Efeitos das microestruturas bainíticas e multifásicas nas propriedades mecânicas de um aço AISI 4340

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Caracterização mecânica e análise microestrutural com a utilização da técnica de tríplice ataque do aço multifásico AISI 4350

Pós-graduação em Engenharia Mecânica - FEG

Comportamento mecânico do aço AISI 4340 revestido com WC-CrCNi; WC-10Ni; Ni-20Cr; Ni-Cr-B-Si-Fe; Cr3C2-NiCr pelo processo HVOF

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

CHARACTERIZATION OF A AISI/SAE 4340 STEEL IN DIFFERENT MICROSTRUCTURAL CONDITIONS

The 4340 are classified as ultra-high strength steels used by the aviation industry and aerospace applications such as aircraft landing gear and several structural applications, usually in quenched and tempered condition. In this situation occurs reduction of toughness, which encourages the study of multiphasic and bainitic structures, in order to maintain strength without loss of toughness. In this study, ferritic-pearlitic structure was compared to bainitic and martensitic structure, identified by the reagents Nital, LePera and Sodium Metabisulfite. Sliding wear tests of the type pin-on-disk were realized and the results related to the microstructure of these materials and also to their hardnesses. It is noted that these different microstructures had very similar behavior, concluding that all three tested pairs can be used according to the request level.

Fatigue Behavior of Weld Repaired AISI 4130 Aeronautic Steel Used in Critical Flight Safety Structures

Since the 1950s, fatigue is the most important project and operational consideration for both civil and military aircrafts. For some aircraft models the most loaded component is one that supports the motor: the Motor Cradle. Because they are considered critical to the flight safety the aeronautic standards are extremely rigorous in manufacturing them by imposing a zero index of defects on the final weld quality (Safe Life), which is 100% inspected by Non-Destructive Testing/NDT. This study has as objective to evaluate the effects of up to four successive TIG welding repairs on the axial fatigue strength of an AISI 4130 steel. Tests were conducted on hot-rolled steel plate specimens, 0.89 mm thick, with load ratio R = 0.1, constant amplitude, at 20 Hz frequency and in room temperature, in accordance with ASTM E466 Standard. The results were related to microhardness and microstructural and geometric changes resulting from welding cycles.

Sn(1-x)LaxO2 thin films deposited on AISI 304 stainless steel substrates

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Avaliação dos mecanismos de endurecimentoda liga AISI 300M submetida a diferentes ciclos de transformações martensíticas

Pós-graduação em Engenharia Mecânica - FEG

Enhancement of Corrosion Resistance AISI 304 Steel by Plasma Polymerized Thin Films

The purpose of this work is the deposition of films in order to increase the corrosion resistance of AISI 304 steel, which is a material used to construct the reactors for bioethanol production. This deposition inhibits the permeation of corrosive species to the film-metal interface. Thin films were prepared by radio-frequency plasma enhanced chemical vapor deposition (RF-PECVD) method using plasmas of hexamethyldisiloxane/argon/oxygen mixtures excited by signals of different powers. The plasma was generated by the application of RF power of 13.56 MHz to the sample holder while keeping grounded the topmost electrode and the chamber walls. The effect of the RF power on the properties of the samples was investigated by perfilometry, X-ray photoelectron spectroscopy (XPS), contact angle, and electrochemical impedance spectroscopy (EIS). The results of the corrosion resistance tests of the AISI 304 steel were interpreted in terms of the energy delivered to the growing layer by plasma excitation power.

Grinding of AISI 4340 steel with interrupted cutting by aluminum oxide grinding wheel

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Análise microestrutural e caracterização mecânica do aço AISI 4350 submetido a diferentes tratamentos térmicos

The multiphase steels are gaining increasing attention in scientific studies because of the different mechanical and microstructural properties that the material can achieve under different thermomechanical and heat treatments that can be submitted. In the present study, it was made a microstructural study thru the triple attack technic associated with optical microscopy and mechanical characterization of medium carbon AISI 4350 steel thru a tensile strength test, subjected to three routes of heat treatment: annealing, quenching and tempering and isothermal annealing. It was verified the predominance of ferrite-perlite constituent in the specimen annealed, martensitic in the quenched and tempered specimen and bainitic in the annealed isothermally specimen. The annealed material showed a higher ductility, while the hardened and tempered specimen showed the highest hardness and ultimately the bainitic specimen showed a combination of the two abovementioned mechanical properties. Thus, we proved that the multiphase steel SAE 4350 can be a versatile material with great potential for various industrial applications

Análise do perfil de dureza e microestrutura de um aço forjado AISI A2 submetido a tratamento térmico com resfriamento em água

Due to the large use of steel in several processes around the world, there is the increasingly concern to find new materials and/or optimization and improvement of the processes, as the need to reduce the cost and a productivity increase in the primary industry, such as the siderurgy. The rolling is the most used mechanical process in the world and therefore is required the development of new tools in high volume and with optimum characteristics to support the market demand. Forged rolls used are for rolling. These rolls have heat treatment that has the purpose to achieve the appropriated mechanical properties to support the variables of the rolling process. The objective of this work is to analyze the hardness profile and the microstructure a tool steel similar to AISI A2, forged in an opened die process and submitted to heat treatment with water-cooling. The results allowed plotting a hardness profile and performing a microstructure analysis, and whereby to confirm that the heat treatment is not a quenching, but it is a material beneficiation by the hardening of superficial layer, since there is no martensitic microstructure. Therefore, this paper provides the support to future studies about the possibility to perform enhancements in this thermal heat made in the rolls produced at Gerdau Plant in Pindamonhangaba

