950 resultados para Crates, of Thebes, 4th cent. B.C.
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Azomethine ylides, generated from imine-derived O-cinnamyl or O-crotonyl salicylaldeyde and α-amino acids, undergo intramolecular 1,3-dipolar cycloaddition, leading to chromene[4,3-b]pyrrolidines. Two reaction conditions are used: (a) microwave-assisted heating (200 W, 185 °C) of a neat mixture of reagents, and (b) conventional heating (170 °C) in PEG-400 as solvent. In both cases, a mixture of two epimers at the α-position of the nitrogen atom in the pyrrolidine nucleus was formed through the less energetic endo-approach (B/C ring fusion). In many cases, the formation of the stereoisomer bearing a trans-arrangement into the B/C ring fusion was observed in high proportions. Comprehensive computational and kinetic simulation studies are detailed. An analysis of the stability of transient 1,3-dipoles, followed by an assessment of the intramolecular pathways and kinetics are also reported.
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National Highway Traffic Safety Administration, Washington, D.C.
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Exhibition and sale at the American Art Galleries, New York.
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Originally published under title: The compleat confectioner. Cf. Bitting, K.G. Gastronomic bib., p. 190.
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Signed: Robert G. Simmons, chairman, Thomas F. Gallagher, member, Joseph L. Miller, member.
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No more published.
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p. 518-524 advertising.
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Mode of access: Internet.
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Portada a dos tintas con escudo y orla xilográficos.
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Contiene: Parte 1º y Parte 2º
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The translators of v. 1-3 are not known; v. 4 was translated by Frederick Clarke, who revised the translation of v. 1-3.
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Includes index.
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Palau,
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Cover title.
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"Vita."