999 resultados para Alface - Doenças e pragas - Controle
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Pós-graduação em Agronomia (Entomologia Agrícola) - FCAV
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Pós-graduação em Agronomia (Proteção de Plantas) - FCA
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Pós-graduação em Agronomia (Proteção de Plantas) - FCA
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Pós-graduação em Agronomia (Produção Vegetal) - FCAV
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Pós-graduação em Agronomia - FEIS
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Pós-graduação em Agronomia (Proteção de Plantas) - FCA
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Pós-graduação em Agronomia (Genética e Melhoramento de Plantas) - FCAV
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Pós-graduação em Agronomia (Genética e Melhoramento de Plantas) - FCAV
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Pós-graduação em Agronomia - FEIS
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Pós-graduação em Agronomia (Proteção de Plantas) - FCA
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Pós-graduação em Agronomia (Entomologia Agrícola) - FCAV
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Pós-graduação em Agronomia (Horticultura) - FCA
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Pós-graduação em Agronomia (Proteção de Plantas) - FCA
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Pós-graduação em Agronomia (Genética e Melhoramento de Plantas) - FCAV
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The use of pesticides to manage pest problems in agriculture has become a common practice around the world. Pesticides consist in chemical substances or biological agents that act preventing, destroying, repelling or mitigating the damage caused by pests in agriculture. In order to a successful treatment, the correct dosage of pesticide has to be applied for each kind of culture. In this context, this project aims to quantify the levels of the active ingredients Imidacloprid and Chlorpyrifos present in formulated technical products and compare with the reported in the ir commercial leaflets. The analyzes were performed by Ultra Performance Liquid Chromatography coupled to a photodiode array detector (CLUE-DAD). The identification of Imidacloprid and Chlorpyrifos in the samples was realized by comparison of the time of retention and UV spectre of those substances with the commercials patterns, resulting in a excellent method specificity of the method. In the scope of determination of active ingredients in formulated products, the method developed showed good sensitivity in the applied conditions, with suitables limits of detection (4,2.10-² mg L-¹ for Imidacloprid and 1,1.10-¹ mg L-¹ to Chlorpyrifos) and quantitation (1,4.10-¹ mg L-¹ and Imidacloprid 3,6.10-¹ mg L-¹ to Chlorpyrifos) for the concentrations found in matrices analyzed. Furthermore, good results were obtained to the method accuracy with coeficiente of variance values in the range of 0,6 to 0,7% for repeatability (intra-day) and 0,4 to 0,58% for intermediate precision (inter- day). The accuracy of the method was determined by recovery tests, the values were comprised in the range of 98 102%. According to the recommendations of the Associação Brasileira de Normas Técnicas, these values show good accuracy of the method. The concentrations obtained in the quantification of the active ingredients in formulated products showed values within permited by ABNT, 60.1% (w/v) ± 0.6%...