Análise microestrutural e caracterização mecânica do aço AISI 4350 submetido a diferentes tratamentos térmicos

The multiphase steels are gaining increasing attention in scientific studies because of the different mechanical and microstructural properties that the material can achieve under different thermomechanical and heat treatments that can be submitted. In the present study, it was made a microstructural study thru the triple attack technic associated with optical microscopy and mechanical characterization of medium carbon AISI 4350 steel thru a tensile strength test, subjected to three routes of heat treatment: annealing, quenching and tempering and isothermal annealing. It was verified the predominance of ferrite-perlite constituent in the specimen annealed, martensitic in the quenched and tempered specimen and bainitic in the annealed isothermally specimen. The annealed material showed a higher ductility, while the hardened and tempered specimen showed the highest hardness and ultimately the bainitic specimen showed a combination of the two abovementioned mechanical properties. Thus, we proved that the multiphase steel SAE 4350 can be a versatile material with great potential for various industrial applications

Análise do perfil de dureza e microestrutura de um aço forjado AISI A2 submetido a tratamento térmico com resfriamento em água

Due to the large use of steel in several processes around the world, there is the increasingly concern to find new materials and/or optimization and improvement of the processes, as the need to reduce the cost and a productivity increase in the primary industry, such as the siderurgy. The rolling is the most used mechanical process in the world and therefore is required the development of new tools in high volume and with optimum characteristics to support the market demand. Forged rolls used are for rolling. These rolls have heat treatment that has the purpose to achieve the appropriated mechanical properties to support the variables of the rolling process. The objective of this work is to analyze the hardness profile and the microstructure a tool steel similar to AISI A2, forged in an opened die process and submitted to heat treatment with water-cooling. The results allowed plotting a hardness profile and performing a microstructure analysis, and whereby to confirm that the heat treatment is not a quenching, but it is a material beneficiation by the hardening of superficial layer, since there is no martensitic microstructure. Therefore, this paper provides the support to future studies about the possibility to perform enhancements in this thermal heat made in the rolls produced at Gerdau Plant in Pindamonhangaba

Application of Mossbauer spectroscopy to the study of corrosion resistance in NaCl solution of plasma nitrided AISI 316L stainless steel

Corrosion research in steels is one of the areas in which Mossbauer spectroscopy has become a required analytical technique, since it is a powerful tool for both identifying and quantifying distinctive phases (which contain Fe) with accuracy. In this manuscript, this technique was used to the study of corrosion resistance of plasma nitrided AISI 316L samples in the presence of chloride anions. Plasma nitriding has been carried out using dc glow-discharge, nitriding treatments, in medium of 80 vol.% H-2 and 20 vol.% N-2, at 673 K, and at different time intervals: 2, 4, and 7 h. Treated samples were characterized by means of phase composition and morphological analysis, and electrochemical tests in NaCl aerated solution in order to investigate the influence of treatment time on the microstructure and the corrosion resistance, proved by conversion electron Mossbauer spectroscopy (CEMS), glancing angle X-ray diffraction (GAXRD), scanning electron microscopy (SEM) and potentiodynamic polarization. A modified layer of about 8 gin was observed for all the nitrided samples, independently of the nitriding time. A metastable phase, S phase or gamma(N), was produced. It seems to be correlated with gamma`-Fe-4 N phase. If the gamma(N) fraction decreases, the gamma` fraction increases. The gamma(N) magnetic nature was analyzed. When the nitriding time increases, the results indicate that there is a significant reduction in the relative fraction of the magnetic gamma(N) (in) phase. In contrast, the paramagnetic gamma(N) (p) phase increases. The GAXRD analysis confirms the Mossbauer results, and it also indicates CrN traces for the sample nitrided for 7 h. Corrosion results demonstrate that time in the plasma nitriding treatment plays an important role for the corrosion resistance. The sample treated for 4 h showed the best result of corrosion resistance. It seems that the epsilon/gamma` fraction ratio plays an important role in thin corrosion resistance since this sample shows the maximum value for this ratio. (c) 2008 Published by Elsevier B.V.

Magnetic Barkhausen emission in lightly deformed AISI 1070 steel

The Magnetic Barkhausen Noise (MBN) technique can evaluate both micro- and macro-residual stresses, and provides indication about the relevance of contribution of these different stress components. MBN measurements were performed in AISI 1070 steel sheet samples, where different strains were applied. The Barkhausen emission is also analyzed when two different sheets, deformed and non-deformed, are evaluated together. This study is useful to understand the effect of a deformed region near the surface on MBN. The low permeability of the deformed region affects MBN, and if the deformed region is below the surface the magnetic Barkhausen signal increases. (C) 2011 Elsevier B.V. All rights reserved.