Applicazione di reticoli di Bragg "chirped" per il monitoraggio strutturale di laminati CFRP

L’uso dei materiali compositi è andato aumentando negli ultimi decenni per la loro elevata rigidezza, la resistenza specifica e il possibile risparmio, notevole in termini di peso dell’intera struttura. Tali materiali introducono però nuove problematiche riguardanti le modalità di danneggiamento e il comportamento a fatica. Mentre questi fenomeni sono relativamente ben compresi nei materiali metallici, per una struttura in composito non esistono ancora modelli in grado di predire con sufficiente affidabilità l’evoluzione del danneggiamento. Negli ultimi anni la ricerca si è focalizzata sullo sviluppo di sistemi in grado di rilevare la presenza e l’evoluzione del danno, definiti Structural Health Monitoring Systems, ovvero sistemi di monitoraggio strutturale. Il danneggiamento strutturale può così essere individuato e identificato per mezzo di sensori distribuiti integrati nella struttura stessa, aventi la possibilità di trasmettere queste informazioni a un sistema di analisi esterno permettendo di valutare lo stato di degrado della struttura in tempo reale. In questo contesto si inseriscono le attività di ricerca sulle strutture intelligenti che, inglobando al loro interno opportune tipologie di sensori e attuatori, sono in grado di monitorare l’ambiente fisico operativo, raccoglierne e interpretarne le informazioni per poi rispondere ai cambiamenti della struttura in modo appropriato attraverso gli attuatori. L’impiego di sensori e attuatori inglobati nelle strutture offre molteplici vantaggi rispetto ai sistemi di trasduzione e attuazione convenzionali. L’attività di ricerca condotta in questa tesi è rivolta all’indagine di tecniche di SHM per mezzo di sensori a fibra ottica. Essi presentano molteplici peculiarità che li rendono i candidati ideali per queste applicazioni. Esistono diversi tipi di sensori che utilizzano le fibre ottiche. Nel presente lavoro si sono utilizzati sensori di deformazione basati sui reticoli di Bragg (FBG) chirped. Questi sensori sono costituiti da un reticolo inscritto all’interno della fibra, che ha l’effetto di riflettere solo alcune lunghezze d’onda della luce incidente. Se le proprietà geometriche del reticolo cambiano per effetto di una deformazione, cambia anche la forma dello spettro riflesso. Inoltre, con il tipo di sensore usato, è possibile correlare lo spettro con la posizione di eventuali danneggiamenti interni al materiale. Gli obbiettivi di questa ricerca sono di verificare gli effetti della presenza di una fibra ottica sulle caratteristiche meccaniche di un laminato e di trovare un legame tra la risposta in frequenza del sensore FBG e lo stato tensionale e il grado di danneggiamento di un componente in composito.

Optical and structural properties of InAlN/GaN Bragg reflectors examined by transmission electron microscopy and electron energy loss spectroscopy

Molecular beam epitaxy growth of ten-period lattice-matched InAlN/GaN distributed Bragg reflectors (DBRs) with peak reflectivity centered around 400nm is reported including optical and transmission electron microscopy (TEM) measurements [1]. Good periodicity heterostructures with crack-free surfaces were confirmed, but, also a significant residual optical absorption below the bandgap was measured. The TEM characterization ascribes the origin of this problem to polymorfism and planar defects in the GaN layers and to the existence of an In-rich layer at the InAlN/GaN interfaces. In this work, several TEM based techniques have been combined.

Optoelectronic Properties of InAlN/GaN Distributed Bragg Reflector Heterostructure Examined by Valence

High-resolution monochromated electron energy loss spectroscopy (EELS) at subnanometric spatial resolution and <200 meV energy resolution has been used to assess the valence band properties of a distributed Bragg reflector multilayer heterostructure composed of InAlN lattice matched to GaN. This work thoroughly presents the collection of methods and computational tools put together for this task. Among these are zero-loss-peak subtraction and nonlinear fitting tools, and theoretical modeling of the electron scattering distribution. EELS analysis allows retrieval of a great amount of information: indium concentration in the InAlN layers is monitored through the local plasmon energy position and calculated using a bowing parameter version of Vegard Law. Also a dielectric characterization of the InAlN and GaN layers has been performed through Kramers-Kronig analysis of the Valence-EELS data, allowing band gap energy to be measured and an insight on the polytypism of the GaN layers.

