Efeito da microabrasão e do clareamento dental na rugosidade superficial e microdureza do esmalte dental: estudo longitudinal ‘in situ’

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Hot turning of a difficult-to-machine steel (sae xev-f) aided by infrared radiation

A possible way for increasing the cutting tool life can be achieved by heating the workpiece in order to diminish the shear stress of material and thus decrease the machining forces. In this study, quartz electrical resistances were set around the workpiece for heating it during the turning. In the tests, heat-resistant austenitic alloy steel was used, hardenable by precipitation, mainly used in combustion engine exhaustion valves, among other special applications for industry. The results showed that in the hot machining the cutting tool life can be increased by 340% for the highest cutting speed tested and had a reduction of 205% on workpiece surface roughness, accompanied by a force decrease in relation to conventional turning. In addition, the chips formed in hot turning exhibited a stronger tendency to continuous chip formation indicating less energy spent in material removal process. Microhardness tests performed in the workpieces subsurface layers at 5 m depth revealed slightly higher values in the hot machining than in conventional, showing a tendency toward the formation of compressive residual stress into plastically deformed layer. The hot turning also showed better performance than machining using cutting fluid. Since it is possible to avoid the use of cutting fluid, this machining method can be considered better for the environment and for the human health.

Martensite decomposition in Cu-Al-Mn-Ag alloys

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Effect of Ceramic Thickness and Shade on Mechanical Properties of a Resin Luting Agent

Purpose: This study aimed to investigate the influence of ceramic thickness and shade on the Knoop hardness and dynamic elastic modulus of a dual-cured resin cement.Materials and Methods: Six ceramic shades (Bleaching, A1, A2, A3, A3.5, B3) and two ceramic thicknesses (1 mm, 3 mm) were evaluated. Disk specimens (diameter: 7 mm; thickness: 2 mm) of the resin cement were light cured under a ceramic block. Light-cured specimens without the ceramic block at distances of 1 and 3mm were also produced. The Knoop hardness number (KHN), density, and dynamic Young's moduli were determined. Statistical analysis was conducted using ANOVA and a Tukey B rank order test (p = 0.05).Results: The bleaching 1-mm-thick group exhibited significantly higher dynamic Young's modulus. Lower dynamic Young's moduli were observed for the 3-mm-thick ceramic groups compared to bleaching 3-mm-thick group, and no difference was found among the other 3-mm groups. For the KHN, when A3.5 3-mm-thick was used, the KHN was significantly lower than bleaching and A1 1-mm-thick ceramic; however, no difference was exhibited between the thicknesses of the same shade.Conclusions: The dual-cured resin cement studied irradiated through the 1-mm-thick ceramic with the lightest shade (bleaching ceramic) exhibited a better elastic modulus, and there was no effect in KHN of the resin cement when light cured under different ceramic shades and thicknesses (1 and 3 mm), except when the A3.5 3-mm-thick ceramic was used.Clinical Significance: Variolink II irradiated through ceramic with the lowest chroma exhibited the highest elastic modulus; therefore, the light activation method might not be the same for all clinical situations.

Effect of Beverages and Mouthwashes on the Hardness of Polymers Used in Intraoral Prostheses

PurposeThe mechanical properties of acrylic resins used in intraoral prostheses may be altered by frequent exposure to liquids such as beverages and mouthwashes. This study aimed to evaluate the effect of thermocycling and liquid immersion on the hardness of four brands of acrylic resins commonly used in removable prostheses (Onda Cryl, QC-20, Classico, Lucitone).Materials and MethodsFor each brand of resin, seven specimens were immersed in each of six solutions (coffee, cola, red wine, Plax-Colgate, Listerine [LI], Oral B), and seven more were placed in artificial saliva (control). The hardness was tested using a microhardness tester before and after 5000 thermocycles and after 1, 3, 24, 48, and 96 hours of immersion. The results were analyzed using three-way repeated-measures ANOVA and Tukey's test (p < 0.05).ResultsThe hardness of the resins decreased following thermocycling and immersion in the solutions. Specimens immersed in cola and wine exhibited significant decreases in hardness after immersion for 96 hours, although the greatest significant decrease in hardness occurred in specimens immersed in LI. However, according to American Dental Association specification 12, the Knoop hardness of acrylic resins for intraoral prostheses should not be below 15. Thus, the median values of superficial hardness observed in most of the acrylic resins in this study are considered clinically acceptable.ConclusionsThe microhardness of polymers used for intraoral prostheses decreases following thermocycling. Among specimens immersed in beverages, those immersed in cola or wine experienced the greatest decrease in microhardness. Immersion of acrylic resins in LI significantly decreased the microhardness in relation to the initial value. Among the resins assessed, QC-20 exhibited the lowest initial hardness.

