Microwave-assisted hydrothermal synthesis of nanocrystalline SnO powders

Tin oxide (SnO) powders were obtained by the microwave-assisted hydrothermal synthesis technique using SnCl2 center dot 2H(2)O as a precursor. By changing the hydrothermal processing time, temperature, the type of mineralizing agent (NaOH, KOH or NH4 OH) and its concentration, SnO crystals having different sizes and morphologies could be achieved. The powders were characterized by X-ray diffraction (X-ray), Field Emission Scanning Electron Microscopy (FE-SEM), High Resolution Transmission Electron Microscopy (HR-TEM) and Selected Area Electron Diffraction (SAED). The results showed that plate-like form is the characteristic morphology of growth and the TEM analyses indicate the growth direction as (200). (c) 2007 Elsevier B.V. All rights reserved.

Comparison of proton energy loss in thick absorbers in terms of a reduced calibration curve

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Asymmetry of the Aharonov-Bohm diffraction pattern and Ehrenfests theorem

The electron-diffraction pattern for two slits with magnetic flux confined to an inaccessible region between them is calculated. The Aharonov-Bohm effect gives a diffraction pattern that is asymmetric but has a symmetric envelope. In general, both the expected displacement and the kinetic momentum of the electron are nonzero as a consequence of the asymmetry. Nevertheless, Ehrenfests theorems and the conservation of momentum are satisfied. © 1992 The American Physical Society.

Histochemical and ultrastructural cytochemistry of glycogen in ovarioles of Neoponera villosa ants (hymenoptera : ponerinae)

In Neoponera villosa ants, we found ovaries of the polytrophic meroistic type which is characterized by the presence of nurse cells forming together with the oocyte, the so-called follicles. The nurse cells have the primary function of supplying the oocyte with RNA, but they contribute to the supply of other elements such as glycogen. With the objetive of detecting the presence of this substance in the ovarioles of workers and queens of N. viillosa ants the ovaries were removed and processed according to electron microscopy technic for glycogen detection. Glycogen is a common element in insect oocytes and is abundantly distributed in the cytoplasm of N. villosa workers and queens. However, in ovarian follicles it can only be detected at stages II and III of development. Glycogen synthesis probably occurs predominantly in nurse cells which transfer it into the oocyte through the nourish pore. This process requires high energy expenditure that justify the large numbers of mitochondria associated with glycogen in the nurse cell cytoplasm. The amount of glycogen in the nurse cells of queens is slightly greater than workers.

Infrared finite solutions for the gluon propagator and the QCD vacuum energy

Nonperturbative infrared finite solutions for the gluon polarization tensor have been found, and the possibility that gluons may have a dynamically generated mass is supported by recent Monte Carlo simulation on the lattice. These solutions differ among themselves, due to different approximations performed when solving the Schwinger-Dyson equations for the gluon polarization tensor. Only approximations that minimize energy are meaningful, and, according to this, we compute an effective potential for composite operators as a function of these solutions in order to distinguish which one is selected by the vacuum. © 1997 Elsevier Science B.V.

Bounds on contact interactions from LEP1 data and high-Q2 HERA events

A contact four-fermion interaction between light quarks and electrons has been evoked as a possible explanation for the excess of events observed by HERA at high-Q2. We explore the 1-loop effects of such interaction in Γ(Z0 → e+e-) measured at LEP and impose strong bounds on the lower limit of the effective scale. Our results are able to discard some of the contact interactions as possible explanation for the HERA events. © 1997 Elsevier Science B.V.

Direct amorphous-to-cubic perovskite phase transformation for lead titanate

The phase evolution of lead titanate processed by the polymeric precursor method was investigated by thermal analysis, X-ray diffraction, and high-resolution transmission electron microscopy. The results showed that the cubic perovskite PbTiO3 (PT) phase is formed from an inorganic amorphous precursor at a temperature of 444 °C. A gradual transition from cubic to tetragonal perovskite PT was observed with the increase of calcination time at this temperature. HRTEM results showed that the cubic PT particles have a size of around 5 nm. The identification of cubic PT as an intermediate phase supports the hypothesis that the chemical homogeneity was kept at the molecular level during the synthesis process, with no cation segregation.

Surface amorphization in diamond turning of silicon crystal investigated by transmission electron microscopy

Silicon crystal exhibits a ductile regime during machining prior to the onset of fracture when appropriate cutting conditions are applied. The present study shows that the ductile regime is a result of a phase transformation which is indirectly evidenced by the amorphous phase detected in the machined surface. Transmission electron microscopy (TEM) planar view studies were successfully performed on monocrystalline silicon (1 0 0) single point diamond turned. TEM electron diffraction patterns show that the machined surface presents diffuse rings along with traces of crystalline material. This is attributed to crystalline silicon immersed in an amorphous matrix. Furthermore, only diffuse rings in the diffraction patterns of the ductile chip are detected, indicating that it is totally amorphous. © 2000 Elsevier Science B.V. All rights reserved.

Dynamical calculation of direct muon-transfer rates from thermalized muonic hydrogen to C6+ and O8+

Moun-transfer reactions from muonic hydrogen to carbon and oxygen nuclei employing a full quantum-mechanical few-body description of rearrangement scattering were studied by solving the Faddeev-Hahn-type equations using close-coupling approximation. The application of a close-coupling-type ansatz led to satisfactory results for direct muon-transfer reactions from muonic hydrogen to C6+ and O8+.