Método de calibración para interrogadores de redes de Bragg en fibra óptica

Se ha desarrollado un método de calibración de interrogadores de redes de Bragg en fibra óptica que compara la respuesta del equipo de prueba con un simulador de red de Bragg compuesto por un filtro sintonizable unido a un espejo de fibra óptica. La longitud de onda simulada obtenida se mide con un interferómetro de referencia calibrado en el Instituto de Óptica del Consejo Superior de Investigaciones Científicas (IO?CSIC). Este método de calibración ha sido aplicado para calibrar varios tipos de interrogadores de redes de Bragg: estáticos y dinámicos. La incertidumbre en la calibración absoluta de los interrogadores es de ±88 pm, y es debida principalmente a la anchura espectral del filtro que simula la red de Bragg. Sin embrago, en calibraciones relativas la incertidumbre baja a ±3 pm, dominado por la incertidumbre en la calibración del interferómetro de referencia.

Packaging and testing of fiber Bragg gratings for use as strain sensor for rock specimens

This paper reports a packaging and calibration procedure for surface mounting of fiber Bragg grating (FBG) sensors to measure strain in rocks. The packaging of FBG sensors is performed with glass fiber and polyester resin, and then subjected to tensile loads in order to obtain strength and deformability parameters, necessaries to assess the mechanical performance of the sensor packaging. For a specific package, an optimal curing condition has been found, showing good repeatability and adaptability for non-planar surfaces, such as occurs in rock engineering. The successfully packaged sensors and electrical strain gages were attached to standard rock specimens of gabbro. Longitudinal and transversal strains under compression loads were measured with both techniques, showing that response of FBG sensors is linear and reliable. An analytical model is used to characterize the influences of rock substrate and FBG packaging in strain transmission. As a result, we obtained a sensor packaging for non-planar and complex natural material under acceptable sensitivity suitable for very small strains as occurs in hard rocks.

Development and Testing of a Fiber Bragg Grating Strain Sensor for Uniaxial Compression of Rock Specimens

Los sensores de fibra óptica son una tecnología que ha madurado en los últimos años, sin embargo, se requiere un mayor desarrollo de aplicaciones para materiales naturales como las rocas, que por ser agregados complejos pueden contener partículas minerales y fracturas de tamaño mucho mayor que las galgas eléctricas usadas tradicionalmente para medir deformaciones en las pruebas de laboratorio, ocasionando que los resultados obtenidos puedan ser no representativos. En este trabajo fueron diseñados, fabricados y probados sensores de deformación de gran área y forma curvada, usando redes de Bragg en fibra óptica (FBG) con el objetivo de obtener registros representativos en rocas que contienen minerales y estructuras de diversas composiciones, tamaños y direcciones. Se presenta el proceso de elaboración del transductor, su caracterización mecánica, su calibración y su evaluación en pruebas de compresión uniaxial en muestras de roca. Para verificar la eficiencia en la transmisión de la deformación de la roca al sensor una vez pegado, también fue realizado el análisis de la transferencia incluyendo los efectos del adhesivo, de la muestra y del transductor. Los resultados experimentales indican que el sensor desarrollado permite registro y transferencia de la deformación fiables, avance necesario para uso en rocas y otros materiales heterogénos, señalando una interesante perspectiva para aplicaciones sobre superficies irregulares, pues permite aumentar a voluntad el tamaño y forma del área de registro, posibilita también obtener mayor fiabilidad de resultados en muestras de pequeño tamaño y sugiere su conveniencia en obras, en las cuales los sistemas eléctricos tradicionales tienen limitaciones. ABSTRACT Optical fiber sensors are a technology that has matured in recent years, however, further development for rock applications is needed. Rocks contain mineral particles and features larger than electrical strain gauges traditionally used in laboratory tests, causing the results to be unrepresentative. In this work were designed, manufactured, and tested large area and curved shape strain gages, using fiber Bragg gratings in optical fiber (FBG) in order to obtain representative measurement on surface rocks samples containing minerals and structures of different compositions, sizes and directions. This reports presents the processes of manufacturing, mechanical characterization, calibration and evaluation under uniaxial compression tests on rock samples. To verify the efficiency of rock deformation transmitted to attached sensor, it was also performed the analysis of the strain transfer including the effects of the bonding, the sample and the transducer. The experimental results indicate that the developed sensor enables reliable measurements of the strain and its transmission from rock to sensor, appropriate for use in heterogeneous materials, pointing an interesting perspective for applications on irregular surfaces, allowing increasing at will the size and shape of the measurement area. This research suggests suitability of the optical strain gauge for real scale, where traditional electrical systems have demonstrated some limitations.

