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A new palladium(II) complex with methionine sulfoxide was synthesized and characterized by a set of chemical and spectroscopic techniques. Elemental and mass spectrometry analyses of the solid complex fit to the composition [Pd(C5H10NO3S)(2)]center dot H2O. C-13 NMR, [H-1-N-15] NMR and infrared spectra indicate coordination of the amino acid to Pd(II) through the carboxylate and amino groups in a square planar geometry. The complex is soluble in water.Biological activity was evaluated by cytotoxic analysis using HeLa cells. Determination of cell death was assessed using a tetrazolium salt colorimetric assay, which reflects the cells viability. After incubation for 48 h, 20% of cell death was achieved at a concentration of 200 mu mol L-1 of the complex. (c) 2006 Elsevier B.V. All rights reserved.

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In this article some considerations obtained during the utilization of rotor response analysis techniques in hydraulic powerplants are discussed. An applied research work was carried out in two hydraulic turbines analysing the rotor response both theoretically and experimentally. A developed mathematical model was used to simulate the rotordynamic behaviour of Francis and Kaplan turbines. The main dynamical effects that appear during the operation of the machines are discussed too. A series of measurements were carried out in the turbines using impact hammers to determine the modal behaviour of the units. The tests were carried out with the machine still and in operation. Some results and the comparison with the theory is presented in this article. The improved theoretical model was used for a sensitivity analysis of the different bearings to the main excitations that fake place during the machine operation. From this analysis, the best measuring points for condition monitoring were determined.

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Traditionally, an (X) over bar -chart is used to control the process mean and an R-chart to control the process variance. However, these charts are not sensitive to small changes in process parameters. A good alternative to these charts is the exponentially weighted moving average (EWMA) control chart for controlling the process mean and variability, which is very effective in detecting small process disturbances. In this paper, we propose a single chart that is based on the non-central chi-square statistic, which is more effective than the joint (X) over bar and R charts in detecting assignable cause(s) that change the process mean and/or increase variability. It is also shown that the EWMA control chart based on a non-central chi-square statistic is more effective in detecting both increases and decreases in mean and/or variability.

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A ten-dimensional super-Poincaré covariant formalism for the superstring was recently developed which involves a BRST operator constructed from superspace matter variables and a pure spinor ghost variable. A super-Poincaré covariant prescription was defined for computing tree amplitudes and was shown to coincide with the standard RNS prescription. In this paper, picture-changing operators are used to define functional integration over the pure spinor ghosts and and to construct a suitable b ghost. A super-Poincaré covariant prescription is then given for the computation of N-point multiloop amplitudes. One can easily prove that massless N-point multiloop amplitudes vanish for N < 4, confirming the perturbative finiteness of superstring theory. One can also prove the Type IIB S-duality conjecture that R4 terms in the effective action receive no perturbative contributions above one loop. © SISSA/ISAS 2004.

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En este documento se presentan los cuadros regionales y nacionales con datos estadísticos de la industria eléctrica en los seis países de Centroamérica (Costa Rica, El Salvador, Guatemala, Honduras, Nicaragua y Panamá), actualizados a 2013. Contiene información sobre la capacidad instalada, la producción y la demanda en cada uno de los países y por tecnología, así como de los mercados mayoristas y regulados de electricidad. Esta edición también incluye cuadros y gráficos de precios finales de la electricidad para los principales grupos de consumidores y un anexo con información de la industria eléctrica de Belice.

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The objective of this work was to evaluate the anesthetic effect of clove oil and benzocaine on the hematology and osmotic fragility of erythrocytes in tambaqui (Colossoma macropomum). Thirty adult fish were evaluated in three treatments: a control, without anesthetic; anesthesia with clove oil at 50 mg L-1; and anesthesia with benzocaine at 100 mg L-1. Blood was collected for hemogram determination, and a test for the erithrocyte osmotic-fragility was applied. The utilized doses of clove oil and benzocaine are not appropriate for hematologic studies to establish reference values for tambaqui because they cause significant changes of the hematologic parameters, such as leukocytosis and iatrogenic hemolysis.

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