradigms of the production of criticism also caused a change in the profile of the literary critics and in the criteria to do the criticism. Before, if the critics were professionals that only needed to have enough erudition to judge the literary works, they turn into literature experts and need to use scientific methodologies in the literary analysis, while the cultural journalist begins to look at the events and literary works as products which belong to a market that needs to be reported. This research proposes studying and comparing the critics published in the column Prosa de Sábado, of the literary supplement Sabático, produced by Silviano Santiago, critic of an academic origin, and Sérgio Augusto, journalist critic, with the objective of identifying similarities and contrasts between them, and analyse the relation of this critics with their distinct fields of literary legitimation, as well as reflecting about the presence of the literary criticism and of the critics in the current press

Biotratamento de sacolas plásticas de supermercado

Supermarket plastic bags are produced by high density polyethylene (HDPE) and low density polyethylene (LDPE) resins. In Brazil, are produced annually around 150 plastic bags per capita. Disposed in landfills, the supermarket plastic bags prevent the passage of water by slowing the breakdown of biodegradable materials and hindering compaction of waste, according to their low degradability. This work investigated the biodegradation of PE bags containing additive oxo-biodegradable and bags without additives: buried in soil columns, exposed in a controlled environment and exposed to air. The analysis methods used to assess the changes brought in the bags with respect to microbial action and exposure time were weight loss, thickness measurement, infrared (FTIR), scanning electron microscopy (SEM) and contact angle. The results showed that the use of prodegradant agents such as oxobiodegradable additives in polyethylene bags, buried in soil for 270 days, was not efficient to accelerate the biodegradation by microorganisms. It seems that these additives have been more efficient to degrade the colored pigmentation of printed bags, under the influence of light and heat.

Associação entre posicionamento do aluno na sala de aula e desempenho escolar

This research was aimed at analyzing whether there is an association between the positioning of the pupil in the classroom and his academic performance, as well as to diagnose the main factors underlying the association. Thus, this study analyzed 4 Elementary School II institutions of both public and private educational systems, in Botucatu, São Paulo, Brazil during a school year bimester. To register the positions students were seated, 29 similar classes (containing 6 rows x 6 columns) were investigated, each one with around 30 students, which resulted in a sampling of 859 students. For the questionnaire application, which objective was to verify the main reason for students’ seat choice, the same 29 classes were investigated. However, the sampling number was reduced to 692 students. In turn, for the collection of school performance and absence percentage of each student for the bimester in question, teachers’ evaluation books were used. As a result, it was found that the lower the percentage of the student's absences, the greater is their performance at school, and the greater their performance at school is, the closer up front to the board they are seated. Finally, the closer up to the board they are seated, the more their motivation and interest in learning increase. Therefore, there is an association between the position of a student in the classroom and his or her academic performance, where the association is conditioned by the motivation and interest in learning

Caracterização da cinza de bagaço de cana-de-açúcar e aplicação no solo

Pós-graduação em Agronomia (Ciência do Solo) - FCAV

Aplicação de cinza de bagaço de cana-de-açúcar nos atributos químicos e biológicos do solo

Pós-graduação em Agronomia (Produção Vegetal) - FCAV

Aplicação e análise da utilização do software Eberick em um projeto residencial popular

Due to new technologies in civil engineering and the competition of the market, the demand for computer programs for the elaboration of structural projects of reinforced concrete is raising in a quick and efficient manner. This paper presents a study based on Eberick, a structural calculation software, and this software was applied to a low cost residence project. By performing structural calculation manually, it is possible to compare and analyze the criteria that Eberick uses for the design and detailing of structural elements like columns, beams and slabs. As the software functionality becomes clear, the engineer will use it careful and safely, exploring all of its resources and advantages

Avaliação da remoção de sulfametoxazol, diclofenaco e 17β-estradiol em águas por adsorção em carvão ativado granular

Pós-graduação em Engenharia Civil - FEIS

Double-setting alpha-tricalcium phosphate cement provided with interconection channels in rabbits after enucleation: a potential implant for the anophthalmic socket

The purpose of this study was to evaluate the macroscopy and microstructure of a double setting alpha-tricalcium phosphate bone cement sphere provided with interconnection channels (alpha-TCP-i), as well as the integration of the implant with the rabbits' orbital tissue, through macroscopic analysis and histopathology. The external and internal surfaces of the alpha-TCP-i were evaluated macroscopically and by electron microscopy. Twelve New Zealand rabbits received 12mm implants of alpha-TCP-i following enucleation of the left eye. The clinical assessment was undertaken daily during the first 15 days, followed by fortnightly assessment until the end of the study period. For the morphological analysis, exenteration was performed in 3 animals per experimental period (15, 45, 90 and 180 days). The external and internal surfaces of the implant appeared solid, smooth and compact, with six channels which interconnected centrally. The micro-architecture was characterized by the formation of columns of hexagonal crystals. No signs of infection, exposure, dehiscence of sutures or extrusion of the implant were noted in any of the animals during the entire period of the study. The morphological evaluation demonstrated the presence of a thin capsule around the implant, from whence appeared fibro-vascular projections, which penetrated it through the interconnecting channels. In the first days after the insertion of the implant, an intense inflammatory reaction was noted. At 180 days, however, there were no signs of inflammation. The alpha-tricalcium phosphate cement implant was well tolerated in this rabbit model and appeared to be relatively inert with some fibrovascular ingrowth through the large channels.

Atributos químicos da solução e do solo após aplicação de resíduo da extração de celulose

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Potencial de lixiviação de herbicidas utilizados na cana-de-açúcar em solos contrastantes

The increased use of herbicides, coupled with inadequate use of these molecules, also increased concerns about the risks of environmental contamination and its effects on humans and animals. The objective of this work evaluates the potential for leaching of herbicides in the crop of cane sugar, in contrasting soils. Used samples were used Psament (NR - sandy texture) and Oxisol Red (LR - clay texture). After application of herbicides ametryne (NR 1.60 kg ha(-1) and LR 2.40 kg ha(-1)), clomazone (NR 0.90 kg ha(-1) and LR 1.10 kg ha(-1)) and diuron (NR 1.60 kg ha(-1) and LR 3.20 kg ha(-1)), were irrigated blades of 0, 20, 40, 60, 80 and 100 mm of water in soil columns. Results indicate that ametryne in NR samples submitted to the handling layer of 5-10 cm when applied blades of 20 and 40 mm of water. It was evident that the clomazone, regardless of the soil, did not exceed 0-5 cm water depths of 0 to 20 mm of water and 5-10 cm deep in the blades above 40 mm of water. With blades up to 80 mm, the diuron leaching only in layers 0-5 cm deep in LR. Conclude that the potential of leaching of diuron and ametryne was influenced by soil texture together with the organic matter content, the same was not true for clomazone.

Influence of the Hall effect on convection in plasmas

The influence of the Hall effect on stationary convection in shearless current-carrying plasma columns is considered. It is shown that the Hall effect can inhibit the formation of convection cells generated by viscosity and resistivity.