Caries progression and inhibition in human and bovine root dentine in situ

Since the use of bovine instead of human dentine to evaluate cariogenic and anticariogenic substances is not well established, this in situ study was conducted. Eleven volunteers wore palatal acrylic devices containing 4 dentine slabs (2 human and 2 bovine). Sucrose solution (20%) was dripped over all slabs 4 times a day, simulating a cariogenic challenge. Dentifrice slurries, fluoridated or not, were dripped over specified dentine slabs 3 times a day to evaluate caries reduction. After 14 days, the biofilm formed on the dentine slabs was collected for microbiological analysis. In dentine, mineral loss (DeltaZ) and lesion depth (LD) were determined by cross-sectional microhardness and by polarized light microscopy, respectively. The total streptococci and mutans streptococci counts in the biofilm formed either on human or on bovine slabs, whether treated or not with fluoride dentifrice, were not statistically different. The DeltaZ and the LID values of dentine treated with fluoride dentifrice were significantly lower than the values of dentine treated with non-fluoride dentifrice. The differences in the DeltaZ and LD values between the human and bovine dentine were not statistically significant. The results suggest that bovine dentine can be used instead of human to evaluate caries development and inhibition. Copyright (C) 2003 S. Karger AG, Basel.

Avaliação da tenacidade CHARPY-V de um tubo de aço API 5L X70 soldado com arco submerso

This research project focused primarily on assessing the impact toughness of the weld and the base material of a steel pipe API 5L X70 submerged arc welded, used to conduct remote oil and gas (linepipes). The analysis followed strictly the Specification for Line Pipe - API 5L Standard, regarding the removal of the specimens of regions-of-proof-long section of the pipe, at 90o and 180o from the welded joint, and mechanical properties of toughness and Charpy-V, both the joint welded as the base material. Specimens of steel tube supplied by Tenaris Confab-SA were sized for tensile and Charpy-V, according to ASTM E 8M and ASTM E23, respectively. The result obtained showed that the API X70 steel tube has high Charpy-V toughness, near to each other at both 90o and 180o from the welded joint of the tube, and both higher than the weld metal. Microstructural and microhardness analysis complemented the present study

Estudo do comportamento em fadiga de uma chapa de aço microligado, grau API 5L X70

In engineering, for correct designing the structural components required for cyclical stresses, it is necessary to determine a limit of resistance to fatigue, which is the maximum amplitude of the applied tension under which the fatigue failure does not occurs after a certain number cycles. The marine environment is hostile, not only by the high pressure, corrosion, but also by low temperatures. Petrol Production units, composed of the risers (pipelines connecting the oil well to the ship), are dimensioned to remain installed for periods of 20 up to 30 years, and must therefore be prepared to support various efforts, such as tidal, wind currents and everything that is related. This paper focuses on a study on the fatigue behavior of microalloyed steel, API 5L Grade X70, used to transport oil and gas by pipelines. For analysis, we obtained the curves S-N (stress vs. number of cycles) using laboratory data collected from cylindrical longitudinal and transverse specimens used in axial fatigue test in accordance with ASTM E466. The tensile tests and microhardness were performed to characterize the mechanical properties of the samples, and it was found that the values meet the specifications of the standard API 5L. To characterize microstructurally the material, it was also made a metallographic analysis of the steel under study, and the origin of the fatigue crack was investigated with the support of a scanning electron microscope (SEM).

Avaliação do comportamento mecânico sob deformação da liga Ti- 30Ta visando aplicações biomédicas

Titanium and its alloys have been used for biomedical applications due their excellent properties such as high corrosion resistance, biocompatibility and mechanical properites. In this study, microstructural and mechanical properties of Ti-30Ta alloy was evaluated during its processing. Ti-30Ta alloy ingots were produced from sheets of commercially pure titanium (99.9%) and tantalum (99.9%). Its melting was realized in arc melting furnace in an argon atmosphere. After homogenizing at 1200ºC, ingots were cold worked by swaging. Samples with 13 mm in diameter were obtained. They were forging at the reduction ratios of 15%. After deformation, microstructure was evaluated by optical microscopy in each condition. Also, Vickers microhardness of samples was measured and phase constitution was evaluated using XRD analysis

Caracterização microestrutural de uma estrutura tubular aeronáutica submetida a sucessivos reparos de solda TIG

This work examines the possible effects of successive repair procedures on the microstructure of welded steel SAE 4130 by TIG welding process. Discussions and results were made about the metallographic analysis , non-metallic inclusions and microhardness tests , which were conducted on samples taken from the cradle engine component after the end of its life , a model airplane T-27 Tucano , made by EMBRAER and belonging were performed FAB . The choice of such component is due to the fact that this is critical to flight safety since it provides support for the aircraft engine . Thus regions of the weld metal , base metal and heat affected , with samples of the original weld bead , free of weld bead and also with four rework procedures for TIG welding zone were analyzed . It was found that after the fourth rework there is an increase in the amount of martensite , which may weaken the material with respect to resistance to fatigue. It was also found that the regions of the heat affected zone and weld metal have higher microhardness values when compared to those found in the base metal due to favoring the formation of ferritic and tempered martensite microstructures . Moreover, a welding process promotes a region with less non-metallic inclusions than metal base , which also explains the difference in the results obtained

Propriedades físicas de vidros Sb2O3-P2O5

This work presents experimental results of some physical properties of antimony phosphate glasses with compositions (x) Sb2O3 - (1-x) P2O5 (x = 0.75, 0.85, 0.90). Mechanical, thermal, optical and electrical properties were investigated: density, elastic moduli (Young's moduli and Poisson's ratio), Vickers microhardness, coefficient of thermal expansion, glass transition temperature, refractive index and electrical conductivity (for x = 0.75). There was no evidence of electronic conductivity by bipolaron hopping. Measurements of energy dispersive spectroscopy (EDS) showed that volatilization of Sb2O3 takes place during the glass melting

Caracterização da liga do sistema binário Ti-15Mo para aplicações biomedicas

As they have excellent mechanical properties, corrosion resistance and biocompatibility, much research has been conducted with respect to biomedical applications of titanium alloys. This work aims to study the experimental system binary alloy Ti-15Mo, in the raw state of fusion and heat treatment after homogenization, solubilization and calcination (simulating conditions employed for nanotube growth) targeting biomedical applications. Samples were obtained by casting the components in an electric arc furnace with inert atmosphere of argon. After obtaining the alloy, it was heat treated at three different heat treatments, namely homogenizing, calcining and simulation solubilization. The phases present were analyzed by X-ray diffraction, optical microscopy and microhardness testing

Usinabilidade e integridade superficial de implantes dentários

Pós-graduação em Engenharia Mecânica - FEIS

Estudo da fadiga em liga de alumínio aeronáutico 7475-T761

This work will address the study of fatigue conditions with constant load in an alloy of aluminum analysis 7475 - T761, so we can better understand the conditions of the aircrafts which contain this alloy in their structures. A literature review, which was discussed the concepts of fracture mechanics, fatigue, aeronautical components, chemical analysis of aluminum alloys, fatigue problems that appears in the aircrafts, metallographic analysis, and testing of optical microscopy tensile, fatigue and microhardness, surface analysis (MEV) study of the chemical composition of the alloy in question, the main causes of crashes, was performed, completing the work, analysis of data from tensile test, hardness and fatigue together with the interpretation of images of optical microscopy and scanning electron was taken. The data indicated the high mechanical strength of the alloy, along with its microstructure indicating elongated grains and high surface contour, which shows such resistance by hindering the movement of dislocations. The grooves are clearly shown in the MEV images as well as the classic with increased fatigue loading and subsequent reduction of the number of cycles to rupture behavior shown in the graphs. Therefore we observed the optimal behavior is supported by the league when subjected to fatigue loadings

Avaliação da aplicação de ondas de ultra-som sobre cimentos de ionômero de vidro: rugosidade superficial e dureza

The application of ultrasonic waves during the initial setting of the glass ionomer cements (GIC) has demonstrated increase of the cure speed, reduction of air bubbles and improves in some mechanical properties. The aim of this study was to evaluate the effect of the ultrasound on the microhardness and the superficial roughness in two GICs (FUJI IX GP (GC Corporation) and Ketac Molar EasyMix (3M ESPE)). Forty specimens were confectioned, twenty for evaluation of the superficial roughness and twenty for evaluation of the microhardness. Half of them received for thirty seconds the ultrasonic waves application. The readings of the roughness had been carried before and after the toothbrushing test. The twenty remaining specimens had been polished with abrasive sandpapers of decreasing granulations and submitted to the hardness test. The results, analyzed for the variance analysis (ANOVA) (p<0,05), had demonstrated increase of the hardness for all the groups with the application of ultrasonic waves, being bigger for the Ketac Molar EasyMix. The ultrasound application also caused significant reduction of the superficial roughness for the Ketac Molar EasyMix. After the toothbrushing test, this last property increased for all the materials. It could be concluded that the application of ultrasonic waves was effective in increasing the superficial hardness of the materials and that it improved the roughness of the Ketac Molar EasyMix before the toothbrushing test.