Constraining the free parameter of the high parton density effects

The high parton density effects are strongly dependent of the spatial gluon distribution within the proton, with radius R, which cannot be derived from perturbative QCD. In this paper we assume that the unitarity corrections are present in the HERA kinematical region and constrain the value of R using the data for the proton structure function and its slope. We obtain that the gluons are not distributed uniformly in the whole proton disc, but behave as concentrated in smaller regions. (C) 2000 Elsevier Science B.V.

Endocytic activity in the thrombocytes of the turtle Phrynopys hilarii (freshwater South American species)

The phagocytic process in cells depends on lysosomal enzymes, high-energy metabolism and cellular recognition. In this paper, we investigated the presence of energy and recognition factors in thrombocytes of turtle Phrynopys hilarii (a freshwater South American species). Turtle thrombocytes (P. hilarii) present glycogen - possibly β particles - dispersed in their cytoplasm and glycoproteins in the cell surface, as well as a large number of enzymes involved in the endocytic process (Pellizzon, 1996). The activity of these enzymes depends on high-energy metabolism and on cellular recognition provided by specific glycoconjugates (Alberts et al., 1994). This metabolic characterization is demonstrated by the large amount of glycogen particles observed in the cytoplasm by Thiéry's method. Glycogen labeling was also observed when concanavalin A-peroxidase was used as a marker for thrombocytes and for endocyted charcoal particles. Our results show that these cells have phagocytic ability, suggesting that their function in blood circulation is not limited to aggregation but may also involve a great potential for phagocytosis.

Coupled Bose-Einstein condensate: Collapse for attractive interaction

The collapse of trapped Boson-Einstein condensate (BEC) of atoms in states 1 and 2 was studied. When the interaction among the atoms in state i was attractive the component i of the condensate experienced collapse. When the interaction between an atom in state 1 and state 2 was attractive both components experienced collapse. The time-dependant Gross-Pitaevski (GP) equation was used to study the time evolution of the collapse. There was an alternate growth and decay in the number of particles experiencing collapse.

Exploring neutrino mixing with low energy superbeams

We explore the features of neutrino oscillation which are relevant for measurements of the leptonic CP violating phase δ and the sign of Delta;m13 2 in experiments with low-energy conventional superbeams. Toward the goal, we introduce a new powerful tool called the CP trajectory diagram in bi-probability space which allows us to represent pictorially the three effects, the effects of (a) genuine CP violation due to the sin δ term, (6) CP conserving cos δ term, and (c) fake CP violation due to earth matter, separately in a single diagram. By using the diagram, we observe that there is a two-fold ambiguity in the determination of S which is related with the sign of Delta;m13 2. Possible ways of resolving the ambiguity are discussed. In particular, we point out that an in situ simultaneous measurement of δ and the sign of Delta;m13 2 can be carried out at distances of about 700 km, or at the Phase II of the JHF experiment provided that sin δ ·Delta;m13 2 < 0, both with a megaton class water Cherenkov detector.

Energy and the AdS/CFT correspondence

We consider a scalar field theory on AdS in both minimally and non-minimally coupled cases. We show that there exist constraints which arise in the quantization of the scalar field theory on AdS which cannot be reproduced through the usual AdS/CFT prescription. We argue that the usual energy, defined through the stress-energy tensor, is not the natural one to be considered in the context of the AdS/CFT correspondence. We analyze a new definition of the energy which makes use of the Noether current corresponding to time displacements in global coordinates. We compute the new energy for Dirichlet, Neumann and mixed boundary conditions on the scalar field and for both the minimally and non-minimally coupled cases. Then, we perform the quantization of the scalar field theory on AdS showing that, for 'regular' and 'irregular' modes, the new energy is conserved, positive and finite. We show that the quantization gives rise, in a natural way, to a generalized AdS/CFT prescription which maps to the boundary all the information contained in the bulk. In particular, we show that the divergent local terms of the on-shell action contain information about the Legendre transformed generating functional, and that the new constraints for which the irregular modes propagate in the bulk are the same constraints for which such divergent local terms cancel out. In this situation, the addition of counterterms is not required. We also show that there exist particular cases for which the unitarity bound is reached, and the conformai dimension becomes independent of the effective mass. This phenomenon has no bulk counterpart.

Phytochrome and light influence on germination and vigor of ocimum gratissimum L. (Lamiaceae) seeds under high irradiance conditions

Ocimum gratissimum seed germination (% germination and vigor) has been found as phytochrome dependent, having a typical High Irradiant Response (HIR). Seven treatments were tested: daylight (DL), red (R), far-red (FR), blue (B), green (G), dark (DK), and reversible (RVB). No statistical difference among the DL, R, FR, B, and G were found. DK and RVB were statistically equal and presented the lowest results. The germination also occurred in the DK treatment but in non-useful rates, and it was nonreversible in the RVB treatment. It allows these seeds to be classified as positively photoblastic. The minimum energy need to initiate the germination was evaluated by a fluency-response curve. It plotted four different exposition times to R light (1 second, 60 seconds, 1 hour, and 13 hours) against percent germination. Useful germination occurred only after 1 hour, confirming the high energy needed to incite the process. The germination rate increased with the raise of the photoequilibrium (j). The high positive correlation index found confirms the phytochrome influence in this process. Facing all the results presented here, it is suggested to sow these seeds under direct and highly intense sunlight. It is preferable to avoid places exposed to variations in the shading, because inhibition induced by dense shade effects (low R/FR ration and consequently low j established) were demonstrated irreversible, and it can lead to undesirable loss of the germination power.