948 resultados para Determinação da concentração


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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

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Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

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Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

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Pós-graduação em Química - IQ

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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

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In order to enable the reuse of the large surplus volume of petroleum produced water for irrigation of crops inedible, the quality evaluation of this water is very important. This work aimed to evaluate the effectiveness of the diffusive gradient in thin films technique (DGT) for the determination of labile Cu (II), Mn (II) and Zn (II) in petroleum produced water destined to reuse in agriculture. Samples were collected at the exit of the wastewater treatment plant (WWTP) (after separation oil/water and flotation) of a Petrobrás onshore production region. Basically, the laboratory experiments with DGT devices involved the evaluation of the behavior of the main variables of the technique for determination of analytes in the samples (diffusion coefficients, immersion time, fractionation of organic and inorganic species, and performance of diffusion gels with different porosities, among others). Also, experiments were conducted based on the solid phase extraction (SPE) protocol with Chelex- 100 resin using previously established protocols to support the study. During the project the possibility of in situ immersions in water treatment plants was evaluated. The DGT technique presented satisfactory results for determination of Mn in produced water, and can be used for in situ determinations. However, the results obtained for Cu and Zn show the need of additional studies

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In the competitive judo, the form as a trainer organizes the process of his/her athlete's training is a very important task for a good acting and a better use of the technical procedures. There is great importance in determining the exercise intensity for the judocas training due to the interest for the high income in several competitions, and few studies returned for this research area, involving those athletes' different physiologic conditions. Therefore, it is necessary to improve protocols of physical evaluation for this modality, increasing his/her applicability. The present study aimed at to verify the validity of a protocol of specific aerobic test of the judo (technique ipon-seoi-nague), no exhausting, adapted of the method of CHASSAIN (1986), using deltas of variations of the lactacidemia and of the Scale of Perception of Effort of Borg, in athletes well. The test adapted to the judo constituted of four exercise series with two efforts similar (double) of 180 seconds with one interval of 90 seconds among them. The series of exercises were accomplished in consecutive days. The intensities of the double tests were of 85%, 95%, 105% and 115% of the minimum lactato for each participant. This work used the technique ipon-seoi-nague, obeying the reasons effort-pause individualized for each athlete, that you/they correspond to the intensities of exercises proposed by the protocol of CHASSAIN (1986). In that way, the athletes applied a blow (maximum speed) and they rested some seconds, depending on the regime effort-pause of the session. At the end of each collection collection of blood (25NL) of each participant's earlobe was accomplished, seeking to measure the concentration of sanguine lactato. The collections were accomplished at the end of the first and of the second efforts, in each one of the series. For the analysis of the Perception of the athletes' Effort, the Scale of Perception... (Complete abstract click electronic access below)

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Preeclampsia is a specific disorder of pregnancy, characterized by arterial hypertension and proteinuria detected after 20 weeks of gestation. This pathology is associated with hyperuricemia, higher levels of pro-inflammatory cytokines, enhanced leukocyte activation and oxidative stress. Adenosine deaminase (ADA) is an enzyme present in all human tissues and, it is involved with the maturation of the immune system. Although its function is not fully understood, ADA is considered an indicator of cellular inflammation and, its increased serum concentration is observed in inflammatory diseases, such as tuberculosis and rheumatoid arthritis. This study aimed to assess serum ADA levels in preeclamptic patients (PE) compared with normotensive pregnant (NT) and non-pregnant women (NP), and to correlate these values with TNF-α and IL-1β production. Ninety pregnant women were included: 60 were pre-eclamptic and 30 were normotensive matched for gestational age. As control group 20 healthy non-pregnant women matched with pregnant for age were included. Peripheral blood mononuclear cells (PMMC) obtained from the three groups studied were cultured with or without lipopolysaccharide (LPS) for 18h at 37oC, and TNF-α and IL-1β production was assessed in the supernatant of cultures by enzyme immunoassay (ELISA). ADA plasmatic concentration was determined by colorimetric method. The results show that ADA plasma levels were significantly higher in PE group compared with NT and NP groups. A positive correlation between ADA and uric acid levels was detected in preeclamptic women. There was no significant difference in relation to ADA levels when PE patients were classified in early and late-onset PE. The endogenous production of IL-1β and TNF-α by PBMC was significantly higher in PE group than in NT and NP women, showing the activation state of these cells in PE. LPS induced...(Complete abstract click electronic access below)