DRFXR.1: a Fortran computer program to calculate crystallographic D-spacings and Bragg angles /

"U.S. Atomic Energy Commission Contract AT(29-1)-1106."

Asymmetric Bragg mirrors for the reduction of emission wavelength dependence on the viewing angle in organic microcavity light emitting diodes

Organic microcavity light emitting diodes typically exhibit a blue shift of the emitting wavelength with increasing viewing angle. While the wavelength shift can be reduced with the appropriate choice of organic materials and metal mirrors, for further reduction of the emission wavelength shift it is necessary to consider a mirror whose phase shift can partly compensate the effect of the change of optical path within the cavity. In this work, we used a genetic algorithm (GA) to design an asymmetric Bragg mirror in order to minimize the emission wavelength shift with viewing angle. Based on simulation results, the use of asymmetric Bragg mirrors represents a promising way to reduce the emission wavelength shift. Detailed comparison between GA optimized and conventional Bragg mirrors in terms of resonant wavelength dependence on the viewing angle, spectral narrowing, and brightness enhancement is given. (C) 2004 Elsevier B.V. All rights reserved.

Microchanneled chirped fiber Bragg grating formed by femto-second laser aided chemical etching for refractive index and temperature measurements

In this work, a microchanneled chirped fiber Bragg grating (MCFBG) is proposed and fabricated through the femtosecond laser-assisted chemical etching. The microchannel (~550 µm) gives access to the external index liquid, thus inducing refractive index (RI) sensitivity to the structure. In the experiment, the transmission bands induced by the reduced effective index in the microchannel region were used to sense the surrounding RI and temperature changes. The experimental results show good agreement with the theoretical analysis. The proposed MCFBG offers enhanced RI sensitivity without degrading the robustness of the device showing good application potential as bio-chemical sensors.

Tunable compensation of second and third order dispersion by non-uniformly strained chirped fibre Bragg grating

A novel fibre grating device is demonstrated with tuneable chromatic dispersion slope. The tuning range is 70 to 190 ps/nm and 0 to 25 ps/nm2 for the second and third order dispersion, respectively.

The interrogation and multiplexing of long period grating curvature sensors using a Bragg grating based, derivative spectroscopy technique

A long period grating is interrogated with a fibre Bragg grating using a derivative spectroscopy technique. A quasi-linear relationship between the output of the sensing scheme and the curvature experienced by the long period grating is demonstrated, with a sensitivity of 5.05 m and with an average curvature resolution of 2.9 × 10-2 m-1. In addition, the feasibility of multiplexing an in-line series of long period gratings with this interrogation scheme is demonstrated with two pairs of fibre Bragg gratings and long period gratings. With this arrangement the cross-talk error between channels was less than ± 2.4 × 10-3 m-1.

Extended range interrogation of wavelength division multiplexed fibre Bragg grating sensors using an arrayed waveguide grating

A technique for interrogating multiplexed fibre Bragg grating (FBG) sensors using an arrayed waveguide grating (AWG) is described. The approach considerably extends the sensing range from that achieved previously, while providing a strain resolution of 17nevHz at 30 Hz.

Extended-range, low coherence dual wavelength interferometry using a superfluorescent fibre source and chirped fibre Bragg gratings

We describe an all-fibre, passive scheme for making extended range interferometric measurements based on the dual wavelength technique. The coherence tuned interferometer network is illuminated with a single superfluorescent fibre source at 1.55 µm and the two wavelengths are synthesised at the output by means of chirped fibre Bragg gratings. We demonstrate an unambiguous sensing range of 270 µm, with a dynamic range of 2.7 × 10 5.

High-resolution, wavelength-division-multiplexed in-fibre Bragg grating sensor system

A novel wavelength-division-multiplexed in-fibre Bragg grating sensor system combined with high resolution drift-compensated interferometric wavelength-shift detection is described. This crosstalk-free system is based on the use of an interferometric wavelength scanner and a low resolution spectrometer. A four element system is demonstrated for temperature measurement, and a resolution of ±0.1°C has been achieved.