Avaliação da microinfiltração marginal em restaurações de resina composta, quando o colágeno dentinário é mantido ou eliminado após o condicionamento ácido, alterando-se o período de armazenamento e a termociclagem

Pós-graduação em Odontologia Restauradora - ICT

Estudo comparativo in vitro da resistência ao cisalhamento de sistemas adesivos em dentina humana: uso de hipoclorito de sódio em sistemas convencionais ou primers acidificados

Pós-graduação em Odontologia Restauradora - ICT

A new surgical technique to treat corneal perforations using amniotic membrane and surgical adhesive

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Painéis aglomerados fabricados com mistura de partículas de madeiras tropicais

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Caracterização do compósito obtido a partir de borracha natural com negro e resíduos de couro aplicado como pisos e revestimentos

Pós-graduação em Ciência e Tecnologia de Materiais - FC

Dentina humana e bovina: estudo comparativo das propriedades físicas e características da hibridização de sistemas adesivos convencionais ou grander modificados: análise em mev

A adesão longitudinal continua a representar um dos maiores desafios da Odontologia moderna. Uma nova proposta para o estabelecimento do equilíbrio da adesão aos tecidos dentários surge, baseada na observação dos resultados obtidos com a tecnologia Grander para revitalização da água. Objetiva-se com o estudo verificar a influência dessa tecnologia nas propriedades físicas de dois sistemas adesivos (convencional e autocondicionante) à partir da medição da tensão superficial e do ângulo de contato; e avaliar a formação e a qualidade da camada híbrida em dentina humana e bovina. A tensão superficial de quatro diferentes líquidos (água, Single Bond- 3M, Primer do Clearfil SE Bond -Kuraray, e Bond do Clearfil SE-Kuraray), foi medida antes e após a modificação pelo procedimento Grander em aparelho goniômetro (Ramé-hart). O ângulo de contato com três substratos distintos (placa de titânio, dentina humana e dentina bovina), foi medido para os quatro líquidos também antes e após a modificação pelo procedimento Grander, também em goniômetro. A formação e qualidade da camada híbrida, foi avaliada em MEV, a partir da confecção de corpos de prova dos substratos humano e bovino, devidamente embutidos, preparados em lixas de variada granulação até a exposição de dentina, submetidos ao procedimento adesivo (SB ou CSEB) normal ou grander modificado, recebendo ao final dupla camada de resina composta Z250-3M, fotopolimerizada por 40s. Após armazenamento em estufa bacteriológica por 24h, os procedimentos para análise ao MEV foram realizados (fixação, desidratação, secagem e metalização). A estatística de Análise de Variância ANOVA e Teste de Tukey 5% revelou que: houve redução estatisticamente significante da tensão superficial para todos os líquidos Grander modificados; houve redução estatisticamente... (Resumo completo, clicar acesso eletrônico abaixo)

Avaliação in vitro da resistência adesiva de braquetes ortodônticos variando-se o tempo de armazenamento e o tipo de fotoativação: luz halógena e led

O objetivo deste estudo in vitro foi comparar os efeitos da fotoativação pelos sistemas luz halógena e LED na adesão de braquetes ortodônticos em diferentes tempos pós-colagem (imediato, 24h e 7d). Braquetes com adesivo pré-aplicado (Gemini series; APC adhesive precoated brackets; 3M Unitek, USA) foram colados na superfície vestibular de dentes bovinos. O esmalte dos dentes foi condicionado utilizando-se o primer auto-condicionante (Transbond SEP, 3M Unitek, USA) em todos os espécimes, conforme recomendações do fabricante. Setenta e dois dentes foram divididos em 2 grupos (n=36), conforme o sistema de fotoativação (luz halógena ou LED) e sub-divididos (n=12) de acordo com o tempo pós-colagem. Para os grupos luz halógena, o tempo de fotoativação foi de 20s e para os grupos LED foi de 10s. O teste de resistência ao cisalhamento foi realizado com auxílio de uma máquina de ensaios universal nos diferentes tempos pós-colagem: imediato, 24h e 7d. O valor médio de adesão para os grupos luz halógena foi de 20,01±5,24MPa e, para os grupos fotoativados pelo sistema LED 17,35±5,07MPa, sendo estes resultados estatisticamente diferentes. Quando comparado o efeito do tempo pós-colagem, os resultados revelaram que os valores de adesão foram significantemente maiores para o tempo de 7d. O resultado do teste ANOVA 2 – fatores revelou não existir diferença estatística entre a interação sistema de fotoativação e tempos pós-colagem. O teste de Tukey mostrou que para as 4 condições experimentais nos tempos imediato e 24h, os resultados não diferiram estatisticamente, independentemente do sistema de fotoativação. Somente com relação ao grupo luz halógena-7d, os resultados mostraram diferenças estatisticamente significantes. O grupo LED-7d desempenhou comportamento intermediário entre os grupos. O índice de adesivo remanescente não revelou diferenças... (Resumo completo, clicar acesso eletrônico abaixo)

Estudo das características térmicas e mecânicas de formulações de adesivos PSA HOT MELT contendo variações de borrachas SBC e resinas taquificantes

The properties of the hot melt adhesive pressure sensitive (HMPSA) using an elastomer as a base polymer a copolymer of styrene and butadiene (SBS) and variation of tackifiers resins such as hydrocarbon resins and hydrogenated hydrocarbon were investigated. The formulations were prepared by mixing process within shear. The adhesives prepared were evaluated in test Brookfield viscosity and softening point Ring and Ball to compare the formulations and the influence of variations in raw materials. Infrared analyzes were performed to detect the reactions between the inputs and investigate the chemical interactions of the same properties of the adhesive. In thermal analysis, the assay was performed thermogravimetry (TG) and diferencial exploratory calorimetry (DSC). Were investigated the parameters of the tensile test on each of the formulations. Finally, were analysed comparatively the basic formulations of adhesives with their respective raw materials

Aproveitamento de resíduos de laminação da madeira para a produção de painel estrutural

Products derived from wood or engineered products are becoming interesting alternatives to the replacement of solid wood in various applications, from structural components to the furniture industry and packaging. Among these products, there are panels built by strands, particles and fibers, each one having their particular characteristics and potential of use. Since the different types of panels are produced, waste generation is part of the process, and that more technological it is, it still generates losses of raw materials. Based on the need for rational use of raw materials and using almost full of industrially processed wood, It arises the proposal of this work, which seeks to use waste from the lamination, like pieces of strands, broken strands, strands rough, cracked strands to produce panels with structural characteristics of the OSL panel (Oriented Strand Lumber), LSL (Laminated Strand Lumber) and OSB (Oriented Strand Lumber). Besides the use of waste, this paper seeks an alternative to the use of the adhesive, because the industry uses formaldehyde-based adhesives, which over the press, they emit large amounts of formaldehyde, which is very aggressive to humans and environment. The panels made with polyurethane resin based on castor oil and hot-pressed were characterized by physical and mechanical tests according to specifications of European Standard (EN). High values of tensile strength, elastic modulus and density were found in the results of tests. Adding to stable values of swelling and moisture content, the panel studied adds attractive features to the panel market, especially in the civil construction

Avaliação do tempo e da concentração do condicionamento com ácido fluorídrico sobre a resistência de união entre cerâmica e cimento resinoso

The aim of this study was to verify through microtensile test the influence of time and concentration of surface conditioning with hydrofluoric acid and its interference in the adhesion of dual resin cement to porcelain.We used 32 bodies of glass-ceramic lithium disilicate system IPS e.max Press LT with dimensions of 6mm thick, 8 mm in length and 8 mm in length, which will be molded to obtain composite resin blocks corresponding to blocks ceramics. Ceramic and resin blocks were divided into 16 groups (n = 4) and numbered according to the concentration of hydrofluoric acid (2.5%, 5%, 7.5% and 10%) and conditioning time (20 seconds, 40 seconds, 1 minute and 2 minutes). The blocks were cleaned in ultrasonic apparatus with distilled water and dried with compressed air, subjected to acid etching and air-jet washed with water, dried with compressed air and received application of silane agent Monobond-S, followed by adhesive Excite ( Ivoclar Vivaden). Each ceramic block was bonded to the corresponding block of resin through the resin cement Multilink Automix. The specimens were cut to obtain nine micro samples for each set of ceramic-resin with 1 mm X 1 mm X 12 mm in length, which were submitted to microtensile test. The results were analyzed with descriptive statistics and analysis of variance with significance level of 5%, revealing that there were statistically significant (p = 0.000001 <0.05). From the Tukey test can be concluded that etching with hydrofluoric acid and 2.5% for 120 seconds gave the best bond strength, however, no statistical difference between the conditioning with the same acid in the concentration of 5.0% for 20 to 40 seconds

Desempenho estrutural de vigas em madeira laminada colada armada

The objective of the present work was to evaluate Pinus’ glued laminated timber (glulam) beams and steel reinforced glulam beams, using PU mono-component adhesive in lamination step and epoxy adhesive to bond steel bars. The mechanical performance was verified through bending test, and the adopted method based on homogenized section, to considerate the differences between wood and steel mechanical properties. The homogenization section method proved itself effective in obtaining the stiffness of the parts in MLCA. The stiffness of reinforced beams increased 91% in comparison with glulam beams, differing only 5.5 % from value of stiffness calculated

Efeito do tratamento da superfície dental com os lasers Nd:YAG e Er: Yag na adesão da resina composta à dentina recém clareada

To evaluate the effect of surface treatment with Er:YAG and Nd:YAG laser on resin composite bond strength to recently bleached dentin. Material and Methods: In this study 120 bovine incisors were used and distributed into two groups: Group C: without bleaching treatment; Group B: with bleaching treatment (35% hydrogen peroxide). Each group was divided into three subgroups: Subgroup N: without laser treatment; Subgroup Nd: irradiation with Nd:YAG laser; Subgroup Er: irradiation with Er:YAG laser. Next, the adhesive system (Adper Single Bond 2) was applied and composite buildups were constructed with Z350 composite. The teeth were sectioned to obtain dentin-resin sticks (1x1mm) and analyzed by microtensile bond testing. The data were statistically analyzed by the ANOVA and Tukey tests. Results: The results showed that the bond strength values in the bleached control group (16.17 MPa) presented no significant difference in comparison with the group bleached and irradiated with Er:YAG laser (14.69 MPa). The non bleached control group (26.79 MPa) presented significant difference in bond strength when compared with the non bleached group irradiated with Er:YAG laser (22.82 MPa) and with the group treated by bleaching and irradiation with Nd:YAG laser (28,792 MPa). The group without bleaching treatment and irradiated with Nd:YAG (36.1 MPa) presented a significant increase in bond strength in comparison with the other groups. Conclusion: The use of Nd:YAG laser on bleached specimens was able of completely reversing the immediate effects of bleaching, obtaining bond strength values similar to those of the control group

Avaliação da colagem de suportes utilizados para fixar cabos elétricos em aeronaves

The most usual method to fix supports that hold the vast majority of electrical cables on an aircraft is accomplished by using, for this purpose, rivets. However, this procedure may some cause some inconveniences such as the need of effecting holes in the structure that is intended to fix these supports, thus decreasing resistance of the structure. In order to have an alternative to seek an increase in the performance of structured materials, the aircraft industry, like other industries, have been studying the use of collage as a method of replacing this usual forms. Against this backdrop, this paper aims to assess the strength and durability of a joint bonded using the adhesive EA9394, manufactured by company Henkel Corporation, and perform a careful survey of the mechanical performance of riveted structures, taking into account different types of conditioning environment and thus create a database that can be used by the aerospace industry

Análise do desempenho físico-mecânico de painéis compensados de Pinus sp. produzidos com adesivos aquosos a base de poliacetato de vinila e de homopolímero vinílico

This study aimed to evaluate the physico-mechanical performance of three PVA adhesive formulations according to the Brazilian standards for plywood testing and to evaluate the results with those presented in the technical literature and specified in normative documents. The study presents the production process of the panels, the obtaining of samples and, finally, the implementation of physico-mechanical characterization tests based on plywood Brazilian standards. For the panels production it was used a gramature of 120 g / m² and applied a pressure of 15 bars and two temperature combinations and pressing time for each adhesive. The commercial adhesives used were PVA 1810, PVA 1060 and Vinyltec 239. The physical tests conducted were thickness swelling, density, moisture content and water absorption. The mechanical tests were static flexion, for the determination of elasticity modulus (MOE) and rupture modulus (MOR), and shear in the glue line. Among the three formulations studied none showed good performance in the presence of water. However, other trials in the adhesive showed better results and closer to the commercially equivalent used, in the case the urea-formaldehyde, was the PVA 1810, that can be applied in non-structural uses and in environments without the presence of moisture

Aplicação de adesivos estruturais em painéis de carros

The automobile industry is increasingly interested in reducing vehicle weight for greater speed, lower fuel consumption and emissions, through innovation of materials and processes. One way to do this is to seek the replacement of conventional processes by the use of structural adhesives. Structural adhesives are highly resistant materials, which can replace rivets, bolts and welds allowing the substrate / adhesive assemble is stronger than the substrate itself. One of the major advantages of gluing with respect to welding is its esthetic appearance, since it does not leave marks. For this reason, parts to be soldered require a minimum thickness so that the marks do not appear, since the pieces from gluing have no restriction as to the thickness. By replacing the vibration welding process for gluing process of the instrument panel parts of an automobile, one obtains a reduction of the thickness of the parts and therefore it decreases the weight of the car. This work aims to study the various structural adhesives that already exist on the market to be applied on the instrument panel. The mechanical test performed to measure the maximum adhesive strength was the Lap Shear Test at 23°C (room temperature), -35°C and 85°C. The types of adhesives used were the hot-melt and the bi-component. By the results obtained, it is in favor using the bi-component for application to the union of instrument